Interfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy
Solid-state NMR can in principle be used to study calcium environments in biomaterials such as bones/teeth, but43Ca lacks receptivity. Here the authors present an approach to acquire 43Ca data for hydroxyapatite at its natural isotopic abundance, distinguishing between core and surface Ca sites.
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Nature Portfolio
2017
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oai:doaj.org-article:32a9adbda9b74b15922d2b5cb897bf632021-12-02T14:40:37ZInterfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy10.1038/ncomms141042041-1723https://doaj.org/article/32a9adbda9b74b15922d2b5cb897bf632017-01-01T00:00:00Zhttps://doi.org/10.1038/ncomms14104https://doaj.org/toc/2041-1723Solid-state NMR can in principle be used to study calcium environments in biomaterials such as bones/teeth, but43Ca lacks receptivity. Here the authors present an approach to acquire 43Ca data for hydroxyapatite at its natural isotopic abundance, distinguishing between core and surface Ca sites.Daniel LeeCésar LeroyCharlène CrevantLaure Bonhomme-CouryFlorence BabonneauDanielle LaurencinChristian BonhommeGaël De PaëpeNature PortfolioarticleScienceQENNature Communications, Vol 8, Iss 1, Pp 1-7 (2017) |
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Science Q Daniel Lee César Leroy Charlène Crevant Laure Bonhomme-Coury Florence Babonneau Danielle Laurencin Christian Bonhomme Gaël De Paëpe Interfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy |
description |
Solid-state NMR can in principle be used to study calcium environments in biomaterials such as bones/teeth, but43Ca lacks receptivity. Here the authors present an approach to acquire 43Ca data for hydroxyapatite at its natural isotopic abundance, distinguishing between core and surface Ca sites. |
format |
article |
author |
Daniel Lee César Leroy Charlène Crevant Laure Bonhomme-Coury Florence Babonneau Danielle Laurencin Christian Bonhomme Gaël De Paëpe |
author_facet |
Daniel Lee César Leroy Charlène Crevant Laure Bonhomme-Coury Florence Babonneau Danielle Laurencin Christian Bonhomme Gaël De Paëpe |
author_sort |
Daniel Lee |
title |
Interfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy |
title_short |
Interfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy |
title_full |
Interfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy |
title_fullStr |
Interfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy |
title_full_unstemmed |
Interfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy |
title_sort |
interfacial ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43ca nmr spectroscopy |
publisher |
Nature Portfolio |
publishDate |
2017 |
url |
https://doaj.org/article/32a9adbda9b74b15922d2b5cb897bf63 |
work_keys_str_mv |
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_version_ |
1718390227560562688 |