Sintesis Mg2+ Doped ZnO dengan Penambahan Albumen Ayam Ras Menggunakan Gabungan Metode Sol-Gel dan Sonokimia

Mg2+ doped ZnO has been successfully synthesized using a combination of sol-gel and sonochemical methods. Zinc acetate dihydrate was used as a precursor, magnesium chloride hexahydrate as a source of Mg dopant, methanol as a solvent, and chicken albumen was used as an additive to replace monoethanol...

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Autores principales:	Sherly Kasuma Warda Ningsih, Umar Kalmar Nizar, Bahrizal Bahrizal, Edi Nasra, Siti Fatimah Mutiara R
Formato:	article
Lenguaje:	EN ID
Publicado:	Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Andalas 2021
Materias:	mg2+ doped zno albumen sol-gel-sonochemical wurtzite hexagonal Chemistry QD1-999 Biochemistry QD415-436
Acceso en línea:	https://doaj.org/article/309d6926166f48a58c9382978437e575
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spelling	oai:doaj.org-article:309d6926166f48a58c9382978437e5752021-12-02T13:55:37ZSintesis Mg2+ Doped ZnO dengan Penambahan Albumen Ayam Ras Menggunakan Gabungan Metode Sol-Gel dan Sonokimia1978-628X2476-896010.25077/jrk.v12i1.374https://doaj.org/article/309d6926166f48a58c9382978437e5752021-04-01T00:00:00Zhttp://jrk.fmipa.unand.ac.id/index.php/jrk/article/view/374https://doaj.org/toc/1978-628Xhttps://doaj.org/toc/2476-8960Mg2+ doped ZnO has been successfully synthesized using a combination of sol-gel and sonochemical methods. Zinc acetate dihydrate was used as a precursor, magnesium chloride hexahydrate as a source of Mg dopant, methanol as a solvent, and chicken albumen was used as an additive to replace monoethanolamine. The sol was heated at 110 °C for 1 hour. The gel formed was calcined at 600 °C for 3 hours. FTIR analysis shows that the absorbance band around 400-450 cm-1 indicates Mg-O stretching, the absorbance band around 500-550 cm-1 indicates Zn-O stretching, the absorbance band around 400-550 cm-1 shows Zn-O-Mg bonds. Mg. Measurements with UV-DRS, obtained the smallest ZnO band gap value doped Mg2+ around 2.7 eV with the addition of 10 mL albumen. The resulting crystal structure was wurtzite with crystal size with the addition of 10, 20, 30, 40 and 50 mL albumen were 25.22-55.91 nm, 32.99-75.87 nm, 45.92-83.91 nm, 45.92-75.89 nm and 46.15-71.47 nm respectively. SEM photo of Mg2+ doped ZnO with the addition of 10 mL of albumen has a hexagonal surface morphology.Sherly Kasuma Warda NingsihUmar Kalmar NizarBahrizal BahrizalEdi NasraSiti Fatimah Mutiara RDepartment of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Andalasarticlemg2+ doped znoalbumensol-gel-sonochemicalwurtzitehexagonalChemistryQD1-999BiochemistryQD415-436ENIDJurnal Riset Kimia, Vol 12, Iss 1, Pp 27-35 (2021)
institution	DOAJ
collection	DOAJ
language	EN ID
topic	mg2+ doped zno albumen sol-gel-sonochemical wurtzite hexagonal Chemistry QD1-999 Biochemistry QD415-436
spellingShingle	mg2+ doped zno albumen sol-gel-sonochemical wurtzite hexagonal Chemistry QD1-999 Biochemistry QD415-436 Sherly Kasuma Warda Ningsih Umar Kalmar Nizar Bahrizal Bahrizal Edi Nasra Siti Fatimah Mutiara R Sintesis Mg2+ Doped ZnO dengan Penambahan Albumen Ayam Ras Menggunakan Gabungan Metode Sol-Gel dan Sonokimia
description	Mg2+ doped ZnO has been successfully synthesized using a combination of sol-gel and sonochemical methods. Zinc acetate dihydrate was used as a precursor, magnesium chloride hexahydrate as a source of Mg dopant, methanol as a solvent, and chicken albumen was used as an additive to replace monoethanolamine. The sol was heated at 110 °C for 1 hour. The gel formed was calcined at 600 °C for 3 hours. FTIR analysis shows that the absorbance band around 400-450 cm-1 indicates Mg-O stretching, the absorbance band around 500-550 cm-1 indicates Zn-O stretching, the absorbance band around 400-550 cm-1 shows Zn-O-Mg bonds. Mg. Measurements with UV-DRS, obtained the smallest ZnO band gap value doped Mg2+ around 2.7 eV with the addition of 10 mL albumen. The resulting crystal structure was wurtzite with crystal size with the addition of 10, 20, 30, 40 and 50 mL albumen were 25.22-55.91 nm, 32.99-75.87 nm, 45.92-83.91 nm, 45.92-75.89 nm and 46.15-71.47 nm respectively. SEM photo of Mg2+ doped ZnO with the addition of 10 mL of albumen has a hexagonal surface morphology.
format	article
author	Sherly Kasuma Warda Ningsih Umar Kalmar Nizar Bahrizal Bahrizal Edi Nasra Siti Fatimah Mutiara R
author_facet	Sherly Kasuma Warda Ningsih Umar Kalmar Nizar Bahrizal Bahrizal Edi Nasra Siti Fatimah Mutiara R
author_sort	Sherly Kasuma Warda Ningsih
title	Sintesis Mg2+ Doped ZnO dengan Penambahan Albumen Ayam Ras Menggunakan Gabungan Metode Sol-Gel dan Sonokimia
title_short	Sintesis Mg2+ Doped ZnO dengan Penambahan Albumen Ayam Ras Menggunakan Gabungan Metode Sol-Gel dan Sonokimia
title_full	Sintesis Mg2+ Doped ZnO dengan Penambahan Albumen Ayam Ras Menggunakan Gabungan Metode Sol-Gel dan Sonokimia
title_fullStr	Sintesis Mg2+ Doped ZnO dengan Penambahan Albumen Ayam Ras Menggunakan Gabungan Metode Sol-Gel dan Sonokimia
title_full_unstemmed	Sintesis Mg2+ Doped ZnO dengan Penambahan Albumen Ayam Ras Menggunakan Gabungan Metode Sol-Gel dan Sonokimia
title_sort	sintesis mg2+ doped zno dengan penambahan albumen ayam ras menggunakan gabungan metode sol-gel dan sonokimia
publisher	Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Andalas
publishDate	2021
url	https://doaj.org/article/309d6926166f48a58c9382978437e575
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Sintesis Mg2+ Doped ZnO dengan Penambahan Albumen Ayam Ras Menggunakan Gabungan Metode Sol-Gel dan Sonokimia

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