Sintesis Senyawa Aurivillius Lapis Empat PbBi4Ti4O15 dan PbBi3NdTi4O15 dengan Metode Lelehan Campuran Garam NaCl-KCl dan Karakterisasi Struktur

Four-layered Aurivillius phases PbBi4Ti4O15doped with Nd3+ with formula PbBi3NdTi4O15 were synthesized by molten-salt technique using NaCl and KCl (1:1 molar ratio) as the flux. Precursors were weighed stoichiometrycally and grinded with salts mixture in 1:7 ratio (product : salts mixture) until hom...

Descripción completa

Guardado en:

Detalles Bibliográficos
Autores principales:	Gita Rachmad Wibowo, Emriadi Emriadi, Zulhadjri Zulhadjri
Formato:	article
Lenguaje:	EN ID
Publicado:	Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Andalas 2019
Materias:	Aurivilius phase Molten Salt NaCl-KCl Le Bail Chemistry QD1-999 Biochemistry QD415-436
Acceso en línea:	https://doaj.org/article/69d94e9109de428d916acb2aca6aa519
Etiquetas:	Agregar Etiqueta Sin Etiquetas, Sea el primero en etiquetar este registro!

id	oai:doaj.org-article:69d94e9109de428d916acb2aca6aa519
record_format	dspace
spelling	oai:doaj.org-article:69d94e9109de428d916acb2aca6aa5192021-12-02T11:41:28ZSintesis Senyawa Aurivillius Lapis Empat PbBi4Ti4O15 dan PbBi3NdTi4O15 dengan Metode Lelehan Campuran Garam NaCl-KCl dan Karakterisasi Struktur1978-628X2476-896010.25077/jrk.v10i2.307https://doaj.org/article/69d94e9109de428d916acb2aca6aa5192019-09-01T00:00:00Zhttp://jrk.fmipa.unand.ac.id/index.php/jrk/article/view/307https://doaj.org/toc/1978-628Xhttps://doaj.org/toc/2476-8960Four-layered Aurivillius phases PbBi4Ti4O15doped with Nd3+ with formula PbBi3NdTi4O15 were synthesized by molten-salt technique using NaCl and KCl (1:1 molar ratio) as the flux. Precursors were weighed stoichiometrycally and grinded with salts mixture in 1:7 ratio (product : salts mixture) until homogenous. The samples were heated at temperature 600oC, 700oC, 800oC, and 900oC for 5 hours for each temperature. The products were characterized by X-ray diffractometer (XRD), Scanning Electron Microscope (SEM) and LCR-meter. XRD data were refined by Rietica program using Le Bail technique. Refinement results showed the best structure as the A21am of space group for both samples. Surface analysis for each samples morphology is the plate-like by SEM characterization. Dielectric constants measured at room temperature show that the sample doped Nd3+ has lower value than sample without containing Nd3+ cation.Gita Rachmad WibowoEmriadi EmriadiZulhadjri ZulhadjriDepartment of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas AndalasarticleAurivilius phaseMolten SaltNaCl-KClLe BailChemistryQD1-999BiochemistryQD415-436ENIDJurnal Riset Kimia, Vol 10, Iss 2, Pp 85-92 (2019)
institution	DOAJ
collection	DOAJ
language	EN ID
topic	Aurivilius phase Molten Salt NaCl-KCl Le Bail Chemistry QD1-999 Biochemistry QD415-436
spellingShingle	Aurivilius phase Molten Salt NaCl-KCl Le Bail Chemistry QD1-999 Biochemistry QD415-436 Gita Rachmad Wibowo Emriadi Emriadi Zulhadjri Zulhadjri Sintesis Senyawa Aurivillius Lapis Empat PbBi4Ti4O15 dan PbBi3NdTi4O15 dengan Metode Lelehan Campuran Garam NaCl-KCl dan Karakterisasi Struktur
description	Four-layered Aurivillius phases PbBi4Ti4O15doped with Nd3+ with formula PbBi3NdTi4O15 were synthesized by molten-salt technique using NaCl and KCl (1:1 molar ratio) as the flux. Precursors were weighed stoichiometrycally and grinded with salts mixture in 1:7 ratio (product : salts mixture) until homogenous. The samples were heated at temperature 600oC, 700oC, 800oC, and 900oC for 5 hours for each temperature. The products were characterized by X-ray diffractometer (XRD), Scanning Electron Microscope (SEM) and LCR-meter. XRD data were refined by Rietica program using Le Bail technique. Refinement results showed the best structure as the A21am of space group for both samples. Surface analysis for each samples morphology is the plate-like by SEM characterization. Dielectric constants measured at room temperature show that the sample doped Nd3+ has lower value than sample without containing Nd3+ cation.
format	article
author	Gita Rachmad Wibowo Emriadi Emriadi Zulhadjri Zulhadjri
author_facet	Gita Rachmad Wibowo Emriadi Emriadi Zulhadjri Zulhadjri
author_sort	Gita Rachmad Wibowo
title	Sintesis Senyawa Aurivillius Lapis Empat PbBi4Ti4O15 dan PbBi3NdTi4O15 dengan Metode Lelehan Campuran Garam NaCl-KCl dan Karakterisasi Struktur
title_short	Sintesis Senyawa Aurivillius Lapis Empat PbBi4Ti4O15 dan PbBi3NdTi4O15 dengan Metode Lelehan Campuran Garam NaCl-KCl dan Karakterisasi Struktur
title_full	Sintesis Senyawa Aurivillius Lapis Empat PbBi4Ti4O15 dan PbBi3NdTi4O15 dengan Metode Lelehan Campuran Garam NaCl-KCl dan Karakterisasi Struktur
title_fullStr	Sintesis Senyawa Aurivillius Lapis Empat PbBi4Ti4O15 dan PbBi3NdTi4O15 dengan Metode Lelehan Campuran Garam NaCl-KCl dan Karakterisasi Struktur
title_full_unstemmed	Sintesis Senyawa Aurivillius Lapis Empat PbBi4Ti4O15 dan PbBi3NdTi4O15 dengan Metode Lelehan Campuran Garam NaCl-KCl dan Karakterisasi Struktur
title_sort	sintesis senyawa aurivillius lapis empat pbbi4ti4o15 dan pbbi3ndti4o15 dengan metode lelehan campuran garam nacl-kcl dan karakterisasi struktur
publisher	Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Andalas
publishDate	2019
url	https://doaj.org/article/69d94e9109de428d916acb2aca6aa519
work_keys_str_mv	AT gitarachmadwibowo sintesissenyawaaurivilliuslapisempatpbbi4ti4o15danpbbi3ndti4o15denganmetodelelehancampurangaramnaclkcldankarakterisasistruktur AT emriadiemriadi sintesissenyawaaurivilliuslapisempatpbbi4ti4o15danpbbi3ndti4o15denganmetodelelehancampurangaramnaclkcldankarakterisasistruktur AT zulhadjrizulhadjri sintesissenyawaaurivilliuslapisempatpbbi4ti4o15danpbbi3ndti4o15denganmetodelelehancampurangaramnaclkcldankarakterisasistruktur
_version_	1718395402348134400

Sintesis Senyawa Aurivillius Lapis Empat PbBi4Ti4O15 dan PbBi3NdTi4O15 dengan Metode Lelehan Campuran Garam NaCl-KCl dan Karakterisasi Struktur

Ejemplares similares