Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure
We successfully prepared Au nanoparticles using the modified polyol methods and design of experiments. The desirable crystal structure and particle size of Au nanoparticles with various kinds of polyhedral and spherical shapes as well as various kinds of their morphologies or complete and rough sphe...
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2021
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oai:doaj.org-article:072a7b7e8b1a453cb46d3d6eed8621532021-11-25T17:17:50ZControlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure10.3390/cryst111112972073-4352https://doaj.org/article/072a7b7e8b1a453cb46d3d6eed8621532021-10-01T00:00:00Zhttps://www.mdpi.com/2073-4352/11/11/1297https://doaj.org/toc/2073-4352We successfully prepared Au nanoparticles using the modified polyol methods and design of experiments. The desirable crystal structure and particle size of Au nanoparticles with various kinds of polyhedral and spherical shapes as well as various kinds of their morphologies or complete and rough spherical crystal surfaces were experimentally predicted in TEM and XRD measurements according to the theoretical calculation and data. The fine crystal formation of Au nanostructures by modified polyol methods with EG, PVP, and NaBH<sub>4</sub> is of great importance to their practical applications. Our research shows that the critical nucleation, growth, and formation of sizes, shapes, and morphologies of Au nanoparticles were experimentally discussed in modified polyol methods and design of experiments. In this context, our particle size calculation can hold the greatest attraction for researchers in the field of nanoparticles.Nguyen Thi Nhat HangYong YangNguyen Quang Thanh NamMasayuki NogamiLe Hong PhucNguyen Huu TriHo Van CuuNguyen Viet LongMDPI AGarticlegold nanoparticlesmodified polyol methodscrystalsurface plasmon resonancebiomedical applicationsassemblyCrystallographyQD901-999ENCrystals, Vol 11, Iss 1297, p 1297 (2021) |
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gold nanoparticles modified polyol methods crystal surface plasmon resonance biomedical applications assembly Crystallography QD901-999 |
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gold nanoparticles modified polyol methods crystal surface plasmon resonance biomedical applications assembly Crystallography QD901-999 Nguyen Thi Nhat Hang Yong Yang Nguyen Quang Thanh Nam Masayuki Nogami Le Hong Phuc Nguyen Huu Tri Ho Van Cuu Nguyen Viet Long Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure |
description |
We successfully prepared Au nanoparticles using the modified polyol methods and design of experiments. The desirable crystal structure and particle size of Au nanoparticles with various kinds of polyhedral and spherical shapes as well as various kinds of their morphologies or complete and rough spherical crystal surfaces were experimentally predicted in TEM and XRD measurements according to the theoretical calculation and data. The fine crystal formation of Au nanostructures by modified polyol methods with EG, PVP, and NaBH<sub>4</sub> is of great importance to their practical applications. Our research shows that the critical nucleation, growth, and formation of sizes, shapes, and morphologies of Au nanoparticles were experimentally discussed in modified polyol methods and design of experiments. In this context, our particle size calculation can hold the greatest attraction for researchers in the field of nanoparticles. |
format |
article |
author |
Nguyen Thi Nhat Hang Yong Yang Nguyen Quang Thanh Nam Masayuki Nogami Le Hong Phuc Nguyen Huu Tri Ho Van Cuu Nguyen Viet Long |
author_facet |
Nguyen Thi Nhat Hang Yong Yang Nguyen Quang Thanh Nam Masayuki Nogami Le Hong Phuc Nguyen Huu Tri Ho Van Cuu Nguyen Viet Long |
author_sort |
Nguyen Thi Nhat Hang |
title |
Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure |
title_short |
Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure |
title_full |
Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure |
title_fullStr |
Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure |
title_full_unstemmed |
Controlled Synthesis of Au Nanoparticles by Modified Polyol Methods: Determination of Their Size, Shape, and Crystal Structure |
title_sort |
controlled synthesis of au nanoparticles by modified polyol methods: determination of their size, shape, and crystal structure |
publisher |
MDPI AG |
publishDate |
2021 |
url |
https://doaj.org/article/072a7b7e8b1a453cb46d3d6eed862153 |
work_keys_str_mv |
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