Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts
The properties of three types of CoMo/USY catalysts with different synthesized methods have been studied. The sequential and co-impregnation methods followed by activation using calcination and reduction process have been conducted. The properties of the catalysts were examined using Fourier-transfo...
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De Gruyter
2021
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oai:doaj.org-article:136b2ed38b864abb9463668b45e405202021-12-05T14:10:44ZEffect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts2391-542010.1515/chem-2021-0064https://doaj.org/article/136b2ed38b864abb9463668b45e405202021-06-01T00:00:00Zhttps://doi.org/10.1515/chem-2021-0064https://doaj.org/toc/2391-5420The properties of three types of CoMo/USY catalysts with different synthesized methods have been studied. The sequential and co-impregnation methods followed by activation using calcination and reduction process have been conducted. The properties of the catalysts were examined using Fourier-transform-infrared (FTIR) spectroscopy, X-ray diffraction (XRD) with refinement, and surface area analyzer (SAA). The FTIR spectrum study revealed the enhanced intensity of its Bronsted acid site, and the XRD diffractogram pattern verified the composition of pure metals, oxides, and alloys in the catalyst. The SAA demonstrated the mesoporous features of the catalyst. Scanning electron microscopy showed an irregular particle morphology. Additional analysis using the transmission electron microscopy indicated that the metal has successfully impregnated without damaging the USY structure.Nugrahaningtyas Khoirina DwiHeraldy EddyRachmadaniHidayat YuniawanKartini IndrianaDe Gruyterarticlecatalystimpregnationphysical activationacidity strengthmorphologyChemistryQD1-999ENOpen Chemistry, Vol 19, Iss 1, Pp 745-754 (2021) |
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catalyst impregnation physical activation acidity strength morphology Chemistry QD1-999 |
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catalyst impregnation physical activation acidity strength morphology Chemistry QD1-999 Nugrahaningtyas Khoirina Dwi Heraldy Eddy Rachmadani Hidayat Yuniawan Kartini Indriana Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts |
description |
The properties of three types of CoMo/USY catalysts with different synthesized methods have been studied. The sequential and co-impregnation methods followed by activation using calcination and reduction process have been conducted. The properties of the catalysts were examined using Fourier-transform-infrared (FTIR) spectroscopy, X-ray diffraction (XRD) with refinement, and surface area analyzer (SAA). The FTIR spectrum study revealed the enhanced intensity of its Bronsted acid site, and the XRD diffractogram pattern verified the composition of pure metals, oxides, and alloys in the catalyst. The SAA demonstrated the mesoporous features of the catalyst. Scanning electron microscopy showed an irregular particle morphology. Additional analysis using the transmission electron microscopy indicated that the metal has successfully impregnated without damaging the USY structure. |
format |
article |
author |
Nugrahaningtyas Khoirina Dwi Heraldy Eddy Rachmadani Hidayat Yuniawan Kartini Indriana |
author_facet |
Nugrahaningtyas Khoirina Dwi Heraldy Eddy Rachmadani Hidayat Yuniawan Kartini Indriana |
author_sort |
Nugrahaningtyas Khoirina Dwi |
title |
Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts |
title_short |
Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts |
title_full |
Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts |
title_fullStr |
Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts |
title_full_unstemmed |
Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts |
title_sort |
effect of synthesis and activation methods on the character of como/ultrastable y-zeolite catalysts |
publisher |
De Gruyter |
publishDate |
2021 |
url |
https://doaj.org/article/136b2ed38b864abb9463668b45e40520 |
work_keys_str_mv |
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_version_ |
1718371776435585024 |