Room-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression

Abstract The plastic deformation behavior of single crystals of two transition-metal diborides, ZrB2 and TiB2 with the AlB2 structure has been investigated at room temperature as a function of crystal orientation and specimen size by micropillar compression tests. Although plastic flow is not observ...

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Autores principales: Zhenghao Chen, Bhaskar Paul, Sanjib Majumdar, Norihiko L. Okamoto, Kyosuke Kishida, Haruyuki Inui, Shigeki Otani
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Publicado: Nature Portfolio 2021
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spelling oai:doaj.org-article:2be8b17fafcd47afb77de93a2b1888752021-12-02T18:30:45ZRoom-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression10.1038/s41598-021-93693-92045-2322https://doaj.org/article/2be8b17fafcd47afb77de93a2b1888752021-07-01T00:00:00Zhttps://doi.org/10.1038/s41598-021-93693-9https://doaj.org/toc/2045-2322Abstract The plastic deformation behavior of single crystals of two transition-metal diborides, ZrB2 and TiB2 with the AlB2 structure has been investigated at room temperature as a function of crystal orientation and specimen size by micropillar compression tests. Although plastic flow is not observed at all for their bulk single crystals at room temperature, plastic flow is successfully observed at room temperature by the operation of slip on {1 $${\bar{1}}$$ 1 ¯ 00}<11 $${\bar{2}}$$ 2 ¯ 3> in ZrB2 and by the operation of slip on {1 $${\bar{1}}$$ 1 ¯ 00}<0001> and {1 $${\bar{1}}$$ 1 ¯ 00}<11 $${\bar{2}}$$ 2 ¯ 0> in TiB2. Critical resolve shear stress values at room temperature are very high, exceeding 1 GPa for all observed slip systems; 3.01 GPa for {1 $${\bar{1}}$$ 1 ¯ 00}<11 $${\bar{2}}$$ 2 ¯ 3> slip in ZrB2 and 1.72 GPa and 5.17 GPa, respectively for {1 $${\bar{1}}$$ 1 ¯ 00}<0001> and {1 $${\bar{1}}$$ 1 ¯ 00}<11 $${\bar{2}}$$ 2 ¯ 0> slip in TiB2. The identified operative slip systems and their CRSS values are discussed in comparison with those identified in the corresponding bulk single crystals at high temperatures and those inferred from micro-hardness anisotropy in the early studies.Zhenghao ChenBhaskar PaulSanjib MajumdarNorihiko L. OkamotoKyosuke KishidaHaruyuki InuiShigeki OtaniNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 11, Iss 1, Pp 1-11 (2021)
institution DOAJ
collection DOAJ
language EN
topic Medicine
R
Science
Q
spellingShingle Medicine
R
Science
Q
Zhenghao Chen
Bhaskar Paul
Sanjib Majumdar
Norihiko L. Okamoto
Kyosuke Kishida
Haruyuki Inui
Shigeki Otani
Room-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression
description Abstract The plastic deformation behavior of single crystals of two transition-metal diborides, ZrB2 and TiB2 with the AlB2 structure has been investigated at room temperature as a function of crystal orientation and specimen size by micropillar compression tests. Although plastic flow is not observed at all for their bulk single crystals at room temperature, plastic flow is successfully observed at room temperature by the operation of slip on {1 $${\bar{1}}$$ 1 ¯ 00}<11 $${\bar{2}}$$ 2 ¯ 3> in ZrB2 and by the operation of slip on {1 $${\bar{1}}$$ 1 ¯ 00}<0001> and {1 $${\bar{1}}$$ 1 ¯ 00}<11 $${\bar{2}}$$ 2 ¯ 0> in TiB2. Critical resolve shear stress values at room temperature are very high, exceeding 1 GPa for all observed slip systems; 3.01 GPa for {1 $${\bar{1}}$$ 1 ¯ 00}<11 $${\bar{2}}$$ 2 ¯ 3> slip in ZrB2 and 1.72 GPa and 5.17 GPa, respectively for {1 $${\bar{1}}$$ 1 ¯ 00}<0001> and {1 $${\bar{1}}$$ 1 ¯ 00}<11 $${\bar{2}}$$ 2 ¯ 0> slip in TiB2. The identified operative slip systems and their CRSS values are discussed in comparison with those identified in the corresponding bulk single crystals at high temperatures and those inferred from micro-hardness anisotropy in the early studies.
format article
author Zhenghao Chen
Bhaskar Paul
Sanjib Majumdar
Norihiko L. Okamoto
Kyosuke Kishida
Haruyuki Inui
Shigeki Otani
author_facet Zhenghao Chen
Bhaskar Paul
Sanjib Majumdar
Norihiko L. Okamoto
Kyosuke Kishida
Haruyuki Inui
Shigeki Otani
author_sort Zhenghao Chen
title Room-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression
title_short Room-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression
title_full Room-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression
title_fullStr Room-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression
title_full_unstemmed Room-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression
title_sort room-temperature deformation of single crystals of zrb2 and tib2 with the hexagonal alb2 structure investigated by micropillar compression
publisher Nature Portfolio
publishDate 2021
url https://doaj.org/article/2be8b17fafcd47afb77de93a2b188875
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