A novel method for in situ TEM measurements of adhesion at the diamond–metal interface

Abstract The procedure for in situ TEM measurements of bonding strength (adhesion) between diamond and the metal matrix using a Hysitron PI 95 TEM Picoindenter holder for mechanical tests and Push-to-Pull devices was proposed. For tensile tests, dog-bone shaped lamellae 280–330 nm thick and ~ 2.5 µm...

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Autores principales: P. A. Loginov, D. A. Sidorenko, A. S. Orekhov, E. A. Levashov
Formato: article
Lenguaje:EN
Publicado: Nature Portfolio 2021
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Acceso en línea:https://doaj.org/article/353d57a57db946cdb31d593b7e92f823
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spelling oai:doaj.org-article:353d57a57db946cdb31d593b7e92f8232021-12-02T14:58:53ZA novel method for in situ TEM measurements of adhesion at the diamond–metal interface10.1038/s41598-021-89536-22045-2322https://doaj.org/article/353d57a57db946cdb31d593b7e92f8232021-05-01T00:00:00Zhttps://doi.org/10.1038/s41598-021-89536-2https://doaj.org/toc/2045-2322Abstract The procedure for in situ TEM measurements of bonding strength (adhesion) between diamond and the metal matrix using a Hysitron PI 95 TEM Picoindenter holder for mechanical tests and Push-to-Pull devices was proposed. For tensile tests, dog-bone shaped lamellae 280–330 nm thick and ~ 2.5 µm long were used as objects of study. The lamellae were manufactured using the focused ion beam technology from the metal–diamond interface of diamond-containing composite material with a single-phase binder made of Fe–Co–Ni alloy. The experimentally determined bonding strength was 110 MPa.P. A. LoginovD. A. SidorenkoA. S. OrekhovE. A. LevashovNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 11, Iss 1, Pp 1-10 (2021)
institution DOAJ
collection DOAJ
language EN
topic Medicine
R
Science
Q
spellingShingle Medicine
R
Science
Q
P. A. Loginov
D. A. Sidorenko
A. S. Orekhov
E. A. Levashov
A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
description Abstract The procedure for in situ TEM measurements of bonding strength (adhesion) between diamond and the metal matrix using a Hysitron PI 95 TEM Picoindenter holder for mechanical tests and Push-to-Pull devices was proposed. For tensile tests, dog-bone shaped lamellae 280–330 nm thick and ~ 2.5 µm long were used as objects of study. The lamellae were manufactured using the focused ion beam technology from the metal–diamond interface of diamond-containing composite material with a single-phase binder made of Fe–Co–Ni alloy. The experimentally determined bonding strength was 110 MPa.
format article
author P. A. Loginov
D. A. Sidorenko
A. S. Orekhov
E. A. Levashov
author_facet P. A. Loginov
D. A. Sidorenko
A. S. Orekhov
E. A. Levashov
author_sort P. A. Loginov
title A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_short A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_full A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_fullStr A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_full_unstemmed A novel method for in situ TEM measurements of adhesion at the diamond–metal interface
title_sort novel method for in situ tem measurements of adhesion at the diamond–metal interface
publisher Nature Portfolio
publishDate 2021
url https://doaj.org/article/353d57a57db946cdb31d593b7e92f823
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