Substrate mediated nitridation of niobium into superconducting Nb2N thin films for phase slip study

Abstract Here we report a novel nitridation technique for transforming niobium into hexagonal Nb2N which appears to be superconducting below 1K. The nitridation is achieved by high temperature annealing of Nb films grown on Si3N4/Si (100) substrate under high vacuum. The structural characterization...

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Autores principales: Bikash Gajar, Sachin Yadav, Deepika Sawle, Kamlesh K. Maurya, Anurag Gupta, R. P. Aloysius, Sangeeta Sahoo
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Publicado: Nature Portfolio 2019
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Acceso en línea:https://doaj.org/article/7606c44e12774c2e94c53987c1bf1cd1
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spelling oai:doaj.org-article:7606c44e12774c2e94c53987c1bf1cd12021-12-02T15:08:32ZSubstrate mediated nitridation of niobium into superconducting Nb2N thin films for phase slip study10.1038/s41598-019-45338-12045-2322https://doaj.org/article/7606c44e12774c2e94c53987c1bf1cd12019-06-01T00:00:00Zhttps://doi.org/10.1038/s41598-019-45338-1https://doaj.org/toc/2045-2322Abstract Here we report a novel nitridation technique for transforming niobium into hexagonal Nb2N which appears to be superconducting below 1K. The nitridation is achieved by high temperature annealing of Nb films grown on Si3N4/Si (100) substrate under high vacuum. The structural characterization directs the formation of a majority Nb2N phase while the morphology shows granular nature of the films. The temperature dependent resistance measurements reveal a wide metal-to-superconductor transition featuring two distinct transition regions. The region close to the normal state varies strongly with the film thickness, whereas, the second region in the vicinity of the superconducting state remains almost unaltered but exhibiting resistive tailing. The current-voltage characteristics also display wide transition embedded with intermediate resistive states originated by phase slip lines. The transition width in current and the number of resistive steps depend on film thickness and they both increase with decrease in thickness. The broadening in transition width is explained by progressive establishment of superconductivity through proximity coupled superconducting nano-grains while finite size effects and quantum fluctuation may lead to the resistive tailing. Finally, by comparing with Nb control samples, we emphasize that Nb2N offers unconventional superconductivity with promises in the field of phase slip based device applications.Bikash GajarSachin YadavDeepika SawleKamlesh K. MauryaAnurag GuptaR. P. AloysiusSangeeta SahooNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 9, Iss 1, Pp 1-11 (2019)
institution DOAJ
collection DOAJ
language EN
topic Medicine
R
Science
Q
spellingShingle Medicine
R
Science
Q
Bikash Gajar
Sachin Yadav
Deepika Sawle
Kamlesh K. Maurya
Anurag Gupta
R. P. Aloysius
Sangeeta Sahoo
Substrate mediated nitridation of niobium into superconducting Nb2N thin films for phase slip study
description Abstract Here we report a novel nitridation technique for transforming niobium into hexagonal Nb2N which appears to be superconducting below 1K. The nitridation is achieved by high temperature annealing of Nb films grown on Si3N4/Si (100) substrate under high vacuum. The structural characterization directs the formation of a majority Nb2N phase while the morphology shows granular nature of the films. The temperature dependent resistance measurements reveal a wide metal-to-superconductor transition featuring two distinct transition regions. The region close to the normal state varies strongly with the film thickness, whereas, the second region in the vicinity of the superconducting state remains almost unaltered but exhibiting resistive tailing. The current-voltage characteristics also display wide transition embedded with intermediate resistive states originated by phase slip lines. The transition width in current and the number of resistive steps depend on film thickness and they both increase with decrease in thickness. The broadening in transition width is explained by progressive establishment of superconductivity through proximity coupled superconducting nano-grains while finite size effects and quantum fluctuation may lead to the resistive tailing. Finally, by comparing with Nb control samples, we emphasize that Nb2N offers unconventional superconductivity with promises in the field of phase slip based device applications.
format article
author Bikash Gajar
Sachin Yadav
Deepika Sawle
Kamlesh K. Maurya
Anurag Gupta
R. P. Aloysius
Sangeeta Sahoo
author_facet Bikash Gajar
Sachin Yadav
Deepika Sawle
Kamlesh K. Maurya
Anurag Gupta
R. P. Aloysius
Sangeeta Sahoo
author_sort Bikash Gajar
title Substrate mediated nitridation of niobium into superconducting Nb2N thin films for phase slip study
title_short Substrate mediated nitridation of niobium into superconducting Nb2N thin films for phase slip study
title_full Substrate mediated nitridation of niobium into superconducting Nb2N thin films for phase slip study
title_fullStr Substrate mediated nitridation of niobium into superconducting Nb2N thin films for phase slip study
title_full_unstemmed Substrate mediated nitridation of niobium into superconducting Nb2N thin films for phase slip study
title_sort substrate mediated nitridation of niobium into superconducting nb2n thin films for phase slip study
publisher Nature Portfolio
publishDate 2019
url https://doaj.org/article/7606c44e12774c2e94c53987c1bf1cd1
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