Improving Texture and Microstructure Homogeneity in High-Purity Ta Sheets by Warm Cross Rolling and Annealing

The evolution of texture and microstructure uniformity in high-purity tantalum (Ta) sheets during 135° warm cross rolling (WCR) was analyzed in detail. X-ray diffraction suggested that relatively uniform ‘ideal’ deformation texture distribution across the thickness could be obtained from WCR, since...

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Autores principales: Doudou Long, Shifeng Liu, Jialin Zhu, Yahui Liu, Shiyuan Zhou, Xiaoli Yuan, Dmytro Orlov
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Lenguaje:EN
Publicado: MDPI AG 2021
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Acceso en línea:https://doaj.org/article/4dc505bd259d491aa351c294234de486
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spelling oai:doaj.org-article:4dc505bd259d491aa351c294234de4862021-11-25T18:21:03ZImproving Texture and Microstructure Homogeneity in High-Purity Ta Sheets by Warm Cross Rolling and Annealing10.3390/met111116652075-4701https://doaj.org/article/4dc505bd259d491aa351c294234de4862021-10-01T00:00:00Zhttps://www.mdpi.com/2075-4701/11/11/1665https://doaj.org/toc/2075-4701The evolution of texture and microstructure uniformity in high-purity tantalum (Ta) sheets during 135° warm cross rolling (WCR) was analyzed in detail. X-ray diffraction suggested that relatively uniform ‘ideal’ deformation texture distribution across the thickness could be obtained from WCR, since more potential slip systems could be activated. Electron backscatter diffraction (EBSD) results indicated that the change in strain path in warm rolling could enhance dislocations mobility and increase the probability of dislocations rearrangement and annihilation. Thus, the proportion of low-angle grain boundaries was significantly reduced, and more sub-grain boundaries or sub-grains were formed via WCR. The calculation of geometrically necessary dislocation density based on the strain gradient model supports this result. The analysis of relative Schmid factor combined with the strain contouring map indicated that inhomogeneous orientation-dependent grain subdivision could be effectively weakened, and relatively uniform strain distribution could be formed in the WCR sample. Upon annealing, uniform fine grain size and more randomly oriented grains were obtained in the WCR sample after the completion of recrystallization because of relatively uniform grain subdivision and stored energy distribution.Doudou LongShifeng LiuJialin ZhuYahui LiuShiyuan ZhouXiaoli YuanDmytro OrlovMDPI AGarticle135° warm cross rollingdislocation movementgeometrically necessary dislocationschmid factorrecrystallizationMining engineering. MetallurgyTN1-997ENMetals, Vol 11, Iss 1665, p 1665 (2021)
institution DOAJ
collection DOAJ
language EN
topic 135° warm cross rolling
dislocation movement
geometrically necessary dislocation
schmid factor
recrystallization
Mining engineering. Metallurgy
TN1-997
spellingShingle 135° warm cross rolling
dislocation movement
geometrically necessary dislocation
schmid factor
recrystallization
Mining engineering. Metallurgy
TN1-997
Doudou Long
Shifeng Liu
Jialin Zhu
Yahui Liu
Shiyuan Zhou
Xiaoli Yuan
Dmytro Orlov
Improving Texture and Microstructure Homogeneity in High-Purity Ta Sheets by Warm Cross Rolling and Annealing
description The evolution of texture and microstructure uniformity in high-purity tantalum (Ta) sheets during 135° warm cross rolling (WCR) was analyzed in detail. X-ray diffraction suggested that relatively uniform ‘ideal’ deformation texture distribution across the thickness could be obtained from WCR, since more potential slip systems could be activated. Electron backscatter diffraction (EBSD) results indicated that the change in strain path in warm rolling could enhance dislocations mobility and increase the probability of dislocations rearrangement and annihilation. Thus, the proportion of low-angle grain boundaries was significantly reduced, and more sub-grain boundaries or sub-grains were formed via WCR. The calculation of geometrically necessary dislocation density based on the strain gradient model supports this result. The analysis of relative Schmid factor combined with the strain contouring map indicated that inhomogeneous orientation-dependent grain subdivision could be effectively weakened, and relatively uniform strain distribution could be formed in the WCR sample. Upon annealing, uniform fine grain size and more randomly oriented grains were obtained in the WCR sample after the completion of recrystallization because of relatively uniform grain subdivision and stored energy distribution.
format article
author Doudou Long
Shifeng Liu
Jialin Zhu
Yahui Liu
Shiyuan Zhou
Xiaoli Yuan
Dmytro Orlov
author_facet Doudou Long
Shifeng Liu
Jialin Zhu
Yahui Liu
Shiyuan Zhou
Xiaoli Yuan
Dmytro Orlov
author_sort Doudou Long
title Improving Texture and Microstructure Homogeneity in High-Purity Ta Sheets by Warm Cross Rolling and Annealing
title_short Improving Texture and Microstructure Homogeneity in High-Purity Ta Sheets by Warm Cross Rolling and Annealing
title_full Improving Texture and Microstructure Homogeneity in High-Purity Ta Sheets by Warm Cross Rolling and Annealing
title_fullStr Improving Texture and Microstructure Homogeneity in High-Purity Ta Sheets by Warm Cross Rolling and Annealing
title_full_unstemmed Improving Texture and Microstructure Homogeneity in High-Purity Ta Sheets by Warm Cross Rolling and Annealing
title_sort improving texture and microstructure homogeneity in high-purity ta sheets by warm cross rolling and annealing
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/4dc505bd259d491aa351c294234de486
work_keys_str_mv AT doudoulong improvingtextureandmicrostructurehomogeneityinhighpuritytasheetsbywarmcrossrollingandannealing
AT shifengliu improvingtextureandmicrostructurehomogeneityinhighpuritytasheetsbywarmcrossrollingandannealing
AT jialinzhu improvingtextureandmicrostructurehomogeneityinhighpuritytasheetsbywarmcrossrollingandannealing
AT yahuiliu improvingtextureandmicrostructurehomogeneityinhighpuritytasheetsbywarmcrossrollingandannealing
AT shiyuanzhou improvingtextureandmicrostructurehomogeneityinhighpuritytasheetsbywarmcrossrollingandannealing
AT xiaoliyuan improvingtextureandmicrostructurehomogeneityinhighpuritytasheetsbywarmcrossrollingandannealing
AT dmytroorlov improvingtextureandmicrostructurehomogeneityinhighpuritytasheetsbywarmcrossrollingandannealing
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