Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments

In this study, several biodegradable Mg alloys (Mg5Zn, Mg5Zn0.3Ca, Mg5Zn0.15Ca, and Mg5Zn0.15Ca0.15Zr, numbers in wt%) were investigated after thermomechanical processing via high-pressure torsion (HPT) at elevated temperature as well as after additional heat treatments. Indirect and direct analyses...

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Autores principales: Andrea Mizelli-Ojdanic, Jelena Horky, Bernhard Mingler, Mattia Fanetti, Sandra Gardonio, Matjaz Valant, Bartosz Sulkowski, Erhard Schafler, Dmytro Orlov, Michael J. Zehetbauer
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spelling oai:doaj.org-article:34bb22de690a47798ad239b7de2724de2021-11-11T17:58:42ZEnhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments10.3390/ma142163991996-1944https://doaj.org/article/34bb22de690a47798ad239b7de2724de2021-10-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/21/6399https://doaj.org/toc/1996-1944In this study, several biodegradable Mg alloys (Mg5Zn, Mg5Zn0.3Ca, Mg5Zn0.15Ca, and Mg5Zn0.15Ca0.15Zr, numbers in wt%) were investigated after thermomechanical processing via high-pressure torsion (HPT) at elevated temperature as well as after additional heat treatments. Indirect and direct analyses of microstructure revealed that the significant strength increases arise not only from dislocations and precipitates but also from vacancy agglomerates. By contrast with former low-temperature processing routes applied by the authors, a significant ductility was obtained because of temperature-induced dynamic recovery. The low initial values of Young’s modulus were not significantly affected by warm HPT-processing. nor by heat treatments afterwards. Also, corrosion resistance did not change or even increase during those treatments. Altogether, the study reveals a viable processing route for the optimization of Mg alloys to provide enhanced mechanical properties while leaving the corrosion properties unaffected, suggesting it for the use as biodegradable implant material.Andrea Mizelli-OjdanicJelena HorkyBernhard MinglerMattia FanettiSandra GardonioMatjaz ValantBartosz SulkowskiErhard SchaflerDmytro OrlovMichael J. ZehetbauerMDPI AGarticlesevere plastic deformation (SPD)precipitatesvacancy agglomeratesmagnesium alloysbiodegradabilityTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6399, p 6399 (2021)
institution DOAJ
collection DOAJ
language EN
topic severe plastic deformation (SPD)
precipitates
vacancy agglomerates
magnesium alloys
biodegradability
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
spellingShingle severe plastic deformation (SPD)
precipitates
vacancy agglomerates
magnesium alloys
biodegradability
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
Andrea Mizelli-Ojdanic
Jelena Horky
Bernhard Mingler
Mattia Fanetti
Sandra Gardonio
Matjaz Valant
Bartosz Sulkowski
Erhard Schafler
Dmytro Orlov
Michael J. Zehetbauer
Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
description In this study, several biodegradable Mg alloys (Mg5Zn, Mg5Zn0.3Ca, Mg5Zn0.15Ca, and Mg5Zn0.15Ca0.15Zr, numbers in wt%) were investigated after thermomechanical processing via high-pressure torsion (HPT) at elevated temperature as well as after additional heat treatments. Indirect and direct analyses of microstructure revealed that the significant strength increases arise not only from dislocations and precipitates but also from vacancy agglomerates. By contrast with former low-temperature processing routes applied by the authors, a significant ductility was obtained because of temperature-induced dynamic recovery. The low initial values of Young’s modulus were not significantly affected by warm HPT-processing. nor by heat treatments afterwards. Also, corrosion resistance did not change or even increase during those treatments. Altogether, the study reveals a viable processing route for the optimization of Mg alloys to provide enhanced mechanical properties while leaving the corrosion properties unaffected, suggesting it for the use as biodegradable implant material.
format article
author Andrea Mizelli-Ojdanic
Jelena Horky
Bernhard Mingler
Mattia Fanetti
Sandra Gardonio
Matjaz Valant
Bartosz Sulkowski
Erhard Schafler
Dmytro Orlov
Michael J. Zehetbauer
author_facet Andrea Mizelli-Ojdanic
Jelena Horky
Bernhard Mingler
Mattia Fanetti
Sandra Gardonio
Matjaz Valant
Bartosz Sulkowski
Erhard Schafler
Dmytro Orlov
Michael J. Zehetbauer
author_sort Andrea Mizelli-Ojdanic
title Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_short Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_full Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_fullStr Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_full_unstemmed Enhancing the Mechanical Properties of Biodegradable Mg Alloys Processed by Warm HPT and Thermal Treatments
title_sort enhancing the mechanical properties of biodegradable mg alloys processed by warm hpt and thermal treatments
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/34bb22de690a47798ad239b7de2724de
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