Synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing

A series of azo dyes incorporated acridine chromophore labelled as 8 (a-d), 10 (a, b), 12 and 14 were prepared in very good yields starting from 9-chloroacridine 1 followed by amination, diazotization and coupling either with rhodanine analogues 6 (a, b) or other coupling partners 9 (a, b),...

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Autores principales: Khalid Hassan, El-khabiry Shaban, Ghada M. ElHaddad, Asmaa B. Sallam, Ibrahim El Sayed
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Publicado: Growing Science 2022
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Acceso en línea:https://doaj.org/article/25a7d9039f384caaa3cd42ae65e1e78a
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spelling oai:doaj.org-article:25a7d9039f384caaa3cd42ae65e1e78a2021-11-12T12:52:42ZSynthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing1927-72961927-730X10.5267/j.ccl.2021.9.002https://doaj.org/article/25a7d9039f384caaa3cd42ae65e1e78a2022-01-01T00:00:00Zhttp://www.growingscience.com/ccl/Vol11/ccl_2021_33.pdfhttps://doaj.org/toc/1927-7296https://doaj.org/toc/1927-730X A series of azo dyes incorporated acridine chromophore labelled as 8 (a-d), 10 (a, b), 12 and 14 were prepared in very good yields starting from 9-chloroacridine 1 followed by amination, diazotization and coupling either with rhodanine analogues 6 (a, b) or other coupling partners 9 (a, b), 11 and 13. FT-IR, 1H NMR, and mass spectroscopic analysis were used to establish the structures of the produced azo dispersed dyes. Moreover, the synthesized azo dyes were used to prepare pastes that were used to print polyester fabric using classic silk-screen printing techniques. The dyes were tested for color strength and fastness properties, and they showed good fastness resistance to washing, rubbing, and perspiration, as well as fastness to sublimation and light. The dyes were further screened for their in vitro antibacterial activity against both Gram (+) and Gram (-) bacterial species. Most of them showed promising activities against these tested organisms.Khalid HassanEl-khabiry ShabanGhada M. ElHaddadAsmaa B. SallamIbrahim El SayedGrowing SciencearticleChemistryQD1-999ENCurrent Chemistry Letters, Vol 11, Iss 1, Pp 83-94 (2022)
institution DOAJ
collection DOAJ
language EN
topic Chemistry
QD1-999
spellingShingle Chemistry
QD1-999
Khalid Hassan
El-khabiry Shaban
Ghada M. ElHaddad
Asmaa B. Sallam
Ibrahim El Sayed
Synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing
description A series of azo dyes incorporated acridine chromophore labelled as 8 (a-d), 10 (a, b), 12 and 14 were prepared in very good yields starting from 9-chloroacridine 1 followed by amination, diazotization and coupling either with rhodanine analogues 6 (a, b) or other coupling partners 9 (a, b), 11 and 13. FT-IR, 1H NMR, and mass spectroscopic analysis were used to establish the structures of the produced azo dispersed dyes. Moreover, the synthesized azo dyes were used to prepare pastes that were used to print polyester fabric using classic silk-screen printing techniques. The dyes were tested for color strength and fastness properties, and they showed good fastness resistance to washing, rubbing, and perspiration, as well as fastness to sublimation and light. The dyes were further screened for their in vitro antibacterial activity against both Gram (+) and Gram (-) bacterial species. Most of them showed promising activities against these tested organisms.
format article
author Khalid Hassan
El-khabiry Shaban
Ghada M. ElHaddad
Asmaa B. Sallam
Ibrahim El Sayed
author_facet Khalid Hassan
El-khabiry Shaban
Ghada M. ElHaddad
Asmaa B. Sallam
Ibrahim El Sayed
author_sort Khalid Hassan
title Synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing
title_short Synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing
title_full Synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing
title_fullStr Synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing
title_full_unstemmed Synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing
title_sort synthesis, characterization, and antibacterial activity of azodyes incorporated acridine chromophore and their applications in polyester printing
publisher Growing Science
publishDate 2022
url https://doaj.org/article/25a7d9039f384caaa3cd42ae65e1e78a
work_keys_str_mv AT khalidhassan synthesischaracterizationandantibacterialactivityofazodyesincorporatedacridinechromophoreandtheirapplicationsinpolyesterprinting
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