Application of Micro Slurry-Jet Erosion (MSE) for the Evaluation of Surface Properties of PVD TiN / TiCN Two-Layer Coatings

In this study, the potential of a Micro Slurry-jet Erosion (MSE) test to swiftly evaluate the intrinsic surface strength properties of thin multi-layer coatings is demonstrated. A slurry containing 1.2 μm alumina particles was impacted at high velocity perpendicular to PVD TiN/TiCN (TiCN on t...

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Autores principales: Yoshiro Iwai, Yoshiyasu Nanjo, Kenichi Okazaki, Masanori Tao, Eisuke Sentoku
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Publicado: Japanese Society of Tribologists 2017
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Acceso en línea:https://doaj.org/article/96368cae9a1447d3a9bc770689678db7
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spelling oai:doaj.org-article:96368cae9a1447d3a9bc770689678db72021-11-05T09:20:33ZApplication of Micro Slurry-Jet Erosion (MSE) for the Evaluation of Surface Properties of PVD TiN / TiCN Two-Layer Coatings1881-219810.2474/trol.12.49https://doaj.org/article/96368cae9a1447d3a9bc770689678db72017-05-01T00:00:00Zhttps://www.jstage.jst.go.jp/article/trol/12/2/12_49/_pdf/-char/enhttps://doaj.org/toc/1881-2198In this study, the potential of a Micro Slurry-jet Erosion (MSE) test to swiftly evaluate the intrinsic surface strength properties of thin multi-layer coatings is demonstrated. A slurry containing 1.2 μm alumina particles was impacted at high velocity perpendicular to PVD TiN/TiCN (TiCN on top of TiN) and TiN coatings deposited on high-speed steel by a hollow cathode discharge (HCD) or an cathodic arc (CA) method. In addition, nano-indentation and XRD, GDOES analyses were done for the original surfaces. By measuring the variation of erosion depth against test time, the MSE test made it possible to evaluate the individual erosion properties of TiCN and TiN layers independent of the substrate. Although the hardness of TiCN layers, coated by HCD or CA, was measured with nano-indentation and found to be approximately 20% higher than for TiN, the erosion rates of TiCN layers were found to be between 32% and 38% of the erosion rate of TiN. For the HCD coating, the erosion proceeded uniformly and produced a mostly smooth surface. On the other hand, for the CA coating, a pitted surface was observed. The existence of the hollows blemishes which caused by macroparticles i. e. droplets in the coating may affect the difference in the erosion rates between HCD and CA coatings. Consequently, the MSE test may be useful to evaluate the difference of the morphology of coatings as well as the surface strength which are related with the fabrication process.Yoshiro IwaiYoshiyasu NanjoKenichi OkazakiMasanori TaoEisuke SentokuJapanese Society of Tribologistsarticlemicro slurry-jet erosionmse, surface strength evaluationtwo-layer coatingtin/ticnPhysicsQC1-999Engineering (General). Civil engineering (General)TA1-2040Mechanical engineering and machineryTJ1-1570ChemistryQD1-999ENTribology Online, Vol 12, Iss 2, Pp 49-57 (2017)
institution DOAJ
collection DOAJ
language EN
topic micro slurry-jet erosion
mse, surface strength evaluation
two-layer coating
tin/ticn
Physics
QC1-999
Engineering (General). Civil engineering (General)
TA1-2040
Mechanical engineering and machinery
TJ1-1570
Chemistry
QD1-999
spellingShingle micro slurry-jet erosion
mse, surface strength evaluation
two-layer coating
tin/ticn
Physics
QC1-999
Engineering (General). Civil engineering (General)
TA1-2040
Mechanical engineering and machinery
TJ1-1570
Chemistry
QD1-999
Yoshiro Iwai
Yoshiyasu Nanjo
Kenichi Okazaki
Masanori Tao
Eisuke Sentoku
Application of Micro Slurry-Jet Erosion (MSE) for the Evaluation of Surface Properties of PVD TiN / TiCN Two-Layer Coatings
description In this study, the potential of a Micro Slurry-jet Erosion (MSE) test to swiftly evaluate the intrinsic surface strength properties of thin multi-layer coatings is demonstrated. A slurry containing 1.2 μm alumina particles was impacted at high velocity perpendicular to PVD TiN/TiCN (TiCN on top of TiN) and TiN coatings deposited on high-speed steel by a hollow cathode discharge (HCD) or an cathodic arc (CA) method. In addition, nano-indentation and XRD, GDOES analyses were done for the original surfaces. By measuring the variation of erosion depth against test time, the MSE test made it possible to evaluate the individual erosion properties of TiCN and TiN layers independent of the substrate. Although the hardness of TiCN layers, coated by HCD or CA, was measured with nano-indentation and found to be approximately 20% higher than for TiN, the erosion rates of TiCN layers were found to be between 32% and 38% of the erosion rate of TiN. For the HCD coating, the erosion proceeded uniformly and produced a mostly smooth surface. On the other hand, for the CA coating, a pitted surface was observed. The existence of the hollows blemishes which caused by macroparticles i. e. droplets in the coating may affect the difference in the erosion rates between HCD and CA coatings. Consequently, the MSE test may be useful to evaluate the difference of the morphology of coatings as well as the surface strength which are related with the fabrication process.
format article
author Yoshiro Iwai
Yoshiyasu Nanjo
Kenichi Okazaki
Masanori Tao
Eisuke Sentoku
author_facet Yoshiro Iwai
Yoshiyasu Nanjo
Kenichi Okazaki
Masanori Tao
Eisuke Sentoku
author_sort Yoshiro Iwai
title Application of Micro Slurry-Jet Erosion (MSE) for the Evaluation of Surface Properties of PVD TiN / TiCN Two-Layer Coatings
title_short Application of Micro Slurry-Jet Erosion (MSE) for the Evaluation of Surface Properties of PVD TiN / TiCN Two-Layer Coatings
title_full Application of Micro Slurry-Jet Erosion (MSE) for the Evaluation of Surface Properties of PVD TiN / TiCN Two-Layer Coatings
title_fullStr Application of Micro Slurry-Jet Erosion (MSE) for the Evaluation of Surface Properties of PVD TiN / TiCN Two-Layer Coatings
title_full_unstemmed Application of Micro Slurry-Jet Erosion (MSE) for the Evaluation of Surface Properties of PVD TiN / TiCN Two-Layer Coatings
title_sort application of micro slurry-jet erosion (mse) for the evaluation of surface properties of pvd tin / ticn two-layer coatings
publisher Japanese Society of Tribologists
publishDate 2017
url https://doaj.org/article/96368cae9a1447d3a9bc770689678db7
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