Optimizing Natural Deep Eutectic Solvent Citric Acid-Glucose Based Microwave-Assisted Extraction of Total Polyphenols Content from <i>Eleutherine bulbosa</i> (Mill.) Bulb

Application of natural deep eutectic solvent (NADES) citric acid-glucose-based microwave-assisted extraction (MAE) method for total polyphenol content (TPC) enriches the use of Eleutherine bulbosa (Mill.) bulb more widely and commercially. Therefore, this study aims to optimize NADES citric acid-glu...

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Autores principales:	Bohari Yusuf, Selvi Jumiatul Astati, Mirhansyah Ardana, Herman Herman, Arsyik Ibrahim, Laode Rijai, Firzan Nainu, Islamudin Ahmad
Formato:	article
Lenguaje:	EN
Publicado:	Department of Chemistry, Universitas Gadjah Mada 2021
Materias:	eleutherine bulbosa mill microwave-assisted extraction natural deep eutectic solvent response surface methodology total polyphenols content Chemistry QD1-999
Acceso en línea:	https://doaj.org/article/0c1bf266337546efbab828da25a3fb22
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spelling	oai:doaj.org-article:0c1bf266337546efbab828da25a3fb222021-12-02T17:09:37ZOptimizing Natural Deep Eutectic Solvent Citric Acid-Glucose Based Microwave-Assisted Extraction of Total Polyphenols Content from <i>Eleutherine bulbosa</i> (Mill.) Bulb1411-94202460-157810.22146/ijc.58467https://doaj.org/article/0c1bf266337546efbab828da25a3fb222021-07-01T00:00:00Zhttps://jurnal.ugm.ac.id/ijc/article/view/58467https://doaj.org/toc/1411-9420https://doaj.org/toc/2460-1578Application of natural deep eutectic solvent (NADES) citric acid-glucose-based microwave-assisted extraction (MAE) method for total polyphenol content (TPC) enriches the use of Eleutherine bulbosa (Mill.) bulb more widely and commercially. Therefore, this study aims to optimize NADES citric acid-glucose-based MAE on the TPC from E. bulbosa bulbs using response surface methodology (RSM). In the present study, the dried sample of E. bulbosa bulb was extracted using the NADES based MAE. Determination of TPC was conducted using Folin-Ciocalteau reagent and standard gallic acid, then measured using a UV-Vis spectrophotometer at 761 nm. Extraction condition optimization of the NADES based MAE method was performed using RSM with Box Behnken Design (four-factors-three-levels and 29 runs) on Design Expert v12. Based on the results study, the optimum condition extraction on the TPC enrichment was obtained at the NADES ratio (citric acid: glucose) 1:1 g/g; solid-liquid ratio 1:8 g/mL; extraction time of 15 min; and 270 Watt microwave power. The confirmation test and scale-up (50 g samples) were obtained with a 61.63 ± 2.23 mg GA/g sample.Bohari YusufSelvi Jumiatul AstatiMirhansyah ArdanaHerman HermanArsyik IbrahimLaode RijaiFirzan NainuIslamudin AhmadDepartment of Chemistry, Universitas Gadjah Madaarticleeleutherine bulbosa millmicrowave-assisted extractionnatural deep eutectic solventresponse surface methodologytotal polyphenols contentChemistryQD1-999ENIndonesian Journal of Chemistry, Vol 21, Iss 4, Pp 797-805 (2021)
institution	DOAJ
collection	DOAJ
language	EN
topic	eleutherine bulbosa mill microwave-assisted extraction natural deep eutectic solvent response surface methodology total polyphenols content Chemistry QD1-999
spellingShingle	eleutherine bulbosa mill microwave-assisted extraction natural deep eutectic solvent response surface methodology total polyphenols content Chemistry QD1-999 Bohari Yusuf Selvi Jumiatul Astati Mirhansyah Ardana Herman Herman Arsyik Ibrahim Laode Rijai Firzan Nainu Islamudin Ahmad Optimizing Natural Deep Eutectic Solvent Citric Acid-Glucose Based Microwave-Assisted Extraction of Total Polyphenols Content from <i>Eleutherine bulbosa</i> (Mill.) Bulb
description	Application of natural deep eutectic solvent (NADES) citric acid-glucose-based microwave-assisted extraction (MAE) method for total polyphenol content (TPC) enriches the use of Eleutherine bulbosa (Mill.) bulb more widely and commercially. Therefore, this study aims to optimize NADES citric acid-glucose-based MAE on the TPC from E. bulbosa bulbs using response surface methodology (RSM). In the present study, the dried sample of E. bulbosa bulb was extracted using the NADES based MAE. Determination of TPC was conducted using Folin-Ciocalteau reagent and standard gallic acid, then measured using a UV-Vis spectrophotometer at 761 nm. Extraction condition optimization of the NADES based MAE method was performed using RSM with Box Behnken Design (four-factors-three-levels and 29 runs) on Design Expert v12. Based on the results study, the optimum condition extraction on the TPC enrichment was obtained at the NADES ratio (citric acid: glucose) 1:1 g/g; solid-liquid ratio 1:8 g/mL; extraction time of 15 min; and 270 Watt microwave power. The confirmation test and scale-up (50 g samples) were obtained with a 61.63 ± 2.23 mg GA/g sample.
format	article
author	Bohari Yusuf Selvi Jumiatul Astati Mirhansyah Ardana Herman Herman Arsyik Ibrahim Laode Rijai Firzan Nainu Islamudin Ahmad
author_facet	Bohari Yusuf Selvi Jumiatul Astati Mirhansyah Ardana Herman Herman Arsyik Ibrahim Laode Rijai Firzan Nainu Islamudin Ahmad
author_sort	Bohari Yusuf
title	Optimizing Natural Deep Eutectic Solvent Citric Acid-Glucose Based Microwave-Assisted Extraction of Total Polyphenols Content from <i>Eleutherine bulbosa</i> (Mill.) Bulb
title_short	Optimizing Natural Deep Eutectic Solvent Citric Acid-Glucose Based Microwave-Assisted Extraction of Total Polyphenols Content from <i>Eleutherine bulbosa</i> (Mill.) Bulb
title_full	Optimizing Natural Deep Eutectic Solvent Citric Acid-Glucose Based Microwave-Assisted Extraction of Total Polyphenols Content from <i>Eleutherine bulbosa</i> (Mill.) Bulb
title_fullStr	Optimizing Natural Deep Eutectic Solvent Citric Acid-Glucose Based Microwave-Assisted Extraction of Total Polyphenols Content from <i>Eleutherine bulbosa</i> (Mill.) Bulb
title_full_unstemmed	Optimizing Natural Deep Eutectic Solvent Citric Acid-Glucose Based Microwave-Assisted Extraction of Total Polyphenols Content from <i>Eleutherine bulbosa</i> (Mill.) Bulb
title_sort	optimizing natural deep eutectic solvent citric acid-glucose based microwave-assisted extraction of total polyphenols content from <i>eleutherine bulbosa</i> (mill.) bulb
publisher	Department of Chemistry, Universitas Gadjah Mada
publishDate	2021
url	https://doaj.org/article/0c1bf266337546efbab828da25a3fb22
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Optimizing Natural Deep Eutectic Solvent Citric Acid-Glucose Based Microwave-Assisted Extraction of Total Polyphenols Content from <i>Eleutherine bulbosa</i> (Mill.) Bulb

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