Microstructure and Mechanical Properties of Vacuum Diffusion Bonded Zr-4 Alloy Joint

The development of welding technology for zirconium alloy has great significance on the safety, stability, and reliability of the operation of the nuclear reactor. In this work, vacuum diffusion bonding of Zr-4 alloy was studied at the diffusion temperature ranging from 760 to 820 °C with holding ti...

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Autores principales: Zeming Wang, Xu Yang, Jing Wang, Zhonglin Xiao, Fugong Qi, Kongbo Sun, Ying Wang, Zhenwen Yang
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Lenguaje:EN
Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:657561e0fd604f46a95f80f66609b81f2021-11-25T17:19:46ZMicrostructure and Mechanical Properties of Vacuum Diffusion Bonded Zr-4 Alloy Joint10.3390/cryst111114372073-4352https://doaj.org/article/657561e0fd604f46a95f80f66609b81f2021-11-01T00:00:00Zhttps://www.mdpi.com/2073-4352/11/11/1437https://doaj.org/toc/2073-4352The development of welding technology for zirconium alloy has great significance on the safety, stability, and reliability of the operation of the nuclear reactor. In this work, vacuum diffusion bonding of Zr-4 alloy was studied at the diffusion temperature ranging from 760 to 820 °C with holding times of 30–90 min. The effects of diffusion bonding temperature and holding time on the interfacial microstructure and mechanical properties of the diffusion bonded Zr-4 alloy joints were investigated in detail, and the relationship between the interfacial microstructure and shear strength of the diffusion bonded joints was discussed. The results show that the interface bonding ratio of the diffusion bonded Zr-4 joint gradually increased from 74% to 95% with the increasing of bonding temperature. In addition, the grain size of the base material became a larger and brittle second phase composed of Zr(Cr, Fe)<sub>2</sub> and eutectic α-Zr + Zr(Fe, Cr)<sub>2</sub> formed in the joint with the increase of the temperature as well as the extension of the bonding time. The highest shear strength of 349 MPa was obtained at 800 °C for 30 min under 7 MPa, and the crack of the joint was primarily propagated along with the base material rather than the bonded interface.Zeming WangXu YangJing WangZhonglin XiaoFugong QiKongbo SunYing WangZhenwen YangMDPI AGarticleZr-4 alloydiffusion bondingshear strengthinterfacial microstructureCrystallographyQD901-999ENCrystals, Vol 11, Iss 1437, p 1437 (2021)
institution DOAJ
collection DOAJ
language EN
topic Zr-4 alloy
diffusion bonding
shear strength
interfacial microstructure
Crystallography
QD901-999
spellingShingle Zr-4 alloy
diffusion bonding
shear strength
interfacial microstructure
Crystallography
QD901-999
Zeming Wang
Xu Yang
Jing Wang
Zhonglin Xiao
Fugong Qi
Kongbo Sun
Ying Wang
Zhenwen Yang
Microstructure and Mechanical Properties of Vacuum Diffusion Bonded Zr-4 Alloy Joint
description The development of welding technology for zirconium alloy has great significance on the safety, stability, and reliability of the operation of the nuclear reactor. In this work, vacuum diffusion bonding of Zr-4 alloy was studied at the diffusion temperature ranging from 760 to 820 °C with holding times of 30–90 min. The effects of diffusion bonding temperature and holding time on the interfacial microstructure and mechanical properties of the diffusion bonded Zr-4 alloy joints were investigated in detail, and the relationship between the interfacial microstructure and shear strength of the diffusion bonded joints was discussed. The results show that the interface bonding ratio of the diffusion bonded Zr-4 joint gradually increased from 74% to 95% with the increasing of bonding temperature. In addition, the grain size of the base material became a larger and brittle second phase composed of Zr(Cr, Fe)<sub>2</sub> and eutectic α-Zr + Zr(Fe, Cr)<sub>2</sub> formed in the joint with the increase of the temperature as well as the extension of the bonding time. The highest shear strength of 349 MPa was obtained at 800 °C for 30 min under 7 MPa, and the crack of the joint was primarily propagated along with the base material rather than the bonded interface.
format article
author Zeming Wang
Xu Yang
Jing Wang
Zhonglin Xiao
Fugong Qi
Kongbo Sun
Ying Wang
Zhenwen Yang
author_facet Zeming Wang
Xu Yang
Jing Wang
Zhonglin Xiao
Fugong Qi
Kongbo Sun
Ying Wang
Zhenwen Yang
author_sort Zeming Wang
title Microstructure and Mechanical Properties of Vacuum Diffusion Bonded Zr-4 Alloy Joint
title_short Microstructure and Mechanical Properties of Vacuum Diffusion Bonded Zr-4 Alloy Joint
title_full Microstructure and Mechanical Properties of Vacuum Diffusion Bonded Zr-4 Alloy Joint
title_fullStr Microstructure and Mechanical Properties of Vacuum Diffusion Bonded Zr-4 Alloy Joint
title_full_unstemmed Microstructure and Mechanical Properties of Vacuum Diffusion Bonded Zr-4 Alloy Joint
title_sort microstructure and mechanical properties of vacuum diffusion bonded zr-4 alloy joint
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/657561e0fd604f46a95f80f66609b81f
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