The Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt

Three-layer Aurivillius compound bismuth titanate (Bi4Ti3O12) is well known for having interesting properties such as ferroelectric and photocatalyst. Many researchers reported that the unique plate-like shaped particle affecting ferroelectric and photocatalyst properties. The molten salt synthesis...

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Autores principales: Sheley Marela, Nur Aini, Arie Hardian, Veinardi Suendo, Anton Prasetyo
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Lenguaje:EN
Publicado: University of Brawijaya 2021
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Acceso en línea:https://doaj.org/article/645f1348e63e43a8aaef4406daf71082
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spelling oai:doaj.org-article:645f1348e63e43a8aaef4406daf710822021-11-24T11:50:36ZThe Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt2302-46902541-0733https://doaj.org/article/645f1348e63e43a8aaef4406daf710822021-04-01T00:00:00Zhttps://jpacr.ub.ac.id/index.php/jpacr/article/view/570/pdfhttps://doaj.org/toc/2302-4690https://doaj.org/toc/2541-0733Three-layer Aurivillius compound bismuth titanate (Bi4Ti3O12) is well known for having interesting properties such as ferroelectric and photocatalyst. Many researchers reported that the unique plate-like shaped particle affecting ferroelectric and photocatalyst properties. The molten salt synthesis is the common simple method to obtain that unique morphology. In this research, Bi4Ti3O12 was synthesized using single molten salt NaCl at various temperatures, which is 800, 850, 900, and 950 oC. X-Ray Diffraction data showed that all obtained Bi4Ti3O12 have a B2cb space group with no impurities detected. The Raman spectra shows the characteristic vibration modes of Bi4Ti3O12 at 62, 117, 228, 269, 332, 364, 536, 851 cm-1. The plate-like shaped particle was confirmed by SEM analysis. Based on SEM images, the size of the particle increased along with the synthesis temperature, which is due to the thermal effect on grain growth.Sheley MarelaNur AiniArie HardianVeinardi SuendoAnton PrasetyoUniversity of Brawijayaarticlebismuth titanatetemperature synthesismolten salt synthesisplate-like shaped particleChemistryQD1-999ENJournal of Pure and Applied Chemistry Research, Vol 10, Iss 1, Pp 64-71 (2021)
institution DOAJ
collection DOAJ
language EN
topic bismuth titanate
temperature synthesis
molten salt synthesis
plate-like shaped particle
Chemistry
QD1-999
spellingShingle bismuth titanate
temperature synthesis
molten salt synthesis
plate-like shaped particle
Chemistry
QD1-999
Sheley Marela
Nur Aini
Arie Hardian
Veinardi Suendo
Anton Prasetyo
The Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt
description Three-layer Aurivillius compound bismuth titanate (Bi4Ti3O12) is well known for having interesting properties such as ferroelectric and photocatalyst. Many researchers reported that the unique plate-like shaped particle affecting ferroelectric and photocatalyst properties. The molten salt synthesis is the common simple method to obtain that unique morphology. In this research, Bi4Ti3O12 was synthesized using single molten salt NaCl at various temperatures, which is 800, 850, 900, and 950 oC. X-Ray Diffraction data showed that all obtained Bi4Ti3O12 have a B2cb space group with no impurities detected. The Raman spectra shows the characteristic vibration modes of Bi4Ti3O12 at 62, 117, 228, 269, 332, 364, 536, 851 cm-1. The plate-like shaped particle was confirmed by SEM analysis. Based on SEM images, the size of the particle increased along with the synthesis temperature, which is due to the thermal effect on grain growth.
format article
author Sheley Marela
Nur Aini
Arie Hardian
Veinardi Suendo
Anton Prasetyo
author_facet Sheley Marela
Nur Aini
Arie Hardian
Veinardi Suendo
Anton Prasetyo
author_sort Sheley Marela
title The Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt
title_short The Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt
title_full The Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt
title_fullStr The Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt
title_full_unstemmed The Effect of Temperature Synthesis on the Plate-Like Particle of Bi4Ti3O12 Obtained by Single Molten NaCl Salt
title_sort effect of temperature synthesis on the plate-like particle of bi4ti3o12 obtained by single molten nacl salt
publisher University of Brawijaya
publishDate 2021
url https://doaj.org/article/645f1348e63e43a8aaef4406daf71082
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