Graphene Enhanced Secondary Ion Mass Spectrometry (GESIMS)

Abstract The following invention - Graphene Enhanced Secondary Ion Mass Spectrometry - (pending European patent application no. EP 16461554.4) is related to a method of analysing a solid substrate by means of Secondary Ion Mass Spectrometry (SIMS). It comprises the steps of providing a graphene laye...

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Autores principales: Paweł Piotr Michałowski, Wawrzyniec Kaszub, Iwona Pasternak, Włodek Strupiński
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Lenguaje:EN
Publicado: Nature Portfolio 2017
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Acceso en línea:https://doaj.org/article/7c2bf08d3b674ec3acf20de4206fbf05
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spelling oai:doaj.org-article:7c2bf08d3b674ec3acf20de4206fbf052021-12-02T11:53:13ZGraphene Enhanced Secondary Ion Mass Spectrometry (GESIMS)10.1038/s41598-017-07984-12045-2322https://doaj.org/article/7c2bf08d3b674ec3acf20de4206fbf052017-08-01T00:00:00Zhttps://doi.org/10.1038/s41598-017-07984-1https://doaj.org/toc/2045-2322Abstract The following invention - Graphene Enhanced Secondary Ion Mass Spectrometry - (pending European patent application no. EP 16461554.4) is related to a method of analysing a solid substrate by means of Secondary Ion Mass Spectrometry (SIMS). It comprises the steps of providing a graphene layer over the substrate surface and analysing ejected secondary anions through mass spectrometry analysis. The graphene layer acts as a kind of filament that emits a lot of secondary electrons during the experiment which significantly increases the negative ionization probability and thus the intensity of the SIMS signal can be more than two orders of magnitude higher than that of a similar sample without graphene. The method is particularly useful for the analysis of surfaces, 2D materials and ultra-thin films. The intensity of dopants and contamination signals can be enhanced up to 35 times, which approaches the detection limit of ~1015 atoms/cm 3, otherwise unreachable in a standard static SIMS analysis.Paweł Piotr MichałowskiWawrzyniec KaszubIwona PasternakWłodek StrupińskiNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 7, Iss 1, Pp 1-8 (2017)
institution DOAJ
collection DOAJ
language EN
topic Medicine
R
Science
Q
spellingShingle Medicine
R
Science
Q
Paweł Piotr Michałowski
Wawrzyniec Kaszub
Iwona Pasternak
Włodek Strupiński
Graphene Enhanced Secondary Ion Mass Spectrometry (GESIMS)
description Abstract The following invention - Graphene Enhanced Secondary Ion Mass Spectrometry - (pending European patent application no. EP 16461554.4) is related to a method of analysing a solid substrate by means of Secondary Ion Mass Spectrometry (SIMS). It comprises the steps of providing a graphene layer over the substrate surface and analysing ejected secondary anions through mass spectrometry analysis. The graphene layer acts as a kind of filament that emits a lot of secondary electrons during the experiment which significantly increases the negative ionization probability and thus the intensity of the SIMS signal can be more than two orders of magnitude higher than that of a similar sample without graphene. The method is particularly useful for the analysis of surfaces, 2D materials and ultra-thin films. The intensity of dopants and contamination signals can be enhanced up to 35 times, which approaches the detection limit of ~1015 atoms/cm 3, otherwise unreachable in a standard static SIMS analysis.
format article
author Paweł Piotr Michałowski
Wawrzyniec Kaszub
Iwona Pasternak
Włodek Strupiński
author_facet Paweł Piotr Michałowski
Wawrzyniec Kaszub
Iwona Pasternak
Włodek Strupiński
author_sort Paweł Piotr Michałowski
title Graphene Enhanced Secondary Ion Mass Spectrometry (GESIMS)
title_short Graphene Enhanced Secondary Ion Mass Spectrometry (GESIMS)
title_full Graphene Enhanced Secondary Ion Mass Spectrometry (GESIMS)
title_fullStr Graphene Enhanced Secondary Ion Mass Spectrometry (GESIMS)
title_full_unstemmed Graphene Enhanced Secondary Ion Mass Spectrometry (GESIMS)
title_sort graphene enhanced secondary ion mass spectrometry (gesims)
publisher Nature Portfolio
publishDate 2017
url https://doaj.org/article/7c2bf08d3b674ec3acf20de4206fbf05
work_keys_str_mv AT pawełpiotrmichałowski grapheneenhancedsecondaryionmassspectrometrygesims
AT wawrzynieckaszub grapheneenhancedsecondaryionmassspectrometrygesims
AT iwonapasternak grapheneenhancedsecondaryionmassspectrometrygesims
AT włodekstrupinski grapheneenhancedsecondaryionmassspectrometrygesims
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