Analysis, Design and Realization of a Furnace for In Situ Wettability Experiments at High Temperatures under X-ray Microtomography

In this study, we analyzed the problem of a compact furnace, to be used for in situ experiments in a cone-beam X-ray microtomography commercial system. The design process was accomplished and outlined through its main steps, until the realization of a prototype. The furnace was conceived to carry ou...

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Autores principales:	Roberto Fedele, Fareeha Hameed, Nicola Cefis, Gabriele Vergani
Formato:	article
Lenguaje:	EN
Publicado:	MDPI AG 2021
Materias:	X-ray microtomography in situ experiments wettability brazing joints materials science Photography TR1-1050 Computer applications to medicine. Medical informatics R858-859.7 Electronic computers. Computer science QA75.5-76.95
Acceso en línea:	https://doaj.org/article/907e66b671804a3e8d480ef92153d685
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id	oai:doaj.org-article:907e66b671804a3e8d480ef92153d685
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spelling	oai:doaj.org-article:907e66b671804a3e8d480ef92153d6852021-11-25T18:03:32ZAnalysis, Design and Realization of a Furnace for In Situ Wettability Experiments at High Temperatures under X-ray Microtomography10.3390/jimaging71102402313-433Xhttps://doaj.org/article/907e66b671804a3e8d480ef92153d6852021-11-01T00:00:00Zhttps://www.mdpi.com/2313-433X/7/11/240https://doaj.org/toc/2313-433XIn this study, we analyzed the problem of a compact furnace, to be used for in situ experiments in a cone-beam X-ray microtomography commercial system. The design process was accomplished and outlined through its main steps, until the realization of a prototype. The furnace was conceived to carry out wettability experiments at temperatures up to 700 °C and under inert atmosphere on sessile droplets of a molten metal alloy, with a few millimeters diameter, posed on a thin ceramic substrate. X-ray imaging of the molten droplet is expected to permit an accurate three-dimensional reconstruction of the droplet profile and a robust estimation of the related quantities (such as the contact angle and the surface tension) utilized for the assessment of metal-ceramic joints by brazing. The challenges faced during this project, mostly related to the constraints of the setup, and the novel solutions implemented were discussed also with the support of analytical and numerical tools, in terms of interaction of X-rays with matter, geometry and working principle, heat transfer and insulation, material selection.Roberto FedeleFareeha HameedNicola CefisGabriele VerganiMDPI AGarticleX-ray microtomographyin situ experimentswettabilitybrazing jointsmaterials sciencePhotographyTR1-1050Computer applications to medicine. Medical informaticsR858-859.7Electronic computers. Computer scienceQA75.5-76.95ENJournal of Imaging, Vol 7, Iss 240, p 240 (2021)
institution	DOAJ
collection	DOAJ
language	EN
topic	X-ray microtomography in situ experiments wettability brazing joints materials science Photography TR1-1050 Computer applications to medicine. Medical informatics R858-859.7 Electronic computers. Computer science QA75.5-76.95
spellingShingle	X-ray microtomography in situ experiments wettability brazing joints materials science Photography TR1-1050 Computer applications to medicine. Medical informatics R858-859.7 Electronic computers. Computer science QA75.5-76.95 Roberto Fedele Fareeha Hameed Nicola Cefis Gabriele Vergani Analysis, Design and Realization of a Furnace for In Situ Wettability Experiments at High Temperatures under X-ray Microtomography
description	In this study, we analyzed the problem of a compact furnace, to be used for in situ experiments in a cone-beam X-ray microtomography commercial system. The design process was accomplished and outlined through its main steps, until the realization of a prototype. The furnace was conceived to carry out wettability experiments at temperatures up to 700 °C and under inert atmosphere on sessile droplets of a molten metal alloy, with a few millimeters diameter, posed on a thin ceramic substrate. X-ray imaging of the molten droplet is expected to permit an accurate three-dimensional reconstruction of the droplet profile and a robust estimation of the related quantities (such as the contact angle and the surface tension) utilized for the assessment of metal-ceramic joints by brazing. The challenges faced during this project, mostly related to the constraints of the setup, and the novel solutions implemented were discussed also with the support of analytical and numerical tools, in terms of interaction of X-rays with matter, geometry and working principle, heat transfer and insulation, material selection.
format	article
author	Roberto Fedele Fareeha Hameed Nicola Cefis Gabriele Vergani
author_facet	Roberto Fedele Fareeha Hameed Nicola Cefis Gabriele Vergani
author_sort	Roberto Fedele
title	Analysis, Design and Realization of a Furnace for In Situ Wettability Experiments at High Temperatures under X-ray Microtomography
title_short	Analysis, Design and Realization of a Furnace for In Situ Wettability Experiments at High Temperatures under X-ray Microtomography
title_full	Analysis, Design and Realization of a Furnace for In Situ Wettability Experiments at High Temperatures under X-ray Microtomography
title_fullStr	Analysis, Design and Realization of a Furnace for In Situ Wettability Experiments at High Temperatures under X-ray Microtomography
title_full_unstemmed	Analysis, Design and Realization of a Furnace for In Situ Wettability Experiments at High Temperatures under X-ray Microtomography
title_sort	analysis, design and realization of a furnace for in situ wettability experiments at high temperatures under x-ray microtomography
publisher	MDPI AG
publishDate	2021
url	https://doaj.org/article/907e66b671804a3e8d480ef92153d685
work_keys_str_mv	AT robertofedele analysisdesignandrealizationofafurnaceforinsituwettabilityexperimentsathightemperaturesunderxraymicrotomography AT fareehahameed analysisdesignandrealizationofafurnaceforinsituwettabilityexperimentsathightemperaturesunderxraymicrotomography AT nicolacefis analysisdesignandrealizationofafurnaceforinsituwettabilityexperimentsathightemperaturesunderxraymicrotomography AT gabrielevergani analysisdesignandrealizationofafurnaceforinsituwettabilityexperimentsathightemperaturesunderxraymicrotomography
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Analysis, Design and Realization of a Furnace for In Situ Wettability Experiments at High Temperatures under X-ray Microtomography

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