Titanium-Enriched Slag Prepared by Atmospheric Hydrochloric Acid Leaching of Mechanically Activated Vanadium Titanomagnetite Concentrates

The titanium-enriched slag was obtained via atmospheric hydrochloric acid leaching of mechanically activated vanadium titanomagnetite concentrates (VTMCs). Under the influence of mechanical activation, specific physicochemical changes were observed via X-ray diffractometry, scanning electron microsc...

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Autores principales: En-Hui Wu, Yin-He Lin, Jun Liu, Zhe Wang, Jin-Chuan Liu, Guo-Liang Yin, Jing-Wei Li, Xiang-Kui Cheng, Yu-Long Jia
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spelling oai:doaj.org-article:64e26017bafd49f382361fd8af8662242021-11-25T18:13:09ZTitanium-Enriched Slag Prepared by Atmospheric Hydrochloric Acid Leaching of Mechanically Activated Vanadium Titanomagnetite Concentrates10.3390/ma142267361996-1944https://doaj.org/article/64e26017bafd49f382361fd8af8662242021-11-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/22/6736https://doaj.org/toc/1996-1944The titanium-enriched slag was obtained via atmospheric hydrochloric acid leaching of mechanically activated vanadium titanomagnetite concentrates (VTMCs). Under the influence of mechanical activation, specific physicochemical changes were observed via X-ray diffractometry, scanning electron microscopy, and granulometric laser diffraction analysis. Experimental findings revealed that the mechanical activation of VTMCs resulted in a decrease in the median volume particle diameter (d50) and an increase in the specific surface area (SA) with an increased milling time. The results of the leaching experiment revealed that the mechanical activation treatment favors the extraction of iron (Fe) and titanium dioxide (TiO<sub>2</sub>) from the VTMCs. The Fe and TiO<sub>2</sub> extractions from the mechanically activated sample after 10 h compared with the unactivated sample were increased by 12.82% and 4.73%, respectively. The presence of the ilmenite phase in the titanium-enriched slag was confirmed by X-ray diffractometry and EDS patterns, and the content of the TiO<sub>2</sub> in the enriched slag can get as high as 43.75%.En-Hui WuYin-He LinJun LiuZhe WangJin-Chuan LiuGuo-Liang YinJing-Wei LiXiang-Kui ChengYu-Long JiaMDPI AGarticlevanadium titanomagnetite concentratesmechanical activationhydrochloric acid Leachingtitanium-enriched slagTiO<sub>2</sub> extractionTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6736, p 6736 (2021)
institution DOAJ
collection DOAJ
language EN
topic vanadium titanomagnetite concentrates
mechanical activation
hydrochloric acid Leaching
titanium-enriched slag
TiO<sub>2</sub> extraction
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
spellingShingle vanadium titanomagnetite concentrates
mechanical activation
hydrochloric acid Leaching
titanium-enriched slag
TiO<sub>2</sub> extraction
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
En-Hui Wu
Yin-He Lin
Jun Liu
Zhe Wang
Jin-Chuan Liu
Guo-Liang Yin
Jing-Wei Li
Xiang-Kui Cheng
Yu-Long Jia
Titanium-Enriched Slag Prepared by Atmospheric Hydrochloric Acid Leaching of Mechanically Activated Vanadium Titanomagnetite Concentrates
description The titanium-enriched slag was obtained via atmospheric hydrochloric acid leaching of mechanically activated vanadium titanomagnetite concentrates (VTMCs). Under the influence of mechanical activation, specific physicochemical changes were observed via X-ray diffractometry, scanning electron microscopy, and granulometric laser diffraction analysis. Experimental findings revealed that the mechanical activation of VTMCs resulted in a decrease in the median volume particle diameter (d50) and an increase in the specific surface area (SA) with an increased milling time. The results of the leaching experiment revealed that the mechanical activation treatment favors the extraction of iron (Fe) and titanium dioxide (TiO<sub>2</sub>) from the VTMCs. The Fe and TiO<sub>2</sub> extractions from the mechanically activated sample after 10 h compared with the unactivated sample were increased by 12.82% and 4.73%, respectively. The presence of the ilmenite phase in the titanium-enriched slag was confirmed by X-ray diffractometry and EDS patterns, and the content of the TiO<sub>2</sub> in the enriched slag can get as high as 43.75%.
format article
author En-Hui Wu
Yin-He Lin
Jun Liu
Zhe Wang
Jin-Chuan Liu
Guo-Liang Yin
Jing-Wei Li
Xiang-Kui Cheng
Yu-Long Jia
author_facet En-Hui Wu
Yin-He Lin
Jun Liu
Zhe Wang
Jin-Chuan Liu
Guo-Liang Yin
Jing-Wei Li
Xiang-Kui Cheng
Yu-Long Jia
author_sort En-Hui Wu
title Titanium-Enriched Slag Prepared by Atmospheric Hydrochloric Acid Leaching of Mechanically Activated Vanadium Titanomagnetite Concentrates
title_short Titanium-Enriched Slag Prepared by Atmospheric Hydrochloric Acid Leaching of Mechanically Activated Vanadium Titanomagnetite Concentrates
title_full Titanium-Enriched Slag Prepared by Atmospheric Hydrochloric Acid Leaching of Mechanically Activated Vanadium Titanomagnetite Concentrates
title_fullStr Titanium-Enriched Slag Prepared by Atmospheric Hydrochloric Acid Leaching of Mechanically Activated Vanadium Titanomagnetite Concentrates
title_full_unstemmed Titanium-Enriched Slag Prepared by Atmospheric Hydrochloric Acid Leaching of Mechanically Activated Vanadium Titanomagnetite Concentrates
title_sort titanium-enriched slag prepared by atmospheric hydrochloric acid leaching of mechanically activated vanadium titanomagnetite concentrates
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/64e26017bafd49f382361fd8af866224
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