Effects of He-D Interaction on Irradiation-Induced Swelling in Fe9Cr Alloys

The atomic-scale defects such as (deuterium, helium)-vacancy clusters in nuclear energy materials are one of the causes for the deterioration of the macroscopic properties of materials. Unfortunately, they cannot be observed by transmission electron microscopy (TEM) before they grow to the nanometer...

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Autores principales: Haibiao Wu, Zhen Wang, Te Zhu, Qiu Xu, Baoyi Wang, Detao Xiao, Xingzhong Cao
Formato: article
Lenguaje:EN
Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:3ea68402418440c393e9ca5c593485e32021-11-11T18:11:02ZEffects of He-D Interaction on Irradiation-Induced Swelling in Fe9Cr Alloys10.3390/ma142166691996-1944https://doaj.org/article/3ea68402418440c393e9ca5c593485e32021-11-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/21/6669https://doaj.org/toc/1996-1944The atomic-scale defects such as (deuterium, helium)-vacancy clusters in nuclear energy materials are one of the causes for the deterioration of the macroscopic properties of materials. Unfortunately, they cannot be observed by transmission electron microscopy (TEM) before they grow to the nanometer scale. Positron annihilation spectroscopy (PAS) has been proven to be sensitive to open-volume defects, and could characterize the evolution of the size and concentration of the vacancy-like nanoclusters. We have investigated the effects of He-D interaction on the formation of nanoscale cavities in Fe9Cr alloys by PAS and TEM. The results show that small-sized bubbles are formed in the specimen irradiated with 5 × 10<sup>16</sup> He<sup>+</sup>/cm<sup>2</sup>, and the subsequent implanted D-ions contribute to the growth of these helium bubbles. The most likely reason is that helium bubbles previously formed in the sample captured deuterium injected later, causing bubbles to grow. In the lower dose He-irradiated samples, a large number of small dislocations and vacancies are generated and form helium-vacancy clusters with the helium atoms.Haibiao WuZhen WangTe ZhuQiu XuBaoyi WangDetao XiaoXingzhong CaoMDPI AGarticlehelium/deuteriumnanoclusterspositron annihilation spectroscopyirradiation damageTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6669, p 6669 (2021)
institution DOAJ
collection DOAJ
language EN
topic helium/deuterium
nanoclusters
positron annihilation spectroscopy
irradiation damage
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
spellingShingle helium/deuterium
nanoclusters
positron annihilation spectroscopy
irradiation damage
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
Haibiao Wu
Zhen Wang
Te Zhu
Qiu Xu
Baoyi Wang
Detao Xiao
Xingzhong Cao
Effects of He-D Interaction on Irradiation-Induced Swelling in Fe9Cr Alloys
description The atomic-scale defects such as (deuterium, helium)-vacancy clusters in nuclear energy materials are one of the causes for the deterioration of the macroscopic properties of materials. Unfortunately, they cannot be observed by transmission electron microscopy (TEM) before they grow to the nanometer scale. Positron annihilation spectroscopy (PAS) has been proven to be sensitive to open-volume defects, and could characterize the evolution of the size and concentration of the vacancy-like nanoclusters. We have investigated the effects of He-D interaction on the formation of nanoscale cavities in Fe9Cr alloys by PAS and TEM. The results show that small-sized bubbles are formed in the specimen irradiated with 5 × 10<sup>16</sup> He<sup>+</sup>/cm<sup>2</sup>, and the subsequent implanted D-ions contribute to the growth of these helium bubbles. The most likely reason is that helium bubbles previously formed in the sample captured deuterium injected later, causing bubbles to grow. In the lower dose He-irradiated samples, a large number of small dislocations and vacancies are generated and form helium-vacancy clusters with the helium atoms.
format article
author Haibiao Wu
Zhen Wang
Te Zhu
Qiu Xu
Baoyi Wang
Detao Xiao
Xingzhong Cao
author_facet Haibiao Wu
Zhen Wang
Te Zhu
Qiu Xu
Baoyi Wang
Detao Xiao
Xingzhong Cao
author_sort Haibiao Wu
title Effects of He-D Interaction on Irradiation-Induced Swelling in Fe9Cr Alloys
title_short Effects of He-D Interaction on Irradiation-Induced Swelling in Fe9Cr Alloys
title_full Effects of He-D Interaction on Irradiation-Induced Swelling in Fe9Cr Alloys
title_fullStr Effects of He-D Interaction on Irradiation-Induced Swelling in Fe9Cr Alloys
title_full_unstemmed Effects of He-D Interaction on Irradiation-Induced Swelling in Fe9Cr Alloys
title_sort effects of he-d interaction on irradiation-induced swelling in fe9cr alloys
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/3ea68402418440c393e9ca5c593485e3
work_keys_str_mv AT haibiaowu effectsofhedinteractiononirradiationinducedswellinginfe9cralloys
AT zhenwang effectsofhedinteractiononirradiationinducedswellinginfe9cralloys
AT tezhu effectsofhedinteractiononirradiationinducedswellinginfe9cralloys
AT qiuxu effectsofhedinteractiononirradiationinducedswellinginfe9cralloys
AT baoyiwang effectsofhedinteractiononirradiationinducedswellinginfe9cralloys
AT detaoxiao effectsofhedinteractiononirradiationinducedswellinginfe9cralloys
AT xingzhongcao effectsofhedinteractiononirradiationinducedswellinginfe9cralloys
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