VISCOMETRY OF NANODISPERSE MAGNETIC LIQUIDS AND LUBRICATING OILS. 2. METROLOGICAL ANALYSIS OF A DEVICE FOR RHEOLOGICAL STUDIES OF MAGNETIC NANODISPERSE LIQUID MEDIA

An analysis is carried out of the main sources of methodological errors of the magnetic rotary viscometer. The analysis allowed to improve design and to eliminate critical modes of the research. Theoretical evaluations of the systematic error of the device showed that the value of the relative measu...

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Autores principales: A.N. Bolotov, O.O. Novikova, V.V. Meshkov
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Lenguaje:RU
Publicado: Tver State University 2021
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spelling oai:doaj.org-article:4f70516b2aa14bc996143d63c492efb52021-12-03T08:31:54ZVISCOMETRY OF NANODISPERSE MAGNETIC LIQUIDS AND LUBRICATING OILS. 2. METROLOGICAL ANALYSIS OF A DEVICE FOR RHEOLOGICAL STUDIES OF MAGNETIC NANODISPERSE LIQUID MEDIA10.26456/pcascnn/2021.13.0562226-44422658-4360https://doaj.org/article/4f70516b2aa14bc996143d63c492efb52021-12-01T00:00:00Zhttps://physchemaspects.ru/2021/doi-10-26456-pcascnn-2021-13-056/?lang=enhttps://doaj.org/toc/2226-4442https://doaj.org/toc/2658-4360An analysis is carried out of the main sources of methodological errors of the magnetic rotary viscometer. The analysis allowed to improve design and to eliminate critical modes of the research. Theoretical evaluations of the systematic error of the device showed that the value of the relative measurement error can be brought to a value of less than 1%. The greatest contribution to the systematic error of the device is made by the instability of the temperature regime of the nanofluid under study and by the inaccuracy of determining the height of the liquid layer in contact with the measuring cylinder. The measurement of the viscosity of the reference liquids on the magnetic viscometer showed that experimental values are slightly, by about 0.9% overestimated. Calibration of the device on various reference liquids allowed reducing the total measurement error down to tenths of a percent. The magnetic rotary viscometer can be used in non-standard scientific studies of the structure and rheological characteristics of nanofluids, for operational control of the processes of synthesis of magnetic liquids and certification of magnetic nanofluids intended for technical use.A.N. BolotovO.O. NovikovaV.V. MeshkovTver State Universityarticlemagnetic nanofluidrheologyviscometershear stressshear ratePhysical and theoretical chemistryQD450-801RUФизико-химические аспекты изучения кластеров, наноструктур и наноматериалов, Iss 13, Pp 56-64 (2021)
institution DOAJ
collection DOAJ
language RU
topic magnetic nanofluid
rheology
viscometer
shear stress
shear rate
Physical and theoretical chemistry
QD450-801
spellingShingle magnetic nanofluid
rheology
viscometer
shear stress
shear rate
Physical and theoretical chemistry
QD450-801
A.N. Bolotov
O.O. Novikova
V.V. Meshkov
VISCOMETRY OF NANODISPERSE MAGNETIC LIQUIDS AND LUBRICATING OILS. 2. METROLOGICAL ANALYSIS OF A DEVICE FOR RHEOLOGICAL STUDIES OF MAGNETIC NANODISPERSE LIQUID MEDIA
description An analysis is carried out of the main sources of methodological errors of the magnetic rotary viscometer. The analysis allowed to improve design and to eliminate critical modes of the research. Theoretical evaluations of the systematic error of the device showed that the value of the relative measurement error can be brought to a value of less than 1%. The greatest contribution to the systematic error of the device is made by the instability of the temperature regime of the nanofluid under study and by the inaccuracy of determining the height of the liquid layer in contact with the measuring cylinder. The measurement of the viscosity of the reference liquids on the magnetic viscometer showed that experimental values are slightly, by about 0.9% overestimated. Calibration of the device on various reference liquids allowed reducing the total measurement error down to tenths of a percent. The magnetic rotary viscometer can be used in non-standard scientific studies of the structure and rheological characteristics of nanofluids, for operational control of the processes of synthesis of magnetic liquids and certification of magnetic nanofluids intended for technical use.
format article
author A.N. Bolotov
O.O. Novikova
V.V. Meshkov
author_facet A.N. Bolotov
O.O. Novikova
V.V. Meshkov
author_sort A.N. Bolotov
title VISCOMETRY OF NANODISPERSE MAGNETIC LIQUIDS AND LUBRICATING OILS. 2. METROLOGICAL ANALYSIS OF A DEVICE FOR RHEOLOGICAL STUDIES OF MAGNETIC NANODISPERSE LIQUID MEDIA
title_short VISCOMETRY OF NANODISPERSE MAGNETIC LIQUIDS AND LUBRICATING OILS. 2. METROLOGICAL ANALYSIS OF A DEVICE FOR RHEOLOGICAL STUDIES OF MAGNETIC NANODISPERSE LIQUID MEDIA
title_full VISCOMETRY OF NANODISPERSE MAGNETIC LIQUIDS AND LUBRICATING OILS. 2. METROLOGICAL ANALYSIS OF A DEVICE FOR RHEOLOGICAL STUDIES OF MAGNETIC NANODISPERSE LIQUID MEDIA
title_fullStr VISCOMETRY OF NANODISPERSE MAGNETIC LIQUIDS AND LUBRICATING OILS. 2. METROLOGICAL ANALYSIS OF A DEVICE FOR RHEOLOGICAL STUDIES OF MAGNETIC NANODISPERSE LIQUID MEDIA
title_full_unstemmed VISCOMETRY OF NANODISPERSE MAGNETIC LIQUIDS AND LUBRICATING OILS. 2. METROLOGICAL ANALYSIS OF A DEVICE FOR RHEOLOGICAL STUDIES OF MAGNETIC NANODISPERSE LIQUID MEDIA
title_sort viscometry of nanodisperse magnetic liquids and lubricating oils. 2. metrological analysis of a device for rheological studies of magnetic nanodisperse liquid media
publisher Tver State University
publishDate 2021
url https://doaj.org/article/4f70516b2aa14bc996143d63c492efb5
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