PENGARUH RUTE SINTESIS TERHADAP KEEFEKTIFAN PENGIKATAN GUGUS PDETA PADA SINTESIS Fe3O4@SiO2@PDETA

Synthesis of Fe3O4@SiO2 modified with propyldiethylenetriamine (Fe3O4@SiO2@PDETA) with variation of synthesis routes have been investigated. Research was begun with synthesis of Fe3O4 using dispersion agent of trisodium citrate at coprecipitation system through stirring using ultrasonic wave. Coatin...

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Autores principales:	Susanto Susanto, Ricka Prasdiantika
Formato:	article
Lenguaje:	EN ID
Publicado:	Universitas Gadjah Mada 2019
Materias:	effectiveness binding magnetite propyldiethylene-triamine silica modified synthesis routes Technology T Technology (General) T1-995 Science Q Science (General) Q1-390
Acceso en línea:	https://doaj.org/article/8a29284160594e0caa9f211ba5010a96
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spelling	oai:doaj.org-article:8a29284160594e0caa9f211ba5010a962021-11-14T03:34:21ZPENGARUH RUTE SINTESIS TERHADAP KEEFEKTIFAN PENGIKATAN GUGUS PDETA PADA SINTESIS Fe3O4@SiO2@PDETA2089-61312443-131110.22146/teknosains.36264https://doaj.org/article/8a29284160594e0caa9f211ba5010a962019-01-01T00:00:00Zhttps://jurnal.ugm.ac.id/teknosains/article/view/36264https://doaj.org/toc/2089-6131https://doaj.org/toc/2443-1311Synthesis of Fe3O4@SiO2 modified with propyldiethylenetriamine (Fe3O4@SiO2@PDETA) with variation of synthesis routes have been investigated. Research was begun with synthesis of Fe3O4 using dispersion agent of trisodium citrate at coprecipitation system through stirring using ultrasonic wave. Coating magnetite with propyldiethylenetriamine modified silica was carried out through sol-gel process with two different mixing sequences of raw materials (two synthesis routes) with main materials of Fe3O4 synthesized, N-[3-(Trimethoxysilyl)propyl]-diethylenetriamine (TMSPDETA) and Na2SiO3. The products were characterized by fourier transform infrared (FTIR) spectrophotometer and scanning electron microscope-energy dispersive X-ray (SEM-EDX). Results indicate that Fe3O4@SiO2@PDETA has been synthesized succesfully. Fe3O4@SiO2@PDETA synthesized through route 1 (magnetite mixed with a mixture TMSPDETA and Na2SiO3) contains more propyldiethylenetriamine group than that of through route 2 (magnetite mixed with Na2SiO3 solution, then mixed with TMSPDETA)Susanto SusantoRicka PrasdiantikaUniversitas Gadjah Madaarticleeffectiveness bindingmagnetitepropyldiethylene-triaminesilica modifiedsynthesis routesTechnologyTTechnology (General)T1-995ScienceQScience (General)Q1-390ENIDJurnal Teknosains: Jurnal Ilmiah Sains dan Teknologi, Vol 8, Iss 1, Pp 39-47 (2019)
institution	DOAJ
collection	DOAJ
language	EN ID
topic	effectiveness binding magnetite propyldiethylene-triamine silica modified synthesis routes Technology T Technology (General) T1-995 Science Q Science (General) Q1-390
spellingShingle	effectiveness binding magnetite propyldiethylene-triamine silica modified synthesis routes Technology T Technology (General) T1-995 Science Q Science (General) Q1-390 Susanto Susanto Ricka Prasdiantika PENGARUH RUTE SINTESIS TERHADAP KEEFEKTIFAN PENGIKATAN GUGUS PDETA PADA SINTESIS Fe3O4@SiO2@PDETA
description	Synthesis of Fe3O4@SiO2 modified with propyldiethylenetriamine (Fe3O4@SiO2@PDETA) with variation of synthesis routes have been investigated. Research was begun with synthesis of Fe3O4 using dispersion agent of trisodium citrate at coprecipitation system through stirring using ultrasonic wave. Coating magnetite with propyldiethylenetriamine modified silica was carried out through sol-gel process with two different mixing sequences of raw materials (two synthesis routes) with main materials of Fe3O4 synthesized, N-[3-(Trimethoxysilyl)propyl]-diethylenetriamine (TMSPDETA) and Na2SiO3. The products were characterized by fourier transform infrared (FTIR) spectrophotometer and scanning electron microscope-energy dispersive X-ray (SEM-EDX). Results indicate that Fe3O4@SiO2@PDETA has been synthesized succesfully. Fe3O4@SiO2@PDETA synthesized through route 1 (magnetite mixed with a mixture TMSPDETA and Na2SiO3) contains more propyldiethylenetriamine group than that of through route 2 (magnetite mixed with Na2SiO3 solution, then mixed with TMSPDETA)
format	article
author	Susanto Susanto Ricka Prasdiantika
author_facet	Susanto Susanto Ricka Prasdiantika
author_sort	Susanto Susanto
title	PENGARUH RUTE SINTESIS TERHADAP KEEFEKTIFAN PENGIKATAN GUGUS PDETA PADA SINTESIS Fe3O4@SiO2@PDETA
title_short	PENGARUH RUTE SINTESIS TERHADAP KEEFEKTIFAN PENGIKATAN GUGUS PDETA PADA SINTESIS Fe3O4@SiO2@PDETA
title_full	PENGARUH RUTE SINTESIS TERHADAP KEEFEKTIFAN PENGIKATAN GUGUS PDETA PADA SINTESIS Fe3O4@SiO2@PDETA
title_fullStr	PENGARUH RUTE SINTESIS TERHADAP KEEFEKTIFAN PENGIKATAN GUGUS PDETA PADA SINTESIS Fe3O4@SiO2@PDETA
title_full_unstemmed	PENGARUH RUTE SINTESIS TERHADAP KEEFEKTIFAN PENGIKATAN GUGUS PDETA PADA SINTESIS Fe3O4@SiO2@PDETA
title_sort	pengaruh rute sintesis terhadap keefektifan pengikatan gugus pdeta pada sintesis fe3o4@sio2@pdeta
publisher	Universitas Gadjah Mada
publishDate	2019
url	https://doaj.org/article/8a29284160594e0caa9f211ba5010a96
work_keys_str_mv	AT susantosusanto pengaruhrutesintesisterhadapkeefektifanpengikatanguguspdetapadasintesisfe3o4sio2pdeta AT rickaprasdiantika pengaruhrutesintesisterhadapkeefektifanpengikatanguguspdetapadasintesisfe3o4sio2pdeta
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PENGARUH RUTE SINTESIS TERHADAP KEEFEKTIFAN PENGIKATAN GUGUS PDETA PADA SINTESIS Fe3O4@SiO2@PDETA

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