Extraction of Sodium Alginate from Sargassum sp. using Microwave-Assisted Extraction (MAE)

The method used in alginate extraction has been using conventional heating. Lately, Microwave-Assisted Extraction (MAE) has been widely used to extract active compounds from natural ingredients. This study aims to extract sodium alginate from Sargassum sp. using MAE method. This research was conduct...

Descripción completa

Guardado en:
Detalles Bibliográficos
Autores principales: Ruslan Ruslan, Amran Amir, Agrippina Wiraningtyas
Formato: article
Lenguaje:EN
Publicado: University of Brawijaya 2019
Materias:
Acceso en línea:http://dx.doi.org/10.21776/ub.jpacr.2019.008.01.420
https://doaj.org/article/4fc467a8c2234cd282871f61059fa32b
Etiquetas: Agregar Etiqueta
Sin Etiquetas, Sea el primero en etiquetar este registro!
id oai:doaj.org-article:4fc467a8c2234cd282871f61059fa32b
record_format dspace
spelling oai:doaj.org-article:4fc467a8c2234cd282871f61059fa32b2021-12-02T13:13:59ZExtraction of Sodium Alginate from Sargassum sp. using Microwave-Assisted Extraction (MAE)http://dx.doi.org/10.21776/ub.jpacr.2019.008.01.4202302-46902302-4690https://doaj.org/article/4fc467a8c2234cd282871f61059fa32b2019-01-01T00:00:00Zhttps://jpacr.ub.ac.id/index.php/jpacr/article/view/420/pdfhttps://doaj.org/toc/2302-4690https://doaj.org/toc/2302-4690The method used in alginate extraction has been using conventional heating. Lately, Microwave-Assisted Extraction (MAE) has been widely used to extract active compounds from natural ingredients. This study aims to extract sodium alginate from Sargassum sp. using MAE method. This research was conducted by determining the optimum power level and extraction time using a commercial microwave. Power level optimization is carried out at level 70; 80; 90 and 100, while extraction time is carried out for 15; 16; 17 and 18 minutes. The results showed that sodium alginate products were obtained at levels 70, 80, 90 and 100, respectively 0.5%; 37.13%; 23.36% and 1.2%. While sodium alginate products are obtained at variations in extraction time for 15; 16; 17 and 18 minutes were obtained respectively 27.4%; 37.13%; 26.1% and 25.76%. The characterization of sodium alginate products was carried out by analysis of water content, ash content, brightness, and viscosity in the sequence obtained by 14.43%; 14.63%; 78.62 and 95.00 cps. The results of the analysis of heavy metal content obtained that the product of sodium alginate extracted did not contain metal Pb and Hg. FTIR spectra results showed the presence of hydroxyl (-OH) functional groups at wave numbers 3448.7 cm-1 and 1620.21 cm-1; C-H bond at 2931.8 cm-1; alkene group at 2337.7 cm-1; sodium (Na) bond at 1419.61 cm-1; carbonyl group at 1095.57 cm-1 and carboxylic and ketone groups at 1033.85 cm-1. Based on the results of the characterization proving that the product obtained is a sodium alginate compound.Ruslan RuslanAmran AmirAgrippina WiraningtyasUniversity of Brawijayaarticlesodium alginatephysicochemical propertiesmae methodChemistryQD1-999ENJournal of Pure and Applied Chemistry Research, Vol 8, Iss 1, Pp 23-30 (2019)
institution DOAJ
collection DOAJ
language EN
topic sodium alginate
physicochemical properties
mae method
Chemistry
QD1-999
spellingShingle sodium alginate
physicochemical properties
mae method
Chemistry
QD1-999
Ruslan Ruslan
Amran Amir
Agrippina Wiraningtyas
Extraction of Sodium Alginate from Sargassum sp. using Microwave-Assisted Extraction (MAE)
description The method used in alginate extraction has been using conventional heating. Lately, Microwave-Assisted Extraction (MAE) has been widely used to extract active compounds from natural ingredients. This study aims to extract sodium alginate from Sargassum sp. using MAE method. This research was conducted by determining the optimum power level and extraction time using a commercial microwave. Power level optimization is carried out at level 70; 80; 90 and 100, while extraction time is carried out for 15; 16; 17 and 18 minutes. The results showed that sodium alginate products were obtained at levels 70, 80, 90 and 100, respectively 0.5%; 37.13%; 23.36% and 1.2%. While sodium alginate products are obtained at variations in extraction time for 15; 16; 17 and 18 minutes were obtained respectively 27.4%; 37.13%; 26.1% and 25.76%. The characterization of sodium alginate products was carried out by analysis of water content, ash content, brightness, and viscosity in the sequence obtained by 14.43%; 14.63%; 78.62 and 95.00 cps. The results of the analysis of heavy metal content obtained that the product of sodium alginate extracted did not contain metal Pb and Hg. FTIR spectra results showed the presence of hydroxyl (-OH) functional groups at wave numbers 3448.7 cm-1 and 1620.21 cm-1; C-H bond at 2931.8 cm-1; alkene group at 2337.7 cm-1; sodium (Na) bond at 1419.61 cm-1; carbonyl group at 1095.57 cm-1 and carboxylic and ketone groups at 1033.85 cm-1. Based on the results of the characterization proving that the product obtained is a sodium alginate compound.
format article
author Ruslan Ruslan
Amran Amir
Agrippina Wiraningtyas
author_facet Ruslan Ruslan
Amran Amir
Agrippina Wiraningtyas
author_sort Ruslan Ruslan
title Extraction of Sodium Alginate from Sargassum sp. using Microwave-Assisted Extraction (MAE)
title_short Extraction of Sodium Alginate from Sargassum sp. using Microwave-Assisted Extraction (MAE)
title_full Extraction of Sodium Alginate from Sargassum sp. using Microwave-Assisted Extraction (MAE)
title_fullStr Extraction of Sodium Alginate from Sargassum sp. using Microwave-Assisted Extraction (MAE)
title_full_unstemmed Extraction of Sodium Alginate from Sargassum sp. using Microwave-Assisted Extraction (MAE)
title_sort extraction of sodium alginate from sargassum sp. using microwave-assisted extraction (mae)
publisher University of Brawijaya
publishDate 2019
url http://dx.doi.org/10.21776/ub.jpacr.2019.008.01.420
https://doaj.org/article/4fc467a8c2234cd282871f61059fa32b
work_keys_str_mv AT ruslanruslan extractionofsodiumalginatefromsargassumspusingmicrowaveassistedextractionmae
AT amranamir extractionofsodiumalginatefromsargassumspusingmicrowaveassistedextractionmae
AT agrippinawiraningtyas extractionofsodiumalginatefromsargassumspusingmicrowaveassistedextractionmae
_version_ 1718393384527200256