Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel
Commercial rolled AISI 321 stainless steel samples were irradiated with Al<sup>+</sup> ions with an energy of 80 keV and fluence of 10<sup>17</sup> ion/cm<sup>2</sup>. The effect of Al implantation on the chemical and phase composition of the steel surface layer w...
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oai:doaj.org-article:3019e859694d44279228fe7bdf99140e2021-11-25T18:21:23ZEffect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel10.3390/met111117062075-4701https://doaj.org/article/3019e859694d44279228fe7bdf99140e2021-10-01T00:00:00Zhttps://www.mdpi.com/2075-4701/11/11/1706https://doaj.org/toc/2075-4701Commercial rolled AISI 321 stainless steel samples were irradiated with Al<sup>+</sup> ions with an energy of 80 keV and fluence of 10<sup>17</sup> ion/cm<sup>2</sup>. The effect of Al implantation on the chemical and phase composition of the steel surface layer was studied by X-ray electron spectroscopy and grazing beam mode of X-ray diffraction analysis. A thin surface layer down to a depth of 30 nm after Al<sup>+</sup> ions implantation consists mainly of metal oxides. In the near-surface layers of 5 nm in depth, a noticeable depletion in chromium and nickel was observed. A surface layer (up to 0.5 µm) of non-irradiated steel, in addition to the f.c.c. austenite γ-phase, consists of up to 20 vol% of the b.c.c. α′-phase, which formed at rolling as a result of mechanical deformation. Al implantation results in the significant increase in the α′-phase amount in the surface layer at a depth up to 2 µm. It is indicated that the observed γ → α′ transformation at ion irradiation proceeds predominantly as a result of the effect of post-cascade shock waves, but not as a result of the surface layer chemical composition changes.Pavel V. BykovVladimir Y. BayankinVictor V. TcherdyntsevVasiliy L. Vorob’evElena A. PechinaTatyana A. SviridovaAndrey A. ShushkovAndrey I. ChukavinSvetlana S. AlexandrovaMDPI AGarticlestainless steelaluminumion implantationsurface layerphase compositionMining engineering. MetallurgyTN1-997ENMetals, Vol 11, Iss 1706, p 1706 (2021) |
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stainless steel aluminum ion implantation surface layer phase composition Mining engineering. Metallurgy TN1-997 |
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stainless steel aluminum ion implantation surface layer phase composition Mining engineering. Metallurgy TN1-997 Pavel V. Bykov Vladimir Y. Bayankin Victor V. Tcherdyntsev Vasiliy L. Vorob’ev Elena A. Pechina Tatyana A. Sviridova Andrey A. Shushkov Andrey I. Chukavin Svetlana S. Alexandrova Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel |
description |
Commercial rolled AISI 321 stainless steel samples were irradiated with Al<sup>+</sup> ions with an energy of 80 keV and fluence of 10<sup>17</sup> ion/cm<sup>2</sup>. The effect of Al implantation on the chemical and phase composition of the steel surface layer was studied by X-ray electron spectroscopy and grazing beam mode of X-ray diffraction analysis. A thin surface layer down to a depth of 30 nm after Al<sup>+</sup> ions implantation consists mainly of metal oxides. In the near-surface layers of 5 nm in depth, a noticeable depletion in chromium and nickel was observed. A surface layer (up to 0.5 µm) of non-irradiated steel, in addition to the f.c.c. austenite γ-phase, consists of up to 20 vol% of the b.c.c. α′-phase, which formed at rolling as a result of mechanical deformation. Al implantation results in the significant increase in the α′-phase amount in the surface layer at a depth up to 2 µm. It is indicated that the observed γ → α′ transformation at ion irradiation proceeds predominantly as a result of the effect of post-cascade shock waves, but not as a result of the surface layer chemical composition changes. |
format |
article |
author |
Pavel V. Bykov Vladimir Y. Bayankin Victor V. Tcherdyntsev Vasiliy L. Vorob’ev Elena A. Pechina Tatyana A. Sviridova Andrey A. Shushkov Andrey I. Chukavin Svetlana S. Alexandrova |
author_facet |
Pavel V. Bykov Vladimir Y. Bayankin Victor V. Tcherdyntsev Vasiliy L. Vorob’ev Elena A. Pechina Tatyana A. Sviridova Andrey A. Shushkov Andrey I. Chukavin Svetlana S. Alexandrova |
author_sort |
Pavel V. Bykov |
title |
Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel |
title_short |
Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel |
title_full |
Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel |
title_fullStr |
Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel |
title_full_unstemmed |
Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel |
title_sort |
effect of aluminum ion irradiation on chemical and phase composition of surface layers of rolled aisi 321 stainless steel |
publisher |
MDPI AG |
publishDate |
2021 |
url |
https://doaj.org/article/3019e859694d44279228fe7bdf99140e |
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