Isolation and Elucidation Structure of 28-Hydroxy-3-Friedelanone of Nyamplung (Callophyllum inophyllum, Linn.) Leaves

The isolation triterpenoid from Nyamplung (Callophyllum inophyllum, Linn.) leaves has been conducted. The isolation was employed by maceration using ethanol as solvent and liquids extraction using ethyl acetate. Ethyl acetate extract was partitioned successively using nonpolar solvent with hexane, d...

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Autores principales:	Triana Kusumaningsih, Muhammad Widyo Wartono, Nais Puji Wijanarti
Formato:	article
Lenguaje:	EN
Publicado:	University of Brawijaya 2020
Materias:	callophyllum inophyllum linn. extraction leaf maceration triterpenoid Chemistry QD1-999
Acceso en línea:	https://doaj.org/article/00e06ab072ff4e91ade1942a44e0c920
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spelling	oai:doaj.org-article:00e06ab072ff4e91ade1942a44e0c9202021-12-02T16:39:05ZIsolation and Elucidation Structure of 28-Hydroxy-3-Friedelanone of Nyamplung (Callophyllum inophyllum, Linn.) Leaves2302-46902302-4690https://doaj.org/article/00e06ab072ff4e91ade1942a44e0c9202020-08-01T00:00:00Zhttps://jpacr.ub.ac.id/index.php/jpacr/article/view/518/pdfhttps://doaj.org/toc/2302-4690https://doaj.org/toc/2302-4690The isolation triterpenoid from Nyamplung (Callophyllum inophyllum, Linn.) leaves has been conducted. The isolation was employed by maceration using ethanol as solvent and liquids extraction using ethyl acetate. Ethyl acetate extract was partitioned successively using nonpolar solvent with hexane, dichloromethane, and diethyl ether, respectively. The diethyl ether extract was purified by column chromatography. The isolated compound of fraction D1 was obtained as white solids crystal with yield of 0.0035%. The isolated compound was determined based on the FTIR, 1HNMR, 13CNMR, HSQC, and HMBC spectra. The isolated compound was identified as 28-hydroxy-3-friedelanone.Triana KusumaningsihMuhammad Widyo WartonoNais Puji WijanartiUniversity of Brawijayaarticlecallophyllum inophyllumlinn.extractionleafmacerationtriterpenoidChemistryQD1-999ENJournal of Pure and Applied Chemistry Research, Vol 9, Iss 2, Pp 117-125 (2020)
institution	DOAJ
collection	DOAJ
language	EN
topic	callophyllum inophyllum linn. extraction leaf maceration triterpenoid Chemistry QD1-999
spellingShingle	callophyllum inophyllum linn. extraction leaf maceration triterpenoid Chemistry QD1-999 Triana Kusumaningsih Muhammad Widyo Wartono Nais Puji Wijanarti Isolation and Elucidation Structure of 28-Hydroxy-3-Friedelanone of Nyamplung (Callophyllum inophyllum, Linn.) Leaves
description	The isolation triterpenoid from Nyamplung (Callophyllum inophyllum, Linn.) leaves has been conducted. The isolation was employed by maceration using ethanol as solvent and liquids extraction using ethyl acetate. Ethyl acetate extract was partitioned successively using nonpolar solvent with hexane, dichloromethane, and diethyl ether, respectively. The diethyl ether extract was purified by column chromatography. The isolated compound of fraction D1 was obtained as white solids crystal with yield of 0.0035%. The isolated compound was determined based on the FTIR, 1HNMR, 13CNMR, HSQC, and HMBC spectra. The isolated compound was identified as 28-hydroxy-3-friedelanone.
format	article
author	Triana Kusumaningsih Muhammad Widyo Wartono Nais Puji Wijanarti
author_facet	Triana Kusumaningsih Muhammad Widyo Wartono Nais Puji Wijanarti
author_sort	Triana Kusumaningsih
title	Isolation and Elucidation Structure of 28-Hydroxy-3-Friedelanone of Nyamplung (Callophyllum inophyllum, Linn.) Leaves
title_short	Isolation and Elucidation Structure of 28-Hydroxy-3-Friedelanone of Nyamplung (Callophyllum inophyllum, Linn.) Leaves
title_full	Isolation and Elucidation Structure of 28-Hydroxy-3-Friedelanone of Nyamplung (Callophyllum inophyllum, Linn.) Leaves
title_fullStr	Isolation and Elucidation Structure of 28-Hydroxy-3-Friedelanone of Nyamplung (Callophyllum inophyllum, Linn.) Leaves
title_full_unstemmed	Isolation and Elucidation Structure of 28-Hydroxy-3-Friedelanone of Nyamplung (Callophyllum inophyllum, Linn.) Leaves
title_sort	isolation and elucidation structure of 28-hydroxy-3-friedelanone of nyamplung (callophyllum inophyllum, linn.) leaves
publisher	University of Brawijaya
publishDate	2020
url	https://doaj.org/article/00e06ab072ff4e91ade1942a44e0c920
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Isolation and Elucidation Structure of 28-Hydroxy-3-Friedelanone of Nyamplung (Callophyllum inophyllum, Linn.) Leaves

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