A Wet-Spinning Process for Producing Carbon Nanotube/Polyvinylidene Fluoride Fibers Having Highly Consistent Electrical and Mechanical Properties

Studies of polymer/carbon nanotube (CNT) fibers typically focus on optimizing the overall properties, and the effects of structural variation on these properties are ignored. Thus, we investigated the longitudinal variation in the properties of CNT/polyvinylidene fluoride (CNT/PVDF) fibers prepared...

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Autores principales: Ki-Weon Kang, Chan-Woong Choi, Ji-Won Jin
Formato: article
Lenguaje:EN
Publicado: MDPI AG 2021
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Acceso en línea:https://doaj.org/article/4066b1b3f60846debdad25fa8ce656c5
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spelling oai:doaj.org-article:4066b1b3f60846debdad25fa8ce656c52021-11-25T18:49:43ZA Wet-Spinning Process for Producing Carbon Nanotube/Polyvinylidene Fluoride Fibers Having Highly Consistent Electrical and Mechanical Properties10.3390/polym132240482073-4360https://doaj.org/article/4066b1b3f60846debdad25fa8ce656c52021-11-01T00:00:00Zhttps://www.mdpi.com/2073-4360/13/22/4048https://doaj.org/toc/2073-4360Studies of polymer/carbon nanotube (CNT) fibers typically focus on optimizing the overall properties, and the effects of structural variation on these properties are ignored. Thus, we investigated the longitudinal variation in the properties of CNT/polyvinylidene fluoride (CNT/PVDF) fibers prepared by wet spinning a solution of multi-walled nanotubes, PVDF, and dimethylacetamide. To this end, materials for the CNT/PVDF fiber were selected, and a dope solution was prepared using MWNT, PVDF, and dimethylacetamide (DMAc). To consider the process parameters that would affect the performance of the CNT/PVDF fiber during the wet-spinning process using the dope solution, the initial conditions for wet spinning were selected, including bath concentration, bath temperature, drying temperature, and elongation, and the CNT/PVDF fiber was spun under the corresponding conditions. Additionally, three performance stabilization processes were proposed to improve the initial conditions for wet spinning and manufacturing the fiber. Lastly, to confirm the reliability of the CNT/PVDF fiber in all sections, tensile strength, electrical conductivity, and cross-sectional images were analyzed for the 30 m, 60 m, and 90 m sections of the fiber, and the reliability of the wet-spinning process was verified.Ki-Weon KangChan-Woong ChoiJi-Won JinMDPI AGarticlecarbon nanotubeelectrical conductivitypolyvinylidene fluoridetensile strengthwet spinningOrganic chemistryQD241-441ENPolymers, Vol 13, Iss 4048, p 4048 (2021)
institution DOAJ
collection DOAJ
language EN
topic carbon nanotube
electrical conductivity
polyvinylidene fluoride
tensile strength
wet spinning
Organic chemistry
QD241-441
spellingShingle carbon nanotube
electrical conductivity
polyvinylidene fluoride
tensile strength
wet spinning
Organic chemistry
QD241-441
Ki-Weon Kang
Chan-Woong Choi
Ji-Won Jin
A Wet-Spinning Process for Producing Carbon Nanotube/Polyvinylidene Fluoride Fibers Having Highly Consistent Electrical and Mechanical Properties
description Studies of polymer/carbon nanotube (CNT) fibers typically focus on optimizing the overall properties, and the effects of structural variation on these properties are ignored. Thus, we investigated the longitudinal variation in the properties of CNT/polyvinylidene fluoride (CNT/PVDF) fibers prepared by wet spinning a solution of multi-walled nanotubes, PVDF, and dimethylacetamide. To this end, materials for the CNT/PVDF fiber were selected, and a dope solution was prepared using MWNT, PVDF, and dimethylacetamide (DMAc). To consider the process parameters that would affect the performance of the CNT/PVDF fiber during the wet-spinning process using the dope solution, the initial conditions for wet spinning were selected, including bath concentration, bath temperature, drying temperature, and elongation, and the CNT/PVDF fiber was spun under the corresponding conditions. Additionally, three performance stabilization processes were proposed to improve the initial conditions for wet spinning and manufacturing the fiber. Lastly, to confirm the reliability of the CNT/PVDF fiber in all sections, tensile strength, electrical conductivity, and cross-sectional images were analyzed for the 30 m, 60 m, and 90 m sections of the fiber, and the reliability of the wet-spinning process was verified.
format article
author Ki-Weon Kang
Chan-Woong Choi
Ji-Won Jin
author_facet Ki-Weon Kang
Chan-Woong Choi
Ji-Won Jin
author_sort Ki-Weon Kang
title A Wet-Spinning Process for Producing Carbon Nanotube/Polyvinylidene Fluoride Fibers Having Highly Consistent Electrical and Mechanical Properties
title_short A Wet-Spinning Process for Producing Carbon Nanotube/Polyvinylidene Fluoride Fibers Having Highly Consistent Electrical and Mechanical Properties
title_full A Wet-Spinning Process for Producing Carbon Nanotube/Polyvinylidene Fluoride Fibers Having Highly Consistent Electrical and Mechanical Properties
title_fullStr A Wet-Spinning Process for Producing Carbon Nanotube/Polyvinylidene Fluoride Fibers Having Highly Consistent Electrical and Mechanical Properties
title_full_unstemmed A Wet-Spinning Process for Producing Carbon Nanotube/Polyvinylidene Fluoride Fibers Having Highly Consistent Electrical and Mechanical Properties
title_sort wet-spinning process for producing carbon nanotube/polyvinylidene fluoride fibers having highly consistent electrical and mechanical properties
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/4066b1b3f60846debdad25fa8ce656c5
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