Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure

We successfully prepared Au nanoparticles using the modified polyol methods and design of experiments. The desirable crystal structure and particle size of Au nanoparticles with various kinds of polyhedral and spherical shapes as well as various kinds of their morphologies or complete and rough sphe...

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Autores principales: Nguyen Thi Nhat Hang, Yong Yang, Nguyen Quang Thanh Nam, Masayuki Nogami, Le Hong Phuc, Nguyen Huu Tri, Ho Van Cuu, Nguyen Viet Long
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Publicado: MDPI AG 2021
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Acceso en línea:https://doaj.org/article/072a7b7e8b1a453cb46d3d6eed862153
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spelling oai:doaj.org-article:072a7b7e8b1a453cb46d3d6eed8621532021-11-25T17:17:50ZControlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure10.3390/cryst111112972073-4352https://doaj.org/article/072a7b7e8b1a453cb46d3d6eed8621532021-10-01T00:00:00Zhttps://www.mdpi.com/2073-4352/11/11/1297https://doaj.org/toc/2073-4352We successfully prepared Au nanoparticles using the modified polyol methods and design of experiments. The desirable crystal structure and particle size of Au nanoparticles with various kinds of polyhedral and spherical shapes as well as various kinds of their morphologies or complete and rough spherical crystal surfaces were experimentally predicted in TEM and XRD measurements according to the theoretical calculation and data. The fine crystal formation of Au nanostructures by modified polyol methods with EG, PVP, and NaBH<sub>4</sub> is of great importance to their practical applications. Our research shows that the critical nucleation, growth, and formation of sizes, shapes, and morphologies of Au nanoparticles were experimentally discussed in modified polyol methods and design of experiments. In this context, our particle size calculation can hold the greatest attraction for researchers in the field of nanoparticles.Nguyen Thi Nhat HangYong YangNguyen Quang Thanh NamMasayuki NogamiLe Hong PhucNguyen Huu TriHo Van CuuNguyen Viet LongMDPI AGarticlegold nanoparticlesmodified polyol methodscrystalsurface plasmon resonancebiomedical applicationsassemblyCrystallographyQD901-999ENCrystals, Vol 11, Iss 1297, p 1297 (2021)
institution DOAJ
collection DOAJ
language EN
topic gold nanoparticles
modified polyol methods
crystal
surface plasmon resonance
biomedical applications
assembly
Crystallography
QD901-999
spellingShingle gold nanoparticles
modified polyol methods
crystal
surface plasmon resonance
biomedical applications
assembly
Crystallography
QD901-999
Nguyen Thi Nhat Hang
Yong Yang
Nguyen Quang Thanh Nam
Masayuki Nogami
Le Hong Phuc
Nguyen Huu Tri
Ho Van Cuu
Nguyen Viet Long
Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure
description We successfully prepared Au nanoparticles using the modified polyol methods and design of experiments. The desirable crystal structure and particle size of Au nanoparticles with various kinds of polyhedral and spherical shapes as well as various kinds of their morphologies or complete and rough spherical crystal surfaces were experimentally predicted in TEM and XRD measurements according to the theoretical calculation and data. The fine crystal formation of Au nanostructures by modified polyol methods with EG, PVP, and NaBH<sub>4</sub> is of great importance to their practical applications. Our research shows that the critical nucleation, growth, and formation of sizes, shapes, and morphologies of Au nanoparticles were experimentally discussed in modified polyol methods and design of experiments. In this context, our particle size calculation can hold the greatest attraction for researchers in the field of nanoparticles.
format article
author Nguyen Thi Nhat Hang
Yong Yang
Nguyen Quang Thanh Nam
Masayuki Nogami
Le Hong Phuc
Nguyen Huu Tri
Ho Van Cuu
Nguyen Viet Long
author_facet Nguyen Thi Nhat Hang
Yong Yang
Nguyen Quang Thanh Nam
Masayuki Nogami
Le Hong Phuc
Nguyen Huu Tri
Ho Van Cuu
Nguyen Viet Long
author_sort Nguyen Thi Nhat Hang
title Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure
title_short Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure
title_full Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure
title_fullStr Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure
title_full_unstemmed Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure
title_sort controlled synthesis of au nanoparticles by modified polyol methods: determination of their size, shape, and crystal structure
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/072a7b7e8b1a453cb46d3d6eed862153
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