Structural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped Mn2+ doped CdS nanoparticles and their applications in efficient detection of latent fingerprints

CdS:Mn2+ nanoparticles (NPs) stabilized with 2- mercaptoacetic acid (MAA) as a capping agent at different concentrations were developed by co-precipitation method. The X-ray diffraction (XRD) measurement revealed the existence of the cubic phase for stabilized NPs. Scherer’s method, Williamson-Hall...

Descripción completa

Guardado en:

Detalles Bibliográficos
Autores principales:	E. Indrajith Naik, H.S. Bhojya Naik, R. Viswanath, I.K. Suresh Gowda, B.R. Kirthan
Formato:	article
Lenguaje:	EN
Publicado:	KeAi Communications Co., Ltd. 2021
Materias:	Mn2+ doped CdS 2-Mercaptoacetic acid XRD Band gap tunability Photoluminescence Latent fingerprint Materials of engineering and construction. Mechanics of materials TA401-492 Energy conservation TJ163.26-163.5
Acceso en línea:	https://doaj.org/article/964547794b77445785756211537ad7ea
Etiquetas:	Agregar Etiqueta Sin Etiquetas, Sea el primero en etiquetar este registro!

id	oai:doaj.org-article:964547794b77445785756211537ad7ea
record_format	dspace
spelling	oai:doaj.org-article:964547794b77445785756211537ad7ea2021-11-30T04:16:51ZStructural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped Mn2+ doped CdS nanoparticles and their applications in efficient detection of latent fingerprints2589-299110.1016/j.mset.2020.12.007https://doaj.org/article/964547794b77445785756211537ad7ea2021-01-01T00:00:00Zhttp://www.sciencedirect.com/science/article/pii/S2589299120300938https://doaj.org/toc/2589-2991CdS:Mn2+ nanoparticles (NPs) stabilized with 2- mercaptoacetic acid (MAA) as a capping agent at different concentrations were developed by co-precipitation method. The X-ray diffraction (XRD) measurement revealed the existence of the cubic phase for stabilized NPs. Scherer’s method, Williamson-Hall (W-H) plot and size-strain plots (SSP) were helpful in the evaluation of the crystallite size and lattice strain of formed products. Ultraviolet–Visible absorption spectroscopy was adopted for energy gap determination, where Tauc’s plots infer that the energy gap increased with the increase in MAA volume percentage. The existence of MAA capping on CdS:Mn2+ was confirmed by fourier transform infrared (FTIR) spectroscopy. The outcome of transmission electron microscopy (TEM) results indicated the presence of spherical shape particles with a typical size of 6–7 nm, which is an encouraging feature for numerous applications. Two emission peaks around 477 nm (blue) and 575 nm (yellow) were observed for MAA stabilized CdS:Mn2+ NPs concerning photoluminescence (PL) spectroscopy. The disintegration and oxidation of the samples in the form of foremost weight loss and gain were studied by thermogravimetric analysis (TGA). Visualization of latent fingerprints (LFPs) under normal light on different porous and nonporous surfaces was conducted in the presence of MAA stabilized CdS:Mn2+ NPs. The acquired emissive fingerprint powder gave superior images with high distinction and resolution connecting the ridges and space. Based on these results, MAA capped Mn2+ doped CdS NPs can be used for the recognition of LFPs in solving criminal cases.E. Indrajith NaikH.S. Bhojya NaikR. ViswanathI.K. Suresh GowdaB.R. KirthanKeAi Communications Co., Ltd.articleMn2+ doped CdS2-Mercaptoacetic acidXRDBand gap tunabilityPhotoluminescenceLatent fingerprintMaterials of engineering and construction. Mechanics of materialsTA401-492Energy conservationTJ163.26-163.5ENMaterials Science for Energy Technologies, Vol 4, Iss , Pp 23-33 (2021)
institution	DOAJ
collection	DOAJ
language	EN
topic	Mn2+ doped CdS 2-Mercaptoacetic acid XRD Band gap tunability Photoluminescence Latent fingerprint Materials of engineering and construction. Mechanics of materials TA401-492 Energy conservation TJ163.26-163.5
spellingShingle	Mn2+ doped CdS 2-Mercaptoacetic acid XRD Band gap tunability Photoluminescence Latent fingerprint Materials of engineering and construction. Mechanics of materials TA401-492 Energy conservation TJ163.26-163.5 E. Indrajith Naik H.S. Bhojya Naik R. Viswanath I.K. Suresh Gowda B.R. Kirthan Structural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped Mn2+ doped CdS nanoparticles and their applications in efficient detection of latent fingerprints
description	CdS:Mn2+ nanoparticles (NPs) stabilized with 2- mercaptoacetic acid (MAA) as a capping agent at different concentrations were developed by co-precipitation method. The X-ray diffraction (XRD) measurement revealed the existence of the cubic phase for stabilized NPs. Scherer’s method, Williamson-Hall (W-H) plot and size-strain plots (SSP) were helpful in the evaluation of the crystallite size and lattice strain of formed products. Ultraviolet–Visible absorption spectroscopy was adopted for energy gap determination, where Tauc’s plots infer that the energy gap increased with the increase in MAA volume percentage. The existence of MAA capping on CdS:Mn2+ was confirmed by fourier transform infrared (FTIR) spectroscopy. The outcome of transmission electron microscopy (TEM) results indicated the presence of spherical shape particles with a typical size of 6–7 nm, which is an encouraging feature for numerous applications. Two emission peaks around 477 nm (blue) and 575 nm (yellow) were observed for MAA stabilized CdS:Mn2+ NPs concerning photoluminescence (PL) spectroscopy. The disintegration and oxidation of the samples in the form of foremost weight loss and gain were studied by thermogravimetric analysis (TGA). Visualization of latent fingerprints (LFPs) under normal light on different porous and nonporous surfaces was conducted in the presence of MAA stabilized CdS:Mn2+ NPs. The acquired emissive fingerprint powder gave superior images with high distinction and resolution connecting the ridges and space. Based on these results, MAA capped Mn2+ doped CdS NPs can be used for the recognition of LFPs in solving criminal cases.
format	article
author	E. Indrajith Naik H.S. Bhojya Naik R. Viswanath I.K. Suresh Gowda B.R. Kirthan
author_facet	E. Indrajith Naik H.S. Bhojya Naik R. Viswanath I.K. Suresh Gowda B.R. Kirthan
author_sort	E. Indrajith Naik
title	Structural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped Mn2+ doped CdS nanoparticles and their applications in efficient detection of latent fingerprints
title_short	Structural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped Mn2+ doped CdS nanoparticles and their applications in efficient detection of latent fingerprints
title_full	Structural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped Mn2+ doped CdS nanoparticles and their applications in efficient detection of latent fingerprints
title_fullStr	Structural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped Mn2+ doped CdS nanoparticles and their applications in efficient detection of latent fingerprints
title_full_unstemmed	Structural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped Mn2+ doped CdS nanoparticles and their applications in efficient detection of latent fingerprints
title_sort	structural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped mn2+ doped cds nanoparticles and their applications in efficient detection of latent fingerprints
publisher	KeAi Communications Co., Ltd.
publishDate	2021
url	https://doaj.org/article/964547794b77445785756211537ad7ea
work_keys_str_mv	AT eindrajithnaik structuralopticalandphotoluminescenceenhancementof2mercaptoaceticacidcappedmn2dopedcdsnanoparticlesandtheirapplicationsinefficientdetectionoflatentfingerprints AT hsbhojyanaik structuralopticalandphotoluminescenceenhancementof2mercaptoaceticacidcappedmn2dopedcdsnanoparticlesandtheirapplicationsinefficientdetectionoflatentfingerprints AT rviswanath structuralopticalandphotoluminescenceenhancementof2mercaptoaceticacidcappedmn2dopedcdsnanoparticlesandtheirapplicationsinefficientdetectionoflatentfingerprints AT iksureshgowda structuralopticalandphotoluminescenceenhancementof2mercaptoaceticacidcappedmn2dopedcdsnanoparticlesandtheirapplicationsinefficientdetectionoflatentfingerprints AT brkirthan structuralopticalandphotoluminescenceenhancementof2mercaptoaceticacidcappedmn2dopedcdsnanoparticlesandtheirapplicationsinefficientdetectionoflatentfingerprints
_version_	1718406820193632256

Structural, optical and photoluminescence enhancement of 2-mercaptoacetic acid capped Mn2+ doped CdS nanoparticles and their applications in efficient detection of latent fingerprints

Ejemplares similares