Live Imaging of Micro-Wettability Experiments Performed for Low-Permeability Oil Reservoirs

Abstract Low-permeability (unconventional) hydrocarbon reservoirs exhibit a complex nanopore structure and micro (µm) -scale variability in composition which control fluid distribution, displacement and transport processes. Conventional methods for characterizing fluid-rock interaction are however t...

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Autores principales: Hanford J. Deglint, Christopher R. Clarkson, Chris DeBuhr, Amin Ghanizadeh
Formato: article
Lenguaje:EN
Publicado: Nature Portfolio 2017
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Acceso en línea:https://doaj.org/article/6bf0818697704394a5ca3e2d4ba11eb5
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Sumario:Abstract Low-permeability (unconventional) hydrocarbon reservoirs exhibit a complex nanopore structure and micro (µm) -scale variability in composition which control fluid distribution, displacement and transport processes. Conventional methods for characterizing fluid-rock interaction are however typically performed at a macro (mm) -scale on rock sample surfaces. In this work, innovative methods for the quantification of micro-scale variations in wettability and fluid distribution in a low-permeability oil reservoir was enabled by using an environmental scanning electron microscope. Live imaging of controlled water condensation/evaporation experiments allowed micro-droplet contact angles to be evaluated, while imaging combined with x-ray mapping of cryogenically frozen samples facilitated the evaluation of oil and water micro-droplet contact angles after successive fluid injection. For the first time, live imaging of fluids injected through a micro-injection system has enabled quantification of sessile and dynamic micro-droplet contact angles. Application of these combined methods has revealed dramatic spatial changes in fluid contact angles at the micro-scale, calling into question the applicability of macro-scale observations of fluid-rock interaction.