Simultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography

Abstract So far, the identification and determination of flavor additives in food has gained extensive attention in the area of food safety. However, it remains a big challenge for simultaneous detection of diverse flavor agents. In this work, a novel gas chromatography method coupled with ultrasoun...

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Autores principales:	Junde Li, Xiaojuan Liu, Xin Liang, Manman Zhang, Lei Han, Jiying Song
Formato:	article
Lenguaje:	EN
Publicado:	Nature Portfolio 2019
Materias:	Medicine R Science Q
Acceso en línea:	https://doaj.org/article/152f3776c35d414a9c53320013d91608
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spelling	oai:doaj.org-article:152f3776c35d414a9c53320013d916082021-12-02T15:09:24ZSimultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography10.1038/s41598-019-48522-52045-2322https://doaj.org/article/152f3776c35d414a9c53320013d916082019-08-01T00:00:00Zhttps://doi.org/10.1038/s41598-019-48522-5https://doaj.org/toc/2045-2322Abstract So far, the identification and determination of flavor additives in food has gained extensive attention in the area of food safety. However, it remains a big challenge for simultaneous detection of diverse flavor agents. In this work, a novel gas chromatography method coupled with ultrasound-microwave synergistic extraction was developed for simultaneous detection of five flavor compounds, including butyl butyrate, menthol, methyl salicylate, eugenol and vanilline. In this strategy, ultrasound-microwave synergistic extraction was used to extract the five flavoring agents from chewing gum. The effects of extractants, solid-liquid ratio, extraction time and microwave power on extraction yield were researched by using orthogonal test. After the optimization of programme temperature and splitless injection, the five flavoring agents were well separated and simultaneously detected with wide linear ranges, low limits of detection, high accuracy and good repeatability. Therefore, this proposed method would hold great promise for assay application on the food safety.Junde LiXiaojuan LiuXin LiangManman ZhangLei HanJiying SongNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 9, Iss 1, Pp 1-7 (2019)
institution	DOAJ
collection	DOAJ
language	EN
topic	Medicine R Science Q
spellingShingle	Medicine R Science Q Junde Li Xiaojuan Liu Xin Liang Manman Zhang Lei Han Jiying Song Simultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography
description	Abstract So far, the identification and determination of flavor additives in food has gained extensive attention in the area of food safety. However, it remains a big challenge for simultaneous detection of diverse flavor agents. In this work, a novel gas chromatography method coupled with ultrasound-microwave synergistic extraction was developed for simultaneous detection of five flavor compounds, including butyl butyrate, menthol, methyl salicylate, eugenol and vanilline. In this strategy, ultrasound-microwave synergistic extraction was used to extract the five flavoring agents from chewing gum. The effects of extractants, solid-liquid ratio, extraction time and microwave power on extraction yield were researched by using orthogonal test. After the optimization of programme temperature and splitless injection, the five flavoring agents were well separated and simultaneously detected with wide linear ranges, low limits of detection, high accuracy and good repeatability. Therefore, this proposed method would hold great promise for assay application on the food safety.
format	article
author	Junde Li Xiaojuan Liu Xin Liang Manman Zhang Lei Han Jiying Song
author_facet	Junde Li Xiaojuan Liu Xin Liang Manman Zhang Lei Han Jiying Song
author_sort	Junde Li
title	Simultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography
title_short	Simultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography
title_full	Simultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography
title_fullStr	Simultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography
title_full_unstemmed	Simultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography
title_sort	simultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography
publisher	Nature Portfolio
publishDate	2019
url	https://doaj.org/article/152f3776c35d414a9c53320013d91608
work_keys_str_mv	AT jundeli simultaneousdetectionoffiveflavoringagentsinchewinggumbyultrasoundmicrowavesynergisticextractioncoupledwithgaschromatography AT xiaojuanliu simultaneousdetectionoffiveflavoringagentsinchewinggumbyultrasoundmicrowavesynergisticextractioncoupledwithgaschromatography AT xinliang simultaneousdetectionoffiveflavoringagentsinchewinggumbyultrasoundmicrowavesynergisticextractioncoupledwithgaschromatography AT manmanzhang simultaneousdetectionoffiveflavoringagentsinchewinggumbyultrasoundmicrowavesynergisticextractioncoupledwithgaschromatography AT leihan simultaneousdetectionoffiveflavoringagentsinchewinggumbyultrasoundmicrowavesynergisticextractioncoupledwithgaschromatography AT jiyingsong simultaneousdetectionoffiveflavoringagentsinchewinggumbyultrasoundmicrowavesynergisticextractioncoupledwithgaschromatography
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Simultaneous detection of five flavoring agents in chewing gum by ultrasound-microwave synergistic extraction coupled with gas chromatography

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