Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods

Microstructural changes in grade 2 titanium generated by surface mechanical attrition treatment (SMAT) were studied using positron annihilation lifetime spectroscopy and complementary methods. A significant increase in the mean positron lifetime indicated many lattice defects introduced by SMAT. Two...

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Autores principales: Konrad Skowron, Mirosław Wróbel, Michał Mosiałek, Léa Le Joncour, Ewa Dryzek
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Lenguaje:EN
Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:2dbde30081ff4dde9d371fb1e8e786e62021-11-11T17:55:03ZGradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods10.3390/ma142163471996-1944https://doaj.org/article/2dbde30081ff4dde9d371fb1e8e786e62021-10-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/21/6347https://doaj.org/toc/1996-1944Microstructural changes in grade 2 titanium generated by surface mechanical attrition treatment (SMAT) were studied using positron annihilation lifetime spectroscopy and complementary methods. A significant increase in the mean positron lifetime indicated many lattice defects introduced by SMAT. Two positron lifetime components were resolved in the positron lifetime spectra measured. The longer lifetime revealed the presence of vacancy clusters containing about 3 or 4 vacancies, while the shorter one was attributed to the annihilation of positrons trapped at dislocations. The changes of the positron lifetime indicated a decreasing dislocation density and the presence of a deeper layer with a higher concentration of vacancy clusters at the distance from the treated surface for which the microhardness approached the value for the strain-free matrix. Electrochemical impedance spectroscopy showed the positive effect of SMAT on the corrosion resistance of the titanium studied in a saline environment also after removal of the original oxide layer that was formed during the SMAT.Konrad SkowronMirosław WróbelMichał MosiałekLéa Le JoncourEwa DryzekMDPI AGarticletitaniumsurface mechanical attrition treatmentSMATgradient structured materialspositron annihilation spectroscopycorrosionTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6347, p 6347 (2021)
institution DOAJ
collection DOAJ
language EN
topic titanium
surface mechanical attrition treatment
SMAT
gradient structured materials
positron annihilation spectroscopy
corrosion
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
spellingShingle titanium
surface mechanical attrition treatment
SMAT
gradient structured materials
positron annihilation spectroscopy
corrosion
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
Konrad Skowron
Mirosław Wróbel
Michał Mosiałek
Léa Le Joncour
Ewa Dryzek
Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods
description Microstructural changes in grade 2 titanium generated by surface mechanical attrition treatment (SMAT) were studied using positron annihilation lifetime spectroscopy and complementary methods. A significant increase in the mean positron lifetime indicated many lattice defects introduced by SMAT. Two positron lifetime components were resolved in the positron lifetime spectra measured. The longer lifetime revealed the presence of vacancy clusters containing about 3 or 4 vacancies, while the shorter one was attributed to the annihilation of positrons trapped at dislocations. The changes of the positron lifetime indicated a decreasing dislocation density and the presence of a deeper layer with a higher concentration of vacancy clusters at the distance from the treated surface for which the microhardness approached the value for the strain-free matrix. Electrochemical impedance spectroscopy showed the positive effect of SMAT on the corrosion resistance of the titanium studied in a saline environment also after removal of the original oxide layer that was formed during the SMAT.
format article
author Konrad Skowron
Mirosław Wróbel
Michał Mosiałek
Léa Le Joncour
Ewa Dryzek
author_facet Konrad Skowron
Mirosław Wróbel
Michał Mosiałek
Léa Le Joncour
Ewa Dryzek
author_sort Konrad Skowron
title Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods
title_short Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods
title_full Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods
title_fullStr Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods
title_full_unstemmed Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods
title_sort gradient microstructure induced by surface mechanical attrition treatment in grade 2 titanium studied using positron annihilation spectroscopy and complementary methods
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/2dbde30081ff4dde9d371fb1e8e786e6
work_keys_str_mv AT konradskowron gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods
AT mirosławwrobel gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods
AT michałmosiałek gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods
AT lealejoncour gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods
AT ewadryzek gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods
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