Preparation of Ruthenium chloride-grafted Zeolite from a Clay Mineral Ore and Studying Their Catalytic Properties
This research work include studying one of the natural mineral ores available in Al-Hawy area (Mosul city – Northern Iraq) by chemical analysis and X-ray fluorescence (XRF) to identify its components of the elements as oxides, X-ray diffraction was carried out to determine the percentages of clay m...
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College of Education for Pure Sciences
2021
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oai:doaj.org-article:2343985e08424bf18d74134cc9edd3bf2021-12-01T14:54:26ZPreparation of Ruthenium chloride-grafted Zeolite from a Clay Mineral Ore and Studying Their Catalytic Properties1812-125X2664-253010.33899/edusj.2021.130894.1178https://doaj.org/article/2343985e08424bf18d74134cc9edd3bf2021-12-01T00:00:00Zhttps://edusj.mosuljournals.com/article_169070_64809bd8c1ef56ac770c2dd6db1d6c90.pdfhttps://doaj.org/toc/1812-125Xhttps://doaj.org/toc/2664-2530This research work include studying one of the natural mineral ores available in Al-Hawy area (Mosul city – Northern Iraq) by chemical analysis and X-ray fluorescence (XRF) to identify its components of the elements as oxides, X-ray diffraction was carried out to determine the percentages of clay minerals (natural zeolites) and non-clay minerals in the natural ore. The natural zeolites were concentrated by removing carbonate, iron and separating the convertible silica into sodium silicate, the prepared zeolite was converted into (H-form) by treated with ammonium nitrite solution (1M) ,then grafted with ruthenium chloride (RuCl<sub>3</sub>.6H<sub>2</sub>O) .The properties and specifications of the prepared zeolite (grafted and non-grafted) were studied using techniques of (XRF) ,(XRD),(BET) , (SEM) and (differential& thermo gravimetric analysis(DTA)&(TGA) ) ,it was found that have a chemical and crystalline composition within the specifications of zeolites, as well as a good surface area , thermal stability and selective porous channels<strong>.</strong>Ragheed GhazalDhyaa FathyCollege of Education for Pure Sciencesarticlenatural zeolite,,,،,؛montmorillonite,,,،,؛kaolinite,,,،,؛sem,,,،,؛xrdEducationLScience (General)Q1-390ARENمجلة التربية والعلم, Vol 30, Iss 5, Pp 103-113 (2021) |
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natural zeolite,, ,،,؛montmorillonite,, ,،,؛kaolinite,, ,،,؛sem,, ,،,؛xrd Education L Science (General) Q1-390 |
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natural zeolite,, ,،,؛montmorillonite,, ,،,؛kaolinite,, ,،,؛sem,, ,،,؛xrd Education L Science (General) Q1-390 Ragheed Ghazal Dhyaa Fathy Preparation of Ruthenium chloride-grafted Zeolite from a Clay Mineral Ore and Studying Their Catalytic Properties |
description |
This research work include studying one of the natural mineral ores available in Al-Hawy area (Mosul city – Northern Iraq) by chemical analysis and X-ray fluorescence (XRF) to identify its components of the elements as oxides, X-ray diffraction was carried out to determine the percentages of clay minerals (natural zeolites) and non-clay minerals in the natural ore. The natural zeolites were concentrated by removing carbonate, iron and separating the convertible silica into sodium silicate, the prepared zeolite was converted into (H-form) by treated with ammonium nitrite solution (1M) ,then grafted with ruthenium chloride (RuCl<sub>3</sub>.6H<sub>2</sub>O) .The properties and specifications of the prepared zeolite (grafted and non-grafted) were studied using techniques of (XRF) ,(XRD),(BET) , (SEM) and (differential& thermo gravimetric analysis(DTA)&(TGA) ) ,it was found that have a chemical and crystalline composition within the specifications of zeolites, as well as a good surface area , thermal stability and selective porous channels<strong>.</strong> |
format |
article |
author |
Ragheed Ghazal Dhyaa Fathy |
author_facet |
Ragheed Ghazal Dhyaa Fathy |
author_sort |
Ragheed Ghazal |
title |
Preparation of Ruthenium chloride-grafted Zeolite from a Clay Mineral Ore and Studying Their Catalytic Properties |
title_short |
Preparation of Ruthenium chloride-grafted Zeolite from a Clay Mineral Ore and Studying Their Catalytic Properties |
title_full |
Preparation of Ruthenium chloride-grafted Zeolite from a Clay Mineral Ore and Studying Their Catalytic Properties |
title_fullStr |
Preparation of Ruthenium chloride-grafted Zeolite from a Clay Mineral Ore and Studying Their Catalytic Properties |
title_full_unstemmed |
Preparation of Ruthenium chloride-grafted Zeolite from a Clay Mineral Ore and Studying Their Catalytic Properties |
title_sort |
preparation of ruthenium chloride-grafted zeolite from a clay mineral ore and studying their catalytic properties |
publisher |
College of Education for Pure Sciences |
publishDate |
2021 |
url |
https://doaj.org/article/2343985e08424bf18d74134cc9edd3bf |
work_keys_str_mv |
AT ragheedghazal preparationofrutheniumchloridegraftedzeolitefromaclaymineraloreandstudyingtheircatalyticproperties AT dhyaafathy preparationofrutheniumchloridegraftedzeolitefromaclaymineraloreandstudyingtheircatalyticproperties |
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1718404859203420160 |