Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods
Microstructural changes in grade 2 titanium generated by surface mechanical attrition treatment (SMAT) were studied using positron annihilation lifetime spectroscopy and complementary methods. A significant increase in the mean positron lifetime indicated many lattice defects introduced by SMAT. Two...
Guardado en:
Autores principales: | , , , , |
---|---|
Formato: | article |
Lenguaje: | EN |
Publicado: |
MDPI AG
2021
|
Materias: | |
Acceso en línea: | https://doaj.org/article/2dbde30081ff4dde9d371fb1e8e786e6 |
Etiquetas: |
Agregar Etiqueta
Sin Etiquetas, Sea el primero en etiquetar este registro!
|
id |
oai:doaj.org-article:2dbde30081ff4dde9d371fb1e8e786e6 |
---|---|
record_format |
dspace |
spelling |
oai:doaj.org-article:2dbde30081ff4dde9d371fb1e8e786e62021-11-11T17:55:03ZGradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods10.3390/ma142163471996-1944https://doaj.org/article/2dbde30081ff4dde9d371fb1e8e786e62021-10-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/21/6347https://doaj.org/toc/1996-1944Microstructural changes in grade 2 titanium generated by surface mechanical attrition treatment (SMAT) were studied using positron annihilation lifetime spectroscopy and complementary methods. A significant increase in the mean positron lifetime indicated many lattice defects introduced by SMAT. Two positron lifetime components were resolved in the positron lifetime spectra measured. The longer lifetime revealed the presence of vacancy clusters containing about 3 or 4 vacancies, while the shorter one was attributed to the annihilation of positrons trapped at dislocations. The changes of the positron lifetime indicated a decreasing dislocation density and the presence of a deeper layer with a higher concentration of vacancy clusters at the distance from the treated surface for which the microhardness approached the value for the strain-free matrix. Electrochemical impedance spectroscopy showed the positive effect of SMAT on the corrosion resistance of the titanium studied in a saline environment also after removal of the original oxide layer that was formed during the SMAT.Konrad SkowronMirosław WróbelMichał MosiałekLéa Le JoncourEwa DryzekMDPI AGarticletitaniumsurface mechanical attrition treatmentSMATgradient structured materialspositron annihilation spectroscopycorrosionTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6347, p 6347 (2021) |
institution |
DOAJ |
collection |
DOAJ |
language |
EN |
topic |
titanium surface mechanical attrition treatment SMAT gradient structured materials positron annihilation spectroscopy corrosion Technology T Electrical engineering. Electronics. Nuclear engineering TK1-9971 Engineering (General). Civil engineering (General) TA1-2040 Microscopy QH201-278.5 Descriptive and experimental mechanics QC120-168.85 |
spellingShingle |
titanium surface mechanical attrition treatment SMAT gradient structured materials positron annihilation spectroscopy corrosion Technology T Electrical engineering. Electronics. Nuclear engineering TK1-9971 Engineering (General). Civil engineering (General) TA1-2040 Microscopy QH201-278.5 Descriptive and experimental mechanics QC120-168.85 Konrad Skowron Mirosław Wróbel Michał Mosiałek Léa Le Joncour Ewa Dryzek Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods |
description |
Microstructural changes in grade 2 titanium generated by surface mechanical attrition treatment (SMAT) were studied using positron annihilation lifetime spectroscopy and complementary methods. A significant increase in the mean positron lifetime indicated many lattice defects introduced by SMAT. Two positron lifetime components were resolved in the positron lifetime spectra measured. The longer lifetime revealed the presence of vacancy clusters containing about 3 or 4 vacancies, while the shorter one was attributed to the annihilation of positrons trapped at dislocations. The changes of the positron lifetime indicated a decreasing dislocation density and the presence of a deeper layer with a higher concentration of vacancy clusters at the distance from the treated surface for which the microhardness approached the value for the strain-free matrix. Electrochemical impedance spectroscopy showed the positive effect of SMAT on the corrosion resistance of the titanium studied in a saline environment also after removal of the original oxide layer that was formed during the SMAT. |
format |
article |
author |
Konrad Skowron Mirosław Wróbel Michał Mosiałek Léa Le Joncour Ewa Dryzek |
author_facet |
Konrad Skowron Mirosław Wróbel Michał Mosiałek Léa Le Joncour Ewa Dryzek |
author_sort |
Konrad Skowron |
title |
Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods |
title_short |
Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods |
title_full |
Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods |
title_fullStr |
Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods |
title_full_unstemmed |
Gradient Microstructure Induced by Surface Mechanical Attrition Treatment in Grade 2 Titanium Studied Using Positron Annihilation Spectroscopy and Complementary Methods |
title_sort |
gradient microstructure induced by surface mechanical attrition treatment in grade 2 titanium studied using positron annihilation spectroscopy and complementary methods |
publisher |
MDPI AG |
publishDate |
2021 |
url |
https://doaj.org/article/2dbde30081ff4dde9d371fb1e8e786e6 |
work_keys_str_mv |
AT konradskowron gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods AT mirosławwrobel gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods AT michałmosiałek gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods AT lealejoncour gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods AT ewadryzek gradientmicrostructureinducedbysurfacemechanicalattritiontreatmentingrade2titaniumstudiedusingpositronannihilationspectroscopyandcomplementarymethods |
_version_ |
1718431934151917568 |