DETERMINATION OF CHLORPYRIFOS IN APPLE FROM THE RESEN REGION

The aim of this research is to determine the presence of chlorpyrifos in two varieties of apples: Golden Delicious and Idared in two different locations (Evla and Krveni) from the Resen region in the country. Chlorpyrifos is organophosphate pesticide (insecticide) used to protect apples from insects...

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Autores principales: Vezirka JANKULOSKA, Ilija KAROV, Gorica PAVLOVSKA, Ilija BUZLEVSKI
Formato: article
Lenguaje:EN
Publicado: Stefan cel Mare University of Suceava 2017
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Acceso en línea:https://doaj.org/article/866c957fd6ec46b18e6fcaba8020ed17
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spelling oai:doaj.org-article:866c957fd6ec46b18e6fcaba8020ed172021-12-02T19:27:32ZDETERMINATION OF CHLORPYRIFOS IN APPLE FROM THE RESEN REGION2068-66092559-6381https://doaj.org/article/866c957fd6ec46b18e6fcaba8020ed172017-03-01T00:00:00Zhttp://www.fia.usv.ro/fiajournal/index.php/FENS/article/view/466/462https://doaj.org/toc/2068-6609https://doaj.org/toc/2559-6381The aim of this research is to determine the presence of chlorpyrifos in two varieties of apples: Golden Delicious and Idared in two different locations (Evla and Krveni) from the Resen region in the country. Chlorpyrifos is organophosphate pesticide (insecticide) used to protect apples from insects which can cause significant damage in apple production. The apples are analyzed in four development phases and in each phase the presence of chlorpyrifos is determined. Chlorpiryfos analysis of the apples is performed by liquid chromatography-tandem mass spectrometry (LC-MS/MS) followed by an extraction/separation cleansing with acetonitrile and the dispersive SPE - QuEChERS - method. The results are compared with the maximum residue levels (MRL) prescribed by the legislation of the Republic of Macedonia. The conclusion is that chlorpyrifos is variously represented in most phases, regardless of the phase and location where the apple is grown. At certain phase the concentration exceedes MRL, however during the harvest, apples are safe to be consumed. Higher presence of chlorpyrifos is found in Idared apples at Kriveni location as compared to Evla. Тhe presence of chlorpyrifos in Golden Delicious is almost equal in both locations. From the statistical analysis of the data it is noticeable that the use of chlorpyrifos does not depend on the (type) variety of apple but rather on the location where the apple is grown.Vezirka JANKULOSKAIlija KAROVGorica PAVLOVSKAIlija BUZLEVSKIStefan cel Mare University of SuceavaarticlechlorpyrifospesticidesapplesGolden DeliciousIdaretFood processing and manufactureTP368-456ENFood and Environment Safety, Vol 16, Iss 1, Pp 34-39 (2017)
institution DOAJ
collection DOAJ
language EN
topic chlorpyrifos
pesticides
apples
Golden Delicious
Idaret
Food processing and manufacture
TP368-456
spellingShingle chlorpyrifos
pesticides
apples
Golden Delicious
Idaret
Food processing and manufacture
TP368-456
Vezirka JANKULOSKA
Ilija KAROV
Gorica PAVLOVSKA
Ilija BUZLEVSKI
DETERMINATION OF CHLORPYRIFOS IN APPLE FROM THE RESEN REGION
description The aim of this research is to determine the presence of chlorpyrifos in two varieties of apples: Golden Delicious and Idared in two different locations (Evla and Krveni) from the Resen region in the country. Chlorpyrifos is organophosphate pesticide (insecticide) used to protect apples from insects which can cause significant damage in apple production. The apples are analyzed in four development phases and in each phase the presence of chlorpyrifos is determined. Chlorpiryfos analysis of the apples is performed by liquid chromatography-tandem mass spectrometry (LC-MS/MS) followed by an extraction/separation cleansing with acetonitrile and the dispersive SPE - QuEChERS - method. The results are compared with the maximum residue levels (MRL) prescribed by the legislation of the Republic of Macedonia. The conclusion is that chlorpyrifos is variously represented in most phases, regardless of the phase and location where the apple is grown. At certain phase the concentration exceedes MRL, however during the harvest, apples are safe to be consumed. Higher presence of chlorpyrifos is found in Idared apples at Kriveni location as compared to Evla. Тhe presence of chlorpyrifos in Golden Delicious is almost equal in both locations. From the statistical analysis of the data it is noticeable that the use of chlorpyrifos does not depend on the (type) variety of apple but rather on the location where the apple is grown.
format article
author Vezirka JANKULOSKA
Ilija KAROV
Gorica PAVLOVSKA
Ilija BUZLEVSKI
author_facet Vezirka JANKULOSKA
Ilija KAROV
Gorica PAVLOVSKA
Ilija BUZLEVSKI
author_sort Vezirka JANKULOSKA
title DETERMINATION OF CHLORPYRIFOS IN APPLE FROM THE RESEN REGION
title_short DETERMINATION OF CHLORPYRIFOS IN APPLE FROM THE RESEN REGION
title_full DETERMINATION OF CHLORPYRIFOS IN APPLE FROM THE RESEN REGION
title_fullStr DETERMINATION OF CHLORPYRIFOS IN APPLE FROM THE RESEN REGION
title_full_unstemmed DETERMINATION OF CHLORPYRIFOS IN APPLE FROM THE RESEN REGION
title_sort determination of chlorpyrifos in apple from the resen region
publisher Stefan cel Mare University of Suceava
publishDate 2017
url https://doaj.org/article/866c957fd6ec46b18e6fcaba8020ed17
work_keys_str_mv AT vezirkajankuloska determinationofchlorpyrifosinapplefromtheresenregion
AT ilijakarov determinationofchlorpyrifosinapplefromtheresenregion
AT goricapavlovska determinationofchlorpyrifosinapplefromtheresenregion
AT ilijabuzlevski determinationofchlorpyrifosinapplefromtheresenregion
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