Synthesis and Activation Study of Iron (Fe) Based Fischer Tropsch (FT) Catalyst Using Sol-gel Method

As oil consumption increases from year to year, efforts need to be made to increase energy reserves by developing new renewable energy. One way to develop energy sources is by the synthesis Fischer Tropsch (FT). FT is a synthetic gas conversion reaction (mixture of CO and H2) into a long chain hydro...

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Autores principales: Muchammad Zainul Anwar, Rachmat Triandi Tjahjanto, Uswatun Hasanah
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Lenguaje:EN
Publicado: University of Brawijaya 2019
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Acceso en línea:https://doaj.org/article/31ebf72c0ab8437bb324b269594a59c4
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spelling oai:doaj.org-article:31ebf72c0ab8437bb324b269594a59c42021-12-02T14:38:20ZSynthesis and Activation Study of Iron (Fe) Based Fischer Tropsch (FT) Catalyst Using Sol-gel Method2302-46902302-4690https://doaj.org/article/31ebf72c0ab8437bb324b269594a59c42019-12-01T00:00:00Zhttps://jpacr.ub.ac.id/index.php/jpacr/article/view/480/pdfhttps://doaj.org/toc/2302-4690https://doaj.org/toc/2302-4690As oil consumption increases from year to year, efforts need to be made to increase energy reserves by developing new renewable energy. One way to develop energy sources is by the synthesis Fischer Tropsch (FT). FT is a synthetic gas conversion reaction (mixture of CO and H2) into a long chain hydrocarbon mixture. The FT reaction requires a catalyst called the FT catalyst. So far, many studies that examine the effectiveness of catalysts in converting synthesis gas into long chain hydrocarbons, but rarely information about the composition of the phases that exist on the surface of the catalyst. To study about it, we synthesized FT catalysts at various variations of calcination temperature. Fe(NO3)3 as a precursor and Cu(NO3)2 as promoter (20:1) used in this study. The calcination temperature used are 300, 500, and 700°C. Characterization and analysis of catalysts were formed with XRD and SEM-EDX. Calcined catalysts were activated using CO2 and H2 gas and then re-characterized with XRD and SEM-EDX. Calcination results the formation of an iron oxide phase, while activation results the formation of iron carbide and zero Fe phases.Muchammad Zainul AnwarRachmat Triandi TjahjantoUswatun HasanahUniversity of Brawijayaarticlefischer tropsch catalystsol-gelcalcinationactivationChemistryQD1-999ENJournal of Pure and Applied Chemistry Research, Vol 8, Iss 3, Pp 217-224 (2019)
institution DOAJ
collection DOAJ
language EN
topic fischer tropsch catalyst
sol-gel
calcination
activation
Chemistry
QD1-999
spellingShingle fischer tropsch catalyst
sol-gel
calcination
activation
Chemistry
QD1-999
Muchammad Zainul Anwar
Rachmat Triandi Tjahjanto
Uswatun Hasanah
Synthesis and Activation Study of Iron (Fe) Based Fischer Tropsch (FT) Catalyst Using Sol-gel Method
description As oil consumption increases from year to year, efforts need to be made to increase energy reserves by developing new renewable energy. One way to develop energy sources is by the synthesis Fischer Tropsch (FT). FT is a synthetic gas conversion reaction (mixture of CO and H2) into a long chain hydrocarbon mixture. The FT reaction requires a catalyst called the FT catalyst. So far, many studies that examine the effectiveness of catalysts in converting synthesis gas into long chain hydrocarbons, but rarely information about the composition of the phases that exist on the surface of the catalyst. To study about it, we synthesized FT catalysts at various variations of calcination temperature. Fe(NO3)3 as a precursor and Cu(NO3)2 as promoter (20:1) used in this study. The calcination temperature used are 300, 500, and 700°C. Characterization and analysis of catalysts were formed with XRD and SEM-EDX. Calcined catalysts were activated using CO2 and H2 gas and then re-characterized with XRD and SEM-EDX. Calcination results the formation of an iron oxide phase, while activation results the formation of iron carbide and zero Fe phases.
format article
author Muchammad Zainul Anwar
Rachmat Triandi Tjahjanto
Uswatun Hasanah
author_facet Muchammad Zainul Anwar
Rachmat Triandi Tjahjanto
Uswatun Hasanah
author_sort Muchammad Zainul Anwar
title Synthesis and Activation Study of Iron (Fe) Based Fischer Tropsch (FT) Catalyst Using Sol-gel Method
title_short Synthesis and Activation Study of Iron (Fe) Based Fischer Tropsch (FT) Catalyst Using Sol-gel Method
title_full Synthesis and Activation Study of Iron (Fe) Based Fischer Tropsch (FT) Catalyst Using Sol-gel Method
title_fullStr Synthesis and Activation Study of Iron (Fe) Based Fischer Tropsch (FT) Catalyst Using Sol-gel Method
title_full_unstemmed Synthesis and Activation Study of Iron (Fe) Based Fischer Tropsch (FT) Catalyst Using Sol-gel Method
title_sort synthesis and activation study of iron (fe) based fischer tropsch (ft) catalyst using sol-gel method
publisher University of Brawijaya
publishDate 2019
url https://doaj.org/article/31ebf72c0ab8437bb324b269594a59c4
work_keys_str_mv AT muchammadzainulanwar synthesisandactivationstudyofironfebasedfischertropschftcatalystusingsolgelmethod
AT rachmattrianditjahjanto synthesisandactivationstudyofironfebasedfischertropschftcatalystusingsolgelmethod
AT uswatunhasanah synthesisandactivationstudyofironfebasedfischertropschftcatalystusingsolgelmethod
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