Π-GISANS: probing lateral structures with a fan shaped beam
Abstract We have performed grazing incidence neutron small angle scattering using a fan shaped incident beam focused along one dimension. This allows significantly reduced counting times for measurements of lateral correlations parallel to an interface or in a thin film where limited depth resolutio...
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Nature Portfolio
2021
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oai:doaj.org-article:1a604e3b238f4107b298de8442fa92f02021-12-02T14:58:46ZΠ-GISANS: probing lateral structures with a fan shaped beam10.1038/s41598-021-97112-x2045-2322https://doaj.org/article/1a604e3b238f4107b298de8442fa92f02021-09-01T00:00:00Zhttps://doi.org/10.1038/s41598-021-97112-xhttps://doaj.org/toc/2045-2322Abstract We have performed grazing incidence neutron small angle scattering using a fan shaped incident beam focused along one dimension. This allows significantly reduced counting times for measurements of lateral correlations parallel to an interface or in a thin film where limited depth resolution is required. We resolve the structure factor of iron inclusions in aluminium oxide and show that the ordering of silica particles deposited on a silicon substrate depends on their size. We report hexagonal packing for 50 nm but not for 200 nm silica spheres deposited by a modified Langmuir-Schaefer method on a silicon substrate. For the 200 nm particles we extract the particles shape from the form factor. Moreover, we report dense packing of the particles spread on a free water surface. We name this method π-GISANS to highlight that it differs from GISANS as it gives lateral information while averaging the in-depth structure.Alexei VorobievNicolò ParaciniMarité CárdenasMax WolffNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 11, Iss 1, Pp 1-8 (2021) |
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Medicine R Science Q Alexei Vorobiev Nicolò Paracini Marité Cárdenas Max Wolff Π-GISANS: probing lateral structures with a fan shaped beam |
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Abstract We have performed grazing incidence neutron small angle scattering using a fan shaped incident beam focused along one dimension. This allows significantly reduced counting times for measurements of lateral correlations parallel to an interface or in a thin film where limited depth resolution is required. We resolve the structure factor of iron inclusions in aluminium oxide and show that the ordering of silica particles deposited on a silicon substrate depends on their size. We report hexagonal packing for 50 nm but not for 200 nm silica spheres deposited by a modified Langmuir-Schaefer method on a silicon substrate. For the 200 nm particles we extract the particles shape from the form factor. Moreover, we report dense packing of the particles spread on a free water surface. We name this method π-GISANS to highlight that it differs from GISANS as it gives lateral information while averaging the in-depth structure. |
format |
article |
author |
Alexei Vorobiev Nicolò Paracini Marité Cárdenas Max Wolff |
author_facet |
Alexei Vorobiev Nicolò Paracini Marité Cárdenas Max Wolff |
author_sort |
Alexei Vorobiev |
title |
Π-GISANS: probing lateral structures with a fan shaped beam |
title_short |
Π-GISANS: probing lateral structures with a fan shaped beam |
title_full |
Π-GISANS: probing lateral structures with a fan shaped beam |
title_fullStr |
Π-GISANS: probing lateral structures with a fan shaped beam |
title_full_unstemmed |
Π-GISANS: probing lateral structures with a fan shaped beam |
title_sort |
π-gisans: probing lateral structures with a fan shaped beam |
publisher |
Nature Portfolio |
publishDate |
2021 |
url |
https://doaj.org/article/1a604e3b238f4107b298de8442fa92f0 |
work_keys_str_mv |
AT alexeivorobiev pgisansprobinglateralstructureswithafanshapedbeam AT nicoloparacini pgisansprobinglateralstructureswithafanshapedbeam AT maritecardenas pgisansprobinglateralstructureswithafanshapedbeam AT maxwolff pgisansprobinglateralstructureswithafanshapedbeam |
_version_ |
1718389249273757696 |