Extraction and Physicochemical Properties of Refined Kappa-Carrageenan from Kappaphycus alvarezii Originated from Semporna, Sabah

In this research, the influence of different solvents (1.0 M KOH and 1.0 M NaOH) and different drying methods (freeze dryer and oven) towards the chemical and physical properties of refined carrageenan by using kappaphycus alvarezii collected from Semporna, Sabah were determined. The physical charac...

Descripción completa

Guardado en:
Detalles Bibliográficos
Autores principales: Adnin Awalludin, Nazirah Mingu, Abu Zahrim Yaser, Hasmadi Mamat, Khairul Azfar Kamaruzaman, Zuhair Jamain, Md Lutfor Rahman, Mohd Hafiz Abd Majid, Mohd Sani Sarjadi
Formato: article
Lenguaje:EN
Publicado: Tamkang University Press 2021
Materias:
Acceso en línea:https://doaj.org/article/57d7c69877cf4326869a158477187065
Etiquetas: Agregar Etiqueta
Sin Etiquetas, Sea el primero en etiquetar este registro!
id oai:doaj.org-article:57d7c69877cf4326869a158477187065
record_format dspace
spelling oai:doaj.org-article:57d7c69877cf4326869a1584771870652021-11-24T14:36:44ZExtraction and Physicochemical Properties of Refined Kappa-Carrageenan from Kappaphycus alvarezii Originated from Semporna, Sabah10.6180/jase.202206_25(3).00062708-99672708-9975https://doaj.org/article/57d7c69877cf4326869a1584771870652021-11-01T00:00:00Zhttp://jase.tku.edu.tw/articles/jase-202206-25-3-0006https://doaj.org/toc/2708-9967https://doaj.org/toc/2708-9975In this research, the influence of different solvents (1.0 M KOH and 1.0 M NaOH) and different drying methods (freeze dryer and oven) towards the chemical and physical properties of refined carrageenan by using kappaphycus alvarezii collected from Semporna, Sabah were determined. The physical characterizations involved were viscosity, surface morphology and functional group while, the chemical characterization was sulphate content. The result showed that the carrageenan yield were 12% (carrageenan extracted using 1.0 M KOH) and 18% (carrageenan extracted using 1.0 M NaOH) respectively for oven as a drying method. The carrageenan yield using freeze dryer was 10% (carrageenan extracted using 1.0 M KOH) and 12% (carrageenan extracted using 1.0 M NaOH). The functional groups identification for sulphate ester, anhydro-galactose and galactose were analyzed by using FT-IR. The surface morphology of carrageenan was analyzed by using SEM for different drying method and carrageenan extracted using 1.0 M KOH (Oven as drying method) showed a smooth surface compared with other samples. The sulphate content was analyzed by using UV-Vis spectrophotometer. The concentration of sulphate were 22.5 mg/L (carrageenan extracted using 1.0 M KOH) and 69.4mg/L (carrageenan extracted using 1.0 M NaOH) for oven as drying method. The result for freeze dryer method were 33.8 mg/L (carrageenan extracted using KOH) and 44.9 mg/L (carrageenan extracted using NaOH), respectively.: Adnin AwalludinNazirah MinguAbu Zahrim YaserHasmadi MamatKhairul Azfar KamaruzamanZuhair JamainMd Lutfor RahmanMohd Hafiz Abd MajidMohd Sani SarjadiTamkang University Pressarticleextractionrefined kappa-carrageenankappaphycus alvareziiEngineering (General). Civil engineering (General)TA1-2040Chemical engineeringTP155-156PhysicsQC1-999ENJournal of Applied Science and Engineering, Vol 25, Iss 3, Pp 411-416 (2021)
institution DOAJ
collection DOAJ
language EN
topic extraction
refined kappa-carrageenan
kappaphycus alvarezii
Engineering (General). Civil engineering (General)
TA1-2040
Chemical engineering
TP155-156
Physics
QC1-999
spellingShingle extraction
refined kappa-carrageenan
kappaphycus alvarezii
Engineering (General). Civil engineering (General)
TA1-2040
Chemical engineering
TP155-156
Physics
QC1-999
Adnin Awalludin
Nazirah Mingu
Abu Zahrim Yaser
Hasmadi Mamat
Khairul Azfar Kamaruzaman
Zuhair Jamain
Md Lutfor Rahman
Mohd Hafiz Abd Majid
Mohd Sani Sarjadi
Extraction and Physicochemical Properties of Refined Kappa-Carrageenan from Kappaphycus alvarezii Originated from Semporna, Sabah
description In this research, the influence of different solvents (1.0 M KOH and 1.0 M NaOH) and different drying methods (freeze dryer and oven) towards the chemical and physical properties of refined carrageenan by using kappaphycus alvarezii collected from Semporna, Sabah were determined. The physical characterizations involved were viscosity, surface morphology and functional group while, the chemical characterization was sulphate content. The result showed that the carrageenan yield were 12% (carrageenan extracted using 1.0 M KOH) and 18% (carrageenan extracted using 1.0 M NaOH) respectively for oven as a drying method. The carrageenan yield using freeze dryer was 10% (carrageenan extracted using 1.0 M KOH) and 12% (carrageenan extracted using 1.0 M NaOH). The functional groups identification for sulphate ester, anhydro-galactose and galactose were analyzed by using FT-IR. The surface morphology of carrageenan was analyzed by using SEM for different drying method and carrageenan extracted using 1.0 M KOH (Oven as drying method) showed a smooth surface compared with other samples. The sulphate content was analyzed by using UV-Vis spectrophotometer. The concentration of sulphate were 22.5 mg/L (carrageenan extracted using 1.0 M KOH) and 69.4mg/L (carrageenan extracted using 1.0 M NaOH) for oven as drying method. The result for freeze dryer method were 33.8 mg/L (carrageenan extracted using KOH) and 44.9 mg/L (carrageenan extracted using NaOH), respectively.:
format article
author Adnin Awalludin
Nazirah Mingu
Abu Zahrim Yaser
Hasmadi Mamat
Khairul Azfar Kamaruzaman
Zuhair Jamain
Md Lutfor Rahman
Mohd Hafiz Abd Majid
Mohd Sani Sarjadi
author_facet Adnin Awalludin
Nazirah Mingu
Abu Zahrim Yaser
Hasmadi Mamat
Khairul Azfar Kamaruzaman
Zuhair Jamain
Md Lutfor Rahman
Mohd Hafiz Abd Majid
Mohd Sani Sarjadi
author_sort Adnin Awalludin
title Extraction and Physicochemical Properties of Refined Kappa-Carrageenan from Kappaphycus alvarezii Originated from Semporna, Sabah
title_short Extraction and Physicochemical Properties of Refined Kappa-Carrageenan from Kappaphycus alvarezii Originated from Semporna, Sabah
title_full Extraction and Physicochemical Properties of Refined Kappa-Carrageenan from Kappaphycus alvarezii Originated from Semporna, Sabah
title_fullStr Extraction and Physicochemical Properties of Refined Kappa-Carrageenan from Kappaphycus alvarezii Originated from Semporna, Sabah
title_full_unstemmed Extraction and Physicochemical Properties of Refined Kappa-Carrageenan from Kappaphycus alvarezii Originated from Semporna, Sabah
title_sort extraction and physicochemical properties of refined kappa-carrageenan from kappaphycus alvarezii originated from semporna, sabah
publisher Tamkang University Press
publishDate 2021
url https://doaj.org/article/57d7c69877cf4326869a158477187065
work_keys_str_mv AT adninawalludin extractionandphysicochemicalpropertiesofrefinedkappacarrageenanfromkappaphycusalvareziioriginatedfromsempornasabah
AT nazirahmingu extractionandphysicochemicalpropertiesofrefinedkappacarrageenanfromkappaphycusalvareziioriginatedfromsempornasabah
AT abuzahrimyaser extractionandphysicochemicalpropertiesofrefinedkappacarrageenanfromkappaphycusalvareziioriginatedfromsempornasabah
AT hasmadimamat extractionandphysicochemicalpropertiesofrefinedkappacarrageenanfromkappaphycusalvareziioriginatedfromsempornasabah
AT khairulazfarkamaruzaman extractionandphysicochemicalpropertiesofrefinedkappacarrageenanfromkappaphycusalvareziioriginatedfromsempornasabah
AT zuhairjamain extractionandphysicochemicalpropertiesofrefinedkappacarrageenanfromkappaphycusalvareziioriginatedfromsempornasabah
AT mdlutforrahman extractionandphysicochemicalpropertiesofrefinedkappacarrageenanfromkappaphycusalvareziioriginatedfromsempornasabah
AT mohdhafizabdmajid extractionandphysicochemicalpropertiesofrefinedkappacarrageenanfromkappaphycusalvareziioriginatedfromsempornasabah
AT mohdsanisarjadi extractionandphysicochemicalpropertiesofrefinedkappacarrageenanfromkappaphycusalvareziioriginatedfromsempornasabah
_version_ 1718414990088601600