Fifty years of Rietveld refinement: Methodology and guidelines in superconductors and functional magnetic nanoadsorbents

The Rietveld refinement method has taken high relevance since its creation. Nowadays, it is an useful tool in many fields of industry, materials science, and technology. For these reasons, it becomes a need for scientists and engineers whom pretend to use it for proper analysis of their materials....

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Autores principales:	Diego Alberto Flores Cano, Anais Roxana Chino Quispe, Renzo Rueda Vellasmin, Joao Andre Ocampo Anticona, Juan Carlos González, Juan Adrián Ramos Guivar
Formato:	article
Lenguaje:	EN ES
Publicado:	Instituto de Investigación de Física 2021
Materias:	superconductors magnetic nanoadsorbents Rietveld method multiphasic analysis microstructural parameters Physics QC1-999
Acceso en línea:	https://doaj.org/article/9af7ce09cf6148608698dfd998ba9f48
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spelling	oai:doaj.org-article:9af7ce09cf6148608698dfd998ba9f482021-11-24T02:40:03ZFifty years of Rietveld refinement: Methodology and guidelines in superconductors and functional magnetic nanoadsorbents1605-77241728-2977https://doaj.org/article/9af7ce09cf6148608698dfd998ba9f482021-11-01T00:00:00Zhttps://revistasinvestigacion.unmsm.edu.pe/index.php/fisica/article/view/21028https://doaj.org/toc/1605-7724https://doaj.org/toc/1728-2977 The Rietveld refinement method has taken high relevance since its creation. Nowadays, it is an useful tool in many fields of industry, materials science, and technology. For these reasons, it becomes a need for scientists and engineers whom pretend to use it for proper analysis of their materials. However, the initiation in the method can be slow, taking into account the accelerated rhythm of the research and economic demands. Thus, this work is an intend to fulfill this hole, providing the basic foundations and methodology of the Rietveld refinement in a brief way, this along with the results of its application in superconducting samples of Yttrium Barium Copper Oxide and magnesium diboride, and functional magnetic nanoadsorbents of maghemite and a multiphasic composite (iron oxide, hydroxyapatite and secondary phases). In the process, an in-detail protocol was designed and provided. It was concluded that the samples were successfully refined and that this work represents a fast introduction to the Rietveld method for which beginners can obtain good results while making correct interpretations of the whole refinement process. Diego Alberto Flores CanoAnais Roxana Chino QuispeRenzo Rueda VellasminJoao Andre Ocampo AnticonaJuan Carlos GonzálezJuan Adrián Ramos GuivarInstituto de Investigación de Físicaarticlesuperconductorsmagnetic nanoadsorbentsRietveld methodmultiphasic analysismicrostructural parametersPhysicsQC1-999ENESRevista de Investigación de Física (2021)
institution	DOAJ
collection	DOAJ
language	EN ES
topic	superconductors magnetic nanoadsorbents Rietveld method multiphasic analysis microstructural parameters Physics QC1-999
spellingShingle	superconductors magnetic nanoadsorbents Rietveld method multiphasic analysis microstructural parameters Physics QC1-999 Diego Alberto Flores Cano Anais Roxana Chino Quispe Renzo Rueda Vellasmin Joao Andre Ocampo Anticona Juan Carlos González Juan Adrián Ramos Guivar Fifty years of Rietveld refinement: Methodology and guidelines in superconductors and functional magnetic nanoadsorbents
description	The Rietveld refinement method has taken high relevance since its creation. Nowadays, it is an useful tool in many fields of industry, materials science, and technology. For these reasons, it becomes a need for scientists and engineers whom pretend to use it for proper analysis of their materials. However, the initiation in the method can be slow, taking into account the accelerated rhythm of the research and economic demands. Thus, this work is an intend to fulfill this hole, providing the basic foundations and methodology of the Rietveld refinement in a brief way, this along with the results of its application in superconducting samples of Yttrium Barium Copper Oxide and magnesium diboride, and functional magnetic nanoadsorbents of maghemite and a multiphasic composite (iron oxide, hydroxyapatite and secondary phases). In the process, an in-detail protocol was designed and provided. It was concluded that the samples were successfully refined and that this work represents a fast introduction to the Rietveld method for which beginners can obtain good results while making correct interpretations of the whole refinement process.
format	article
author	Diego Alberto Flores Cano Anais Roxana Chino Quispe Renzo Rueda Vellasmin Joao Andre Ocampo Anticona Juan Carlos González Juan Adrián Ramos Guivar
author_facet	Diego Alberto Flores Cano Anais Roxana Chino Quispe Renzo Rueda Vellasmin Joao Andre Ocampo Anticona Juan Carlos González Juan Adrián Ramos Guivar
author_sort	Diego Alberto Flores Cano
title	Fifty years of Rietveld refinement: Methodology and guidelines in superconductors and functional magnetic nanoadsorbents
title_short	Fifty years of Rietveld refinement: Methodology and guidelines in superconductors and functional magnetic nanoadsorbents
title_full	Fifty years of Rietveld refinement: Methodology and guidelines in superconductors and functional magnetic nanoadsorbents
title_fullStr	Fifty years of Rietveld refinement: Methodology and guidelines in superconductors and functional magnetic nanoadsorbents
title_full_unstemmed	Fifty years of Rietveld refinement: Methodology and guidelines in superconductors and functional magnetic nanoadsorbents
title_sort	fifty years of rietveld refinement: methodology and guidelines in superconductors and functional magnetic nanoadsorbents
publisher	Instituto de Investigación de Física
publishDate	2021
url	https://doaj.org/article/9af7ce09cf6148608698dfd998ba9f48
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Fifty years of Rietveld refinement: Methodology and guidelines in superconductors and functional magnetic nanoadsorbents

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