Mechanical Characterization of Nanocrystalline Materials via a Finite Element Nanoindentation Model

The difficulty of producing sufficient quantities of nanocrystalline materials for test specimens has led to an effort to explore alternative means for the mechanical characterization of small material volumes. In the present work, a numerical model simulating a nanoindentation test was developed us...

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Autores principales: Konstantinos Tserpes, Panagiotis Bazios, Spiros G. Pantelakis, Maria Pappa, Nikolaos Michailidis
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Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:272c3902dea24e678df584bfb239985e2021-11-25T18:22:14ZMechanical Characterization of Nanocrystalline Materials via a Finite Element Nanoindentation Model10.3390/met111118272075-4701https://doaj.org/article/272c3902dea24e678df584bfb239985e2021-11-01T00:00:00Zhttps://www.mdpi.com/2075-4701/11/11/1827https://doaj.org/toc/2075-4701The difficulty of producing sufficient quantities of nanocrystalline materials for test specimens has led to an effort to explore alternative means for the mechanical characterization of small material volumes. In the present work, a numerical model simulating a nanoindentation test was developed using Abaqus software. In order to implement the model, the principal material properties were used. The numerical nanoindentation results were converted to stress–strain curves through an inverse algorithm in order to obtain the macroscopic mechanical properties. For the validation of the developed model, nanoindentation tests were carried out in accordance with the ISO 14577. The composition of 75% wt. tungsten and 25% wt. copper was investigated by producing two batches of specimens with a coarse-grain microstructure with an average grain size of 150 nm and a nanocrystalline microstructure with a grain diameter of 100 nm, respectively. The porosity of both batches was derived to range between 9% and 10% based on X-ray diffraction analyses. The experimental nanoidentation results in terms of load–displacement curves show a good agreement with the numerical nanoindentation results. The proposed numerical technique combined with the inverse algorithm predicts the material properties of a fully dense, nanocrystalline material with very good accuracy, but it shows an appreciable deviation with the corresponding compression results, leading to the finding that the porosity effect is a crucial parameter which needs to be taken into account in the multiscale numerical methodology.Konstantinos TserpesPanagiotis BaziosSpiros G. PantelakisMaria PappaNikolaos MichailidisMDPI AGarticlenanocrystalline materialsfinite element analysisinverse algorithmMining engineering. MetallurgyTN1-997ENMetals, Vol 11, Iss 1827, p 1827 (2021)
institution DOAJ
collection DOAJ
language EN
topic nanocrystalline materials
finite element analysis
inverse algorithm
Mining engineering. Metallurgy
TN1-997
spellingShingle nanocrystalline materials
finite element analysis
inverse algorithm
Mining engineering. Metallurgy
TN1-997
Konstantinos Tserpes
Panagiotis Bazios
Spiros G. Pantelakis
Maria Pappa
Nikolaos Michailidis
Mechanical Characterization of Nanocrystalline Materials via a Finite Element Nanoindentation Model
description The difficulty of producing sufficient quantities of nanocrystalline materials for test specimens has led to an effort to explore alternative means for the mechanical characterization of small material volumes. In the present work, a numerical model simulating a nanoindentation test was developed using Abaqus software. In order to implement the model, the principal material properties were used. The numerical nanoindentation results were converted to stress–strain curves through an inverse algorithm in order to obtain the macroscopic mechanical properties. For the validation of the developed model, nanoindentation tests were carried out in accordance with the ISO 14577. The composition of 75% wt. tungsten and 25% wt. copper was investigated by producing two batches of specimens with a coarse-grain microstructure with an average grain size of 150 nm and a nanocrystalline microstructure with a grain diameter of 100 nm, respectively. The porosity of both batches was derived to range between 9% and 10% based on X-ray diffraction analyses. The experimental nanoidentation results in terms of load–displacement curves show a good agreement with the numerical nanoindentation results. The proposed numerical technique combined with the inverse algorithm predicts the material properties of a fully dense, nanocrystalline material with very good accuracy, but it shows an appreciable deviation with the corresponding compression results, leading to the finding that the porosity effect is a crucial parameter which needs to be taken into account in the multiscale numerical methodology.
format article
author Konstantinos Tserpes
Panagiotis Bazios
Spiros G. Pantelakis
Maria Pappa
Nikolaos Michailidis
author_facet Konstantinos Tserpes
Panagiotis Bazios
Spiros G. Pantelakis
Maria Pappa
Nikolaos Michailidis
author_sort Konstantinos Tserpes
title Mechanical Characterization of Nanocrystalline Materials via a Finite Element Nanoindentation Model
title_short Mechanical Characterization of Nanocrystalline Materials via a Finite Element Nanoindentation Model
title_full Mechanical Characterization of Nanocrystalline Materials via a Finite Element Nanoindentation Model
title_fullStr Mechanical Characterization of Nanocrystalline Materials via a Finite Element Nanoindentation Model
title_full_unstemmed Mechanical Characterization of Nanocrystalline Materials via a Finite Element Nanoindentation Model
title_sort mechanical characterization of nanocrystalline materials via a finite element nanoindentation model
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/272c3902dea24e678df584bfb239985e
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