Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel

Commercial rolled AISI 321 stainless steel samples were irradiated with Al<sup>+</sup> ions with an energy of 80 keV and fluence of 10<sup>17</sup> ion/cm<sup>2</sup>. The effect of Al implantation on the chemical and phase composition of the steel surface layer w...

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Autores principales: Pavel V. Bykov, Vladimir Y. Bayankin, Victor V. Tcherdyntsev, Vasiliy L. Vorob’ev, Elena A. Pechina, Tatyana A. Sviridova, Andrey A. Shushkov, Andrey I. Chukavin, Svetlana S. Alexandrova
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Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:3019e859694d44279228fe7bdf99140e2021-11-25T18:21:23ZEffect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel10.3390/met111117062075-4701https://doaj.org/article/3019e859694d44279228fe7bdf99140e2021-10-01T00:00:00Zhttps://www.mdpi.com/2075-4701/11/11/1706https://doaj.org/toc/2075-4701Commercial rolled AISI 321 stainless steel samples were irradiated with Al<sup>+</sup> ions with an energy of 80 keV and fluence of 10<sup>17</sup> ion/cm<sup>2</sup>. The effect of Al implantation on the chemical and phase composition of the steel surface layer was studied by X-ray electron spectroscopy and grazing beam mode of X-ray diffraction analysis. A thin surface layer down to a depth of 30 nm after Al<sup>+</sup> ions implantation consists mainly of metal oxides. In the near-surface layers of 5 nm in depth, a noticeable depletion in chromium and nickel was observed. A surface layer (up to 0.5 µm) of non-irradiated steel, in addition to the f.c.c. austenite γ-phase, consists of up to 20 vol% of the b.c.c. α′-phase, which formed at rolling as a result of mechanical deformation. Al implantation results in the significant increase in the α′-phase amount in the surface layer at a depth up to 2 µm. It is indicated that the observed γ → α′ transformation at ion irradiation proceeds predominantly as a result of the effect of post-cascade shock waves, but not as a result of the surface layer chemical composition changes.Pavel V. BykovVladimir Y. BayankinVictor V. TcherdyntsevVasiliy L. Vorob’evElena A. PechinaTatyana A. SviridovaAndrey A. ShushkovAndrey I. ChukavinSvetlana S. AlexandrovaMDPI AGarticlestainless steelaluminumion implantationsurface layerphase compositionMining engineering. MetallurgyTN1-997ENMetals, Vol 11, Iss 1706, p 1706 (2021)
institution DOAJ
collection DOAJ
language EN
topic stainless steel
aluminum
ion implantation
surface layer
phase composition
Mining engineering. Metallurgy
TN1-997
spellingShingle stainless steel
aluminum
ion implantation
surface layer
phase composition
Mining engineering. Metallurgy
TN1-997
Pavel V. Bykov
Vladimir Y. Bayankin
Victor V. Tcherdyntsev
Vasiliy L. Vorob’ev
Elena A. Pechina
Tatyana A. Sviridova
Andrey A. Shushkov
Andrey I. Chukavin
Svetlana S. Alexandrova
Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel
description Commercial rolled AISI 321 stainless steel samples were irradiated with Al<sup>+</sup> ions with an energy of 80 keV and fluence of 10<sup>17</sup> ion/cm<sup>2</sup>. The effect of Al implantation on the chemical and phase composition of the steel surface layer was studied by X-ray electron spectroscopy and grazing beam mode of X-ray diffraction analysis. A thin surface layer down to a depth of 30 nm after Al<sup>+</sup> ions implantation consists mainly of metal oxides. In the near-surface layers of 5 nm in depth, a noticeable depletion in chromium and nickel was observed. A surface layer (up to 0.5 µm) of non-irradiated steel, in addition to the f.c.c. austenite γ-phase, consists of up to 20 vol% of the b.c.c. α′-phase, which formed at rolling as a result of mechanical deformation. Al implantation results in the significant increase in the α′-phase amount in the surface layer at a depth up to 2 µm. It is indicated that the observed γ → α′ transformation at ion irradiation proceeds predominantly as a result of the effect of post-cascade shock waves, but not as a result of the surface layer chemical composition changes.
format article
author Pavel V. Bykov
Vladimir Y. Bayankin
Victor V. Tcherdyntsev
Vasiliy L. Vorob’ev
Elena A. Pechina
Tatyana A. Sviridova
Andrey A. Shushkov
Andrey I. Chukavin
Svetlana S. Alexandrova
author_facet Pavel V. Bykov
Vladimir Y. Bayankin
Victor V. Tcherdyntsev
Vasiliy L. Vorob’ev
Elena A. Pechina
Tatyana A. Sviridova
Andrey A. Shushkov
Andrey I. Chukavin
Svetlana S. Alexandrova
author_sort Pavel V. Bykov
title Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel
title_short Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel
title_full Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel
title_fullStr Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel
title_full_unstemmed Effect of Aluminum Ion Irradiation on Chemical and Phase Composition of Surface Layers of Rolled AISI 321 Stainless Steel
title_sort effect of aluminum ion irradiation on chemical and phase composition of surface layers of rolled aisi 321 stainless steel
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/3019e859694d44279228fe7bdf99140e
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