Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts

The properties of three types of CoMo/USY catalysts with different synthesized methods have been studied. The sequential and co-impregnation methods followed by activation using calcination and reduction process have been conducted. The properties of the catalysts were examined using Fourier-transfo...

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Autores principales: Nugrahaningtyas Khoirina Dwi, Heraldy Eddy, Rachmadani, Hidayat Yuniawan, Kartini Indriana
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Publicado: De Gruyter 2021
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Acceso en línea:https://doaj.org/article/136b2ed38b864abb9463668b45e40520
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spelling oai:doaj.org-article:136b2ed38b864abb9463668b45e405202021-12-05T14:10:44ZEffect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts2391-542010.1515/chem-2021-0064https://doaj.org/article/136b2ed38b864abb9463668b45e405202021-06-01T00:00:00Zhttps://doi.org/10.1515/chem-2021-0064https://doaj.org/toc/2391-5420The properties of three types of CoMo/USY catalysts with different synthesized methods have been studied. The sequential and co-impregnation methods followed by activation using calcination and reduction process have been conducted. The properties of the catalysts were examined using Fourier-transform-infrared (FTIR) spectroscopy, X-ray diffraction (XRD) with refinement, and surface area analyzer (SAA). The FTIR spectrum study revealed the enhanced intensity of its Bronsted acid site, and the XRD diffractogram pattern verified the composition of pure metals, oxides, and alloys in the catalyst. The SAA demonstrated the mesoporous features of the catalyst. Scanning electron microscopy showed an irregular particle morphology. Additional analysis using the transmission electron microscopy indicated that the metal has successfully impregnated without damaging the USY structure.Nugrahaningtyas Khoirina DwiHeraldy EddyRachmadaniHidayat YuniawanKartini IndrianaDe Gruyterarticlecatalystimpregnationphysical activationacidity strengthmorphologyChemistryQD1-999ENOpen Chemistry, Vol 19, Iss 1, Pp 745-754 (2021)
institution DOAJ
collection DOAJ
language EN
topic catalyst
impregnation
physical activation
acidity strength
morphology
Chemistry
QD1-999
spellingShingle catalyst
impregnation
physical activation
acidity strength
morphology
Chemistry
QD1-999
Nugrahaningtyas Khoirina Dwi
Heraldy Eddy
Rachmadani
Hidayat Yuniawan
Kartini Indriana
Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts
description The properties of three types of CoMo/USY catalysts with different synthesized methods have been studied. The sequential and co-impregnation methods followed by activation using calcination and reduction process have been conducted. The properties of the catalysts were examined using Fourier-transform-infrared (FTIR) spectroscopy, X-ray diffraction (XRD) with refinement, and surface area analyzer (SAA). The FTIR spectrum study revealed the enhanced intensity of its Bronsted acid site, and the XRD diffractogram pattern verified the composition of pure metals, oxides, and alloys in the catalyst. The SAA demonstrated the mesoporous features of the catalyst. Scanning electron microscopy showed an irregular particle morphology. Additional analysis using the transmission electron microscopy indicated that the metal has successfully impregnated without damaging the USY structure.
format article
author Nugrahaningtyas Khoirina Dwi
Heraldy Eddy
Rachmadani
Hidayat Yuniawan
Kartini Indriana
author_facet Nugrahaningtyas Khoirina Dwi
Heraldy Eddy
Rachmadani
Hidayat Yuniawan
Kartini Indriana
author_sort Nugrahaningtyas Khoirina Dwi
title Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts
title_short Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts
title_full Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts
title_fullStr Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts
title_full_unstemmed Effect of synthesis and activation methods on the character of CoMo/ultrastable Y-zeolite catalysts
title_sort effect of synthesis and activation methods on the character of como/ultrastable y-zeolite catalysts
publisher De Gruyter
publishDate 2021
url https://doaj.org/article/136b2ed38b864abb9463668b45e40520
work_keys_str_mv AT nugrahaningtyaskhoirinadwi effectofsynthesisandactivationmethodsonthecharacterofcomoultrastableyzeolitecatalysts
AT heraldyeddy effectofsynthesisandactivationmethodsonthecharacterofcomoultrastableyzeolitecatalysts
AT rachmadani effectofsynthesisandactivationmethodsonthecharacterofcomoultrastableyzeolitecatalysts
AT hidayatyuniawan effectofsynthesisandactivationmethodsonthecharacterofcomoultrastableyzeolitecatalysts
AT kartiniindriana effectofsynthesisandactivationmethodsonthecharacterofcomoultrastableyzeolitecatalysts
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