Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4

Lithium Ferro Phosphate Carbon Composite (LFP/C) had been synthesized using solid-state reaction method. Magnetite sand Fe3O4 was used as Fe- source in LFP/C synthesized. Calcination temperature of the sample performed at 400, 500, and 600°C. The phase and composition of samples determined by Rietv...

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Autores principales:	Zuffa Anisa, Mochammad Zainuri
Formato:	article
Lenguaje:	EN
Publicado:	University of Brawijaya 2020
Materias:	lfp/c magnetite nasicon diphosphate phase Chemistry QD1-999
Acceso en línea:	http://dx.doi.org/10.21776/jpacr.ub.2020.009.01.517 https://doaj.org/article/0717dd2cdaba46209c090234df8f7d1d
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spelling	oai:doaj.org-article:0717dd2cdaba46209c090234df8f7d1d2021-12-02T14:22:18ZSynthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4http://dx.doi.org/10.21776/jpacr.ub.2020.009.01.5172302-46902302-4690https://doaj.org/article/0717dd2cdaba46209c090234df8f7d1d2020-04-01T00:00:00Zhttps://jpacr.ub.ac.id/index.php/jpacr/article/view/517/pdfhttps://doaj.org/toc/2302-4690https://doaj.org/toc/2302-4690Lithium Ferro Phosphate Carbon Composite (LFP/C) had been synthesized using solid-state reaction method. Magnetite sand Fe3O4 was used as Fe- source in LFP/C synthesized. Calcination temperature of the sample performed at 400, 500, and 600°C. The phase and composition of samples determined by Rietveld analysis of X-ray diffraction (XRD) pattern. The dominant identified phase at 400°C was diphosphate LiFeP2O7, and the others phases were nasicon Li3Fe2(PO4)3 and hematite Fe2O3. As the temperature getting higher the diphosphate phase LiFeP2O7 transform to nasicon Li3Fe2(PO4)3.The chemical bonds, lattice vibration and other structural features of the sample were investigated using FTIR spectroscopy in range of 1400 – 400 cm-1. Specific vibration modes in LFP-1 to LFP-3 for each bonding were shown by the high intense in certain wavenumber.Zuffa AnisaMochammad ZainuriUniversity of Brawijayaarticlelfp/cmagnetitenasicondiphosphatephaseChemistryQD1-999ENJournal of Pure and Applied Chemistry Research, Vol 9, Iss 1, Pp 16-22 (2020)
institution	DOAJ
collection	DOAJ
language	EN
topic	lfp/c magnetite nasicon diphosphate phase Chemistry QD1-999
spellingShingle	lfp/c magnetite nasicon diphosphate phase Chemistry QD1-999 Zuffa Anisa Mochammad Zainuri Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4
description	Lithium Ferro Phosphate Carbon Composite (LFP/C) had been synthesized using solid-state reaction method. Magnetite sand Fe3O4 was used as Fe- source in LFP/C synthesized. Calcination temperature of the sample performed at 400, 500, and 600°C. The phase and composition of samples determined by Rietveld analysis of X-ray diffraction (XRD) pattern. The dominant identified phase at 400°C was diphosphate LiFeP2O7, and the others phases were nasicon Li3Fe2(PO4)3 and hematite Fe2O3. As the temperature getting higher the diphosphate phase LiFeP2O7 transform to nasicon Li3Fe2(PO4)3.The chemical bonds, lattice vibration and other structural features of the sample were investigated using FTIR spectroscopy in range of 1400 – 400 cm-1. Specific vibration modes in LFP-1 to LFP-3 for each bonding were shown by the high intense in certain wavenumber.
format	article
author	Zuffa Anisa Mochammad Zainuri
author_facet	Zuffa Anisa Mochammad Zainuri
author_sort	Zuffa Anisa
title	Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4
title_short	Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4
title_full	Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4
title_fullStr	Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4
title_full_unstemmed	Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4
title_sort	synthesis and characterization of lithium iron phosphate carbon composite (lfp/c) using magnetite sand fe3o4
publisher	University of Brawijaya
publishDate	2020
url	http://dx.doi.org/10.21776/jpacr.ub.2020.009.01.517 https://doaj.org/article/0717dd2cdaba46209c090234df8f7d1d
work_keys_str_mv	AT zuffaanisa synthesisandcharacterizationoflithiumironphosphatecarboncompositelfpcusingmagnetitesandfe3o4 AT mochammadzainuri synthesisandcharacterizationoflithiumironphosphatecarboncompositelfpcusingmagnetitesandfe3o4
_version_	1718391467095883776

Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4

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