Investigation on the interfacial properties of CNTs sized carbon fibres in epoxy resin using push-out method via nano-indentation technique

In this work, the carbon fibres (CFs) surfaces were modified via sizing and coated with a very thin layer of a complex formulation including carbon nanotubes (CNTs). A push-out method was developed based on nanoindentation to assess the interfacial shear strength of the fibre/matrix. The mechanical...

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Autores principales: Zhang Zhenxue, Li Xiaoying, Dong Hanshan, Jestin Simon, Termine Stefania, Trompeta Aikaterini-Flora, Araújo Andreia, Santos Raquel M., Charitidis Costas
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Publicado: EDP Sciences 2021
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Acceso en línea:https://doaj.org/article/1b68987896e848c2818cd7c86d956119
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spelling oai:doaj.org-article:1b68987896e848c2818cd7c86d9561192021-12-02T17:13:46ZInvestigation on the interfacial properties of CNTs sized carbon fibres in epoxy resin using push-out method via nano-indentation technique2261-236X10.1051/matecconf/202134901007https://doaj.org/article/1b68987896e848c2818cd7c86d9561192021-01-01T00:00:00Zhttps://www.matec-conferences.org/articles/matecconf/pdf/2021/18/matecconf_iceaf2021_01007.pdfhttps://doaj.org/toc/2261-236XIn this work, the carbon fibres (CFs) surfaces were modified via sizing and coated with a very thin layer of a complex formulation including carbon nanotubes (CNTs). A push-out method was developed based on nanoindentation to assess the interfacial shear strength of the fibre/matrix. The mechanical properties such as indentation hardness, reduced modulus, indentation displacement and indentation creep of the composite were evaluated by means of the Oliver-Pharr method. The critical load of different composites was measured and the interfacial shear strength (IFSS) was calculated to compare the effect of the CNTs concentration in the sizing solution. Wettability evaluation of the sized fibres was performed prior to nanoindentation to investigate the adhesion of the resin. After push-out testing, characterisation by optical microscopy/SEM was carried out to ratify the results. It was found sizing with a small amount of evenly distributed nano-inclusion on CFs can increase the interfacial shear strength but large amount of sizing could lead to a decrease of the interfacial bonding due to the agglomeration of CNTs on CFs.Zhang ZhenxueLi XiaoyingDong HanshanJestin SimonTermine StefaniaTrompeta Aikaterini-FloraAraújo AndreiaSantos Raquel M.Charitidis CostasEDP Sciencesarticlepush-outcntcarbon fibre reinforced compositenano-indentationwettabilityEngineering (General). Civil engineering (General)TA1-2040ENFRMATEC Web of Conferences, Vol 349, p 01007 (2021)
institution DOAJ
collection DOAJ
language EN
FR
topic push-out
cnt
carbon fibre reinforced composite
nano-indentation
wettability
Engineering (General). Civil engineering (General)
TA1-2040
spellingShingle push-out
cnt
carbon fibre reinforced composite
nano-indentation
wettability
Engineering (General). Civil engineering (General)
TA1-2040
Zhang Zhenxue
Li Xiaoying
Dong Hanshan
Jestin Simon
Termine Stefania
Trompeta Aikaterini-Flora
Araújo Andreia
Santos Raquel M.
Charitidis Costas
Investigation on the interfacial properties of CNTs sized carbon fibres in epoxy resin using push-out method via nano-indentation technique
description In this work, the carbon fibres (CFs) surfaces were modified via sizing and coated with a very thin layer of a complex formulation including carbon nanotubes (CNTs). A push-out method was developed based on nanoindentation to assess the interfacial shear strength of the fibre/matrix. The mechanical properties such as indentation hardness, reduced modulus, indentation displacement and indentation creep of the composite were evaluated by means of the Oliver-Pharr method. The critical load of different composites was measured and the interfacial shear strength (IFSS) was calculated to compare the effect of the CNTs concentration in the sizing solution. Wettability evaluation of the sized fibres was performed prior to nanoindentation to investigate the adhesion of the resin. After push-out testing, characterisation by optical microscopy/SEM was carried out to ratify the results. It was found sizing with a small amount of evenly distributed nano-inclusion on CFs can increase the interfacial shear strength but large amount of sizing could lead to a decrease of the interfacial bonding due to the agglomeration of CNTs on CFs.
format article
author Zhang Zhenxue
Li Xiaoying
Dong Hanshan
Jestin Simon
Termine Stefania
Trompeta Aikaterini-Flora
Araújo Andreia
Santos Raquel M.
Charitidis Costas
author_facet Zhang Zhenxue
Li Xiaoying
Dong Hanshan
Jestin Simon
Termine Stefania
Trompeta Aikaterini-Flora
Araújo Andreia
Santos Raquel M.
Charitidis Costas
author_sort Zhang Zhenxue
title Investigation on the interfacial properties of CNTs sized carbon fibres in epoxy resin using push-out method via nano-indentation technique
title_short Investigation on the interfacial properties of CNTs sized carbon fibres in epoxy resin using push-out method via nano-indentation technique
title_full Investigation on the interfacial properties of CNTs sized carbon fibres in epoxy resin using push-out method via nano-indentation technique
title_fullStr Investigation on the interfacial properties of CNTs sized carbon fibres in epoxy resin using push-out method via nano-indentation technique
title_full_unstemmed Investigation on the interfacial properties of CNTs sized carbon fibres in epoxy resin using push-out method via nano-indentation technique
title_sort investigation on the interfacial properties of cnts sized carbon fibres in epoxy resin using push-out method via nano-indentation technique
publisher EDP Sciences
publishDate 2021
url https://doaj.org/article/1b68987896e848c2818cd7c86d956119
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