Direct curvature measurement of the compartments in bamboo-shaped multi-walled carbon nanotubes via scanning probe microscopy

Abstract Bamboo-shaped multi-walled carbon nanotubes (BS-MWCNTs) have compartmented structures inherently obtained during their catalytic growth, and the curvature of the compartmented structure is known to be determined by the morphology of the metal catalysts. In this study, the inside curvature o...

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Autor principal: Jae-Won Jang
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Publicado: Nature Portfolio 2021
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Acceso en línea:https://doaj.org/article/7a147180e90d4d0da5c2d4a4b7b341d6
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spelling oai:doaj.org-article:7a147180e90d4d0da5c2d4a4b7b341d62021-12-02T14:12:46ZDirect curvature measurement of the compartments in bamboo-shaped multi-walled carbon nanotubes via scanning probe microscopy10.1038/s41598-020-79692-22045-2322https://doaj.org/article/7a147180e90d4d0da5c2d4a4b7b341d62021-01-01T00:00:00Zhttps://doi.org/10.1038/s41598-020-79692-2https://doaj.org/toc/2045-2322Abstract Bamboo-shaped multi-walled carbon nanotubes (BS-MWCNTs) have compartmented structures inherently obtained during their catalytic growth, and the curvature of the compartmented structure is known to be determined by the morphology of the metal catalysts. In this study, the inside curvature of the BS-MWCNTs was directly measured through scanning probe microscopy (SPM). The surface of the compartment structures of BS-MWCNTs has discontinuous graphene layers and different frictional force levels depending on the curvature direction. That of the inside curvature can be directly observed through tribological analysis by adding and subtracting the lateral force microscopy images obtained on opposite sides along the axial direction of the BS-MWCNT (diameter of 500 nm). This tells us the direction of the inside curvature of the BS-MWCNT, which was also confirmed by identifying the growth direction of the BS-MWCNTs via scanning electron microscopy. Our demonstration implies that SPM can give the same insight into the structural characterization of nanomaterials that is relatively inexpensive and more user-friendly than currently used methods.Jae-Won JangNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 11, Iss 1, Pp 1-9 (2021)
institution DOAJ
collection DOAJ
language EN
topic Medicine
R
Science
Q
spellingShingle Medicine
R
Science
Q
Jae-Won Jang
Direct curvature measurement of the compartments in bamboo-shaped multi-walled carbon nanotubes via scanning probe microscopy
description Abstract Bamboo-shaped multi-walled carbon nanotubes (BS-MWCNTs) have compartmented structures inherently obtained during their catalytic growth, and the curvature of the compartmented structure is known to be determined by the morphology of the metal catalysts. In this study, the inside curvature of the BS-MWCNTs was directly measured through scanning probe microscopy (SPM). The surface of the compartment structures of BS-MWCNTs has discontinuous graphene layers and different frictional force levels depending on the curvature direction. That of the inside curvature can be directly observed through tribological analysis by adding and subtracting the lateral force microscopy images obtained on opposite sides along the axial direction of the BS-MWCNT (diameter of 500 nm). This tells us the direction of the inside curvature of the BS-MWCNT, which was also confirmed by identifying the growth direction of the BS-MWCNTs via scanning electron microscopy. Our demonstration implies that SPM can give the same insight into the structural characterization of nanomaterials that is relatively inexpensive and more user-friendly than currently used methods.
format article
author Jae-Won Jang
author_facet Jae-Won Jang
author_sort Jae-Won Jang
title Direct curvature measurement of the compartments in bamboo-shaped multi-walled carbon nanotubes via scanning probe microscopy
title_short Direct curvature measurement of the compartments in bamboo-shaped multi-walled carbon nanotubes via scanning probe microscopy
title_full Direct curvature measurement of the compartments in bamboo-shaped multi-walled carbon nanotubes via scanning probe microscopy
title_fullStr Direct curvature measurement of the compartments in bamboo-shaped multi-walled carbon nanotubes via scanning probe microscopy
title_full_unstemmed Direct curvature measurement of the compartments in bamboo-shaped multi-walled carbon nanotubes via scanning probe microscopy
title_sort direct curvature measurement of the compartments in bamboo-shaped multi-walled carbon nanotubes via scanning probe microscopy
publisher Nature Portfolio
publishDate 2021
url https://doaj.org/article/7a147180e90d4d0da5c2d4a4b7b341d6
work_keys_str_mv AT jaewonjang directcurvaturemeasurementofthecompartmentsinbambooshapedmultiwalledcarbonnanotubesviascanningprobemicroscopy
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