Influence of Calcination Temperature on Size, Morphology and Optical Properties of ZNO/C Composite Synthesized by a Colloidal Method

ZnO is one of the most studied semiconductor materials because of its interesting chemicals, and from a technological point of view, mainly as a consequence of their outstanding properties, such as wurtzite type, non-toxic nature, large band gap, low cost, and environment-friendly. In this work, the...

Descripción completa

Guardado en:

Detalles Bibliográficos
Autores principales:	Siham Lhimr, Saidati Bouhlassa, Bouchaib Ammary
Formato:	article
Lenguaje:	EN
Publicado:	Department of Chemistry, Universitas Gadjah Mada 2021
Materias:	zno/c composite calcination temperature colloidal method morphology optical properties Chemistry QD1-999
Acceso en línea:	https://doaj.org/article/1c64127387104e539a83488cf6e4c796
Etiquetas:	Agregar Etiqueta Sin Etiquetas, Sea el primero en etiquetar este registro!

id	oai:doaj.org-article:1c64127387104e539a83488cf6e4c796
record_format	dspace
spelling	oai:doaj.org-article:1c64127387104e539a83488cf6e4c7962021-12-02T15:56:44ZInfluence of Calcination Temperature on Size, Morphology and Optical Properties of ZNO/C Composite Synthesized by a Colloidal Method1411-94202460-157810.22146/ijc.56309https://doaj.org/article/1c64127387104e539a83488cf6e4c7962021-04-01T00:00:00Zhttps://jurnal.ugm.ac.id/ijc/article/view/56309https://doaj.org/toc/1411-9420https://doaj.org/toc/2460-1578ZnO is one of the most studied semiconductor materials because of its interesting chemicals, and from a technological point of view, mainly as a consequence of their outstanding properties, such as wurtzite type, non-toxic nature, large band gap, low cost, and environment-friendly. In this work, the ZnO/C composite was synthesized by a simple and fast low-temperature method; the solid product was calcination temperature at 100 to 400 °C. The influence of variation in calcination temperature was studied using X-ray diffraction (XRD), Fourier transforms infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and UV-visible diffuse reflectance spectroscopy. The X-ray diffraction patterns indicated a high crystallinity and a nanocrystalline size of the ZnO/C composite hexagonal structure of wurtzite. The SEM image of the samples showed that the powder has a spherical structure of flakes aggregated in the common nucleus like a grid. The sphere consists of spindle and flower-like structures. The optical properties were determined by UV-vis diffuse reflectance spectroscopy, and it was found that the band gap energy of ZnO/C composite increase from 3.210 to 3.329 eV with an increase in calcination temperature from 100 to 400 °C. FTIR spectra and EDS analysis showed that the existence of carbon in the composite.Siham LhimrSaidati BouhlassaBouchaib AmmaryDepartment of Chemistry, Universitas Gadjah Madaarticlezno/c compositecalcination temperaturecolloidal methodmorphologyoptical propertiesChemistryQD1-999ENIndonesian Journal of Chemistry, Vol 21, Iss 3, Pp 537-545 (2021)
institution	DOAJ
collection	DOAJ
language	EN
topic	zno/c composite calcination temperature colloidal method morphology optical properties Chemistry QD1-999
spellingShingle	zno/c composite calcination temperature colloidal method morphology optical properties Chemistry QD1-999 Siham Lhimr Saidati Bouhlassa Bouchaib Ammary Influence of Calcination Temperature on Size, Morphology and Optical Properties of ZNO/C Composite Synthesized by a Colloidal Method
description	ZnO is one of the most studied semiconductor materials because of its interesting chemicals, and from a technological point of view, mainly as a consequence of their outstanding properties, such as wurtzite type, non-toxic nature, large band gap, low cost, and environment-friendly. In this work, the ZnO/C composite was synthesized by a simple and fast low-temperature method; the solid product was calcination temperature at 100 to 400 °C. The influence of variation in calcination temperature was studied using X-ray diffraction (XRD), Fourier transforms infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and UV-visible diffuse reflectance spectroscopy. The X-ray diffraction patterns indicated a high crystallinity and a nanocrystalline size of the ZnO/C composite hexagonal structure of wurtzite. The SEM image of the samples showed that the powder has a spherical structure of flakes aggregated in the common nucleus like a grid. The sphere consists of spindle and flower-like structures. The optical properties were determined by UV-vis diffuse reflectance spectroscopy, and it was found that the band gap energy of ZnO/C composite increase from 3.210 to 3.329 eV with an increase in calcination temperature from 100 to 400 °C. FTIR spectra and EDS analysis showed that the existence of carbon in the composite.
format	article
author	Siham Lhimr Saidati Bouhlassa Bouchaib Ammary
author_facet	Siham Lhimr Saidati Bouhlassa Bouchaib Ammary
author_sort	Siham Lhimr
title	Influence of Calcination Temperature on Size, Morphology and Optical Properties of ZNO/C Composite Synthesized by a Colloidal Method
title_short	Influence of Calcination Temperature on Size, Morphology and Optical Properties of ZNO/C Composite Synthesized by a Colloidal Method
title_full	Influence of Calcination Temperature on Size, Morphology and Optical Properties of ZNO/C Composite Synthesized by a Colloidal Method
title_fullStr	Influence of Calcination Temperature on Size, Morphology and Optical Properties of ZNO/C Composite Synthesized by a Colloidal Method
title_full_unstemmed	Influence of Calcination Temperature on Size, Morphology and Optical Properties of ZNO/C Composite Synthesized by a Colloidal Method
title_sort	influence of calcination temperature on size, morphology and optical properties of zno/c composite synthesized by a colloidal method
publisher	Department of Chemistry, Universitas Gadjah Mada
publishDate	2021
url	https://doaj.org/article/1c64127387104e539a83488cf6e4c796
work_keys_str_mv	AT sihamlhimr influenceofcalcinationtemperatureonsizemorphologyandopticalpropertiesofznoccompositesynthesizedbyacolloidalmethod AT saidatibouhlassa influenceofcalcinationtemperatureonsizemorphologyandopticalpropertiesofznoccompositesynthesizedbyacolloidalmethod AT bouchaibammary influenceofcalcinationtemperatureonsizemorphologyandopticalpropertiesofznoccompositesynthesizedbyacolloidalmethod
_version_	1718385376169558016

Influence of Calcination Temperature on Size, Morphology and Optical Properties of ZNO/C Composite Synthesized by a Colloidal Method

Ejemplares similares