Effect of Reaction Time and Stability Properties of Gold Nanoparticles Synthesized by <i>p</i>-Aminobenzoic Acid and <i>p</i>-Aminosalicylic Acid

In this work, we determined the influenced of the reaction time at the synthesis of gold nanoparticles (AuNPs) by p-aminosalicylic acid and p-aminobenzoic acid as reducing agent. Besides working as a reducing agent, the p-aminobenzoic acid and p-aminosalicylic acid also simultaneously played a role...

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Autores principales: Abdul Aji, Sri Juari Santosa, Eko Sri Kunarti
Formato: article
Lenguaje:EN
Publicado: Department of Chemistry, Universitas Gadjah Mada 2020
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Acceso en línea:https://doaj.org/article/041609d56bb7446c939495cafed9ea06
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spelling oai:doaj.org-article:041609d56bb7446c939495cafed9ea062021-12-02T13:16:24ZEffect of Reaction Time and Stability Properties of Gold Nanoparticles Synthesized by <i>p</i>-Aminobenzoic Acid and <i>p</i>-Aminosalicylic Acid1411-94202460-157810.22146/ijc.44674https://doaj.org/article/041609d56bb7446c939495cafed9ea062020-03-01T00:00:00Zhttps://jurnal.ugm.ac.id/ijc/article/view/44674https://doaj.org/toc/1411-9420https://doaj.org/toc/2460-1578In this work, we determined the influenced of the reaction time at the synthesis of gold nanoparticles (AuNPs) by p-aminosalicylic acid and p-aminobenzoic acid as reducing agent. Besides working as a reducing agent, the p-aminobenzoic acid and p-aminosalicylic acid also simultaneously played a role as a capping agent/stabilizing agent. Gold ion was first mixed with the pH adjusted p-aminobenzoic acid and p-aminosalicylic acid. The mixture then heated in boiling water at 86 °C. The formation of AuNPs was indicated by the appearance of red color and analyzed with UV/Vis spectrophotometry to evaluate their surface plasmon resonance (SPR) absorption in the wavelength range 400–800 nm. The reducing ability of the reducing agents was affected by its structure. Gold nanoparticles that were synthesized with p-aminosalicylic acid were more stable, faster and had a smaller size than its counterpart that is synthesized with p-aminobenzoic acid. The stability test over a periods 5 months showed that AuNPs were relatively stable.Abdul AjiSri Juari SantosaEko Sri KunartiDepartment of Chemistry, Universitas Gadjah Madaarticlegold nanoparticlesp-aminosalicylic acidp-aminobenzoic acidChemistryQD1-999ENIndonesian Journal of Chemistry, Vol 20, Iss 2, Pp 413-421 (2020)
institution DOAJ
collection DOAJ
language EN
topic gold nanoparticles
p-aminosalicylic acid
p-aminobenzoic acid
Chemistry
QD1-999
spellingShingle gold nanoparticles
p-aminosalicylic acid
p-aminobenzoic acid
Chemistry
QD1-999
Abdul Aji
Sri Juari Santosa
Eko Sri Kunarti
Effect of Reaction Time and Stability Properties of Gold Nanoparticles Synthesized by <i>p</i>-Aminobenzoic Acid and <i>p</i>-Aminosalicylic Acid
description In this work, we determined the influenced of the reaction time at the synthesis of gold nanoparticles (AuNPs) by p-aminosalicylic acid and p-aminobenzoic acid as reducing agent. Besides working as a reducing agent, the p-aminobenzoic acid and p-aminosalicylic acid also simultaneously played a role as a capping agent/stabilizing agent. Gold ion was first mixed with the pH adjusted p-aminobenzoic acid and p-aminosalicylic acid. The mixture then heated in boiling water at 86 °C. The formation of AuNPs was indicated by the appearance of red color and analyzed with UV/Vis spectrophotometry to evaluate their surface plasmon resonance (SPR) absorption in the wavelength range 400–800 nm. The reducing ability of the reducing agents was affected by its structure. Gold nanoparticles that were synthesized with p-aminosalicylic acid were more stable, faster and had a smaller size than its counterpart that is synthesized with p-aminobenzoic acid. The stability test over a periods 5 months showed that AuNPs were relatively stable.
format article
author Abdul Aji
Sri Juari Santosa
Eko Sri Kunarti
author_facet Abdul Aji
Sri Juari Santosa
Eko Sri Kunarti
author_sort Abdul Aji
title Effect of Reaction Time and Stability Properties of Gold Nanoparticles Synthesized by <i>p</i>-Aminobenzoic Acid and <i>p</i>-Aminosalicylic Acid
title_short Effect of Reaction Time and Stability Properties of Gold Nanoparticles Synthesized by <i>p</i>-Aminobenzoic Acid and <i>p</i>-Aminosalicylic Acid
title_full Effect of Reaction Time and Stability Properties of Gold Nanoparticles Synthesized by <i>p</i>-Aminobenzoic Acid and <i>p</i>-Aminosalicylic Acid
title_fullStr Effect of Reaction Time and Stability Properties of Gold Nanoparticles Synthesized by <i>p</i>-Aminobenzoic Acid and <i>p</i>-Aminosalicylic Acid
title_full_unstemmed Effect of Reaction Time and Stability Properties of Gold Nanoparticles Synthesized by <i>p</i>-Aminobenzoic Acid and <i>p</i>-Aminosalicylic Acid
title_sort effect of reaction time and stability properties of gold nanoparticles synthesized by <i>p</i>-aminobenzoic acid and <i>p</i>-aminosalicylic acid
publisher Department of Chemistry, Universitas Gadjah Mada
publishDate 2020
url https://doaj.org/article/041609d56bb7446c939495cafed9ea06
work_keys_str_mv AT abdulaji effectofreactiontimeandstabilitypropertiesofgoldnanoparticlessynthesizedbyipiaminobenzoicacidandipiaminosalicylicacid
AT srijuarisantosa effectofreactiontimeandstabilitypropertiesofgoldnanoparticlessynthesizedbyipiaminobenzoicacidandipiaminosalicylicacid
AT ekosrikunarti effectofreactiontimeandstabilitypropertiesofgoldnanoparticlessynthesizedbyipiaminobenzoicacidandipiaminosalicylicacid
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