Synthesis and Characterization of Nanocrystalline Zeolite Y

Worldwide attention is being focused on nanocrystalline zeolites and they are replacing conventional ones due to their pronounced potential in many fields. In this study, NaY zeolite has been prepared hydrothermally using sol –gel method and modified to the proton type by ion –exchange process....

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Autores principales:	Nada S. Ahmedzeki, Selahattin Yilmaz, Ban A. Al-Tabbakh
Formato:	article
Lenguaje:	EN
Publicado:	Al-Khwarizmi College of Engineering – University of Baghdad 2017
Materias:	Zeolite Y, nanozeolite sol-gel method characterization Chemical engineering TP155-156 Engineering (General). Civil engineering (General) TA1-2040
Acceso en línea:	https://doaj.org/article/31b57e7374e94e52b72553f078004f3f
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spelling	oai:doaj.org-article:31b57e7374e94e52b72553f078004f3f2021-12-02T04:46:21ZSynthesis and Characterization of Nanocrystalline Zeolite Y1818-11712312-0789https://doaj.org/article/31b57e7374e94e52b72553f078004f3f2017-12-01T00:00:00Zhttp://alkej.uobaghdad.edu.iq/index.php/alkej/article/view/286https://doaj.org/toc/1818-1171https://doaj.org/toc/2312-0789 Worldwide attention is being focused on nanocrystalline zeolites and they are replacing conventional ones due to their pronounced potential in many fields. In this study, NaY zeolite has been prepared hydrothermally using sol –gel method and modified to the proton type by ion –exchange process. Characterization is made using X-ray diffraction (XRD), thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), Atomic force microscopy (AFM), Brunauer –Emmet- Teller (BET) nitrogen adsorption method, Ammonia Temperature programmed desorption (NH3-TPD) and Scanning electron microscopy( SEM). The effect of aging time, silica to alumina ratio is studied and the results show well defined crystalline structure with nano particle size (70 and 81nm) with surface area of 499m2/gm. Nada S. AhmedzekiSelahattin YilmazBan A. Al-TabbakhAl-Khwarizmi College of Engineering – University of BaghdadarticleZeolite Y, nanozeolitesol-gel methodcharacterizationChemical engineeringTP155-156Engineering (General). Civil engineering (General)TA1-2040ENAl-Khawarizmi Engineering Journal, Vol 12, Iss 1 (2017)
institution	DOAJ
collection	DOAJ
language	EN
topic	Zeolite Y, nanozeolite sol-gel method characterization Chemical engineering TP155-156 Engineering (General). Civil engineering (General) TA1-2040
spellingShingle	Zeolite Y, nanozeolite sol-gel method characterization Chemical engineering TP155-156 Engineering (General). Civil engineering (General) TA1-2040 Nada S. Ahmedzeki Selahattin Yilmaz Ban A. Al-Tabbakh Synthesis and Characterization of Nanocrystalline Zeolite Y
description	Worldwide attention is being focused on nanocrystalline zeolites and they are replacing conventional ones due to their pronounced potential in many fields. In this study, NaY zeolite has been prepared hydrothermally using sol –gel method and modified to the proton type by ion –exchange process. Characterization is made using X-ray diffraction (XRD), thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), Atomic force microscopy (AFM), Brunauer –Emmet- Teller (BET) nitrogen adsorption method, Ammonia Temperature programmed desorption (NH3-TPD) and Scanning electron microscopy( SEM). The effect of aging time, silica to alumina ratio is studied and the results show well defined crystalline structure with nano particle size (70 and 81nm) with surface area of 499m2/gm.
format	article
author	Nada S. Ahmedzeki Selahattin Yilmaz Ban A. Al-Tabbakh
author_facet	Nada S. Ahmedzeki Selahattin Yilmaz Ban A. Al-Tabbakh
author_sort	Nada S. Ahmedzeki
title	Synthesis and Characterization of Nanocrystalline Zeolite Y
title_short	Synthesis and Characterization of Nanocrystalline Zeolite Y
title_full	Synthesis and Characterization of Nanocrystalline Zeolite Y
title_fullStr	Synthesis and Characterization of Nanocrystalline Zeolite Y
title_full_unstemmed	Synthesis and Characterization of Nanocrystalline Zeolite Y
title_sort	synthesis and characterization of nanocrystalline zeolite y
publisher	Al-Khwarizmi College of Engineering – University of Baghdad
publishDate	2017
url	https://doaj.org/article/31b57e7374e94e52b72553f078004f3f
work_keys_str_mv	AT nadasahmedzeki synthesisandcharacterizationofnanocrystallinezeolitey AT selahattinyilmaz synthesisandcharacterizationofnanocrystallinezeolitey AT banaaltabbakh synthesisandcharacterizationofnanocrystallinezeolitey
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Synthesis and Characterization of Nanocrystalline Zeolite Y

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