Evolution of Face-Centered Cubic Ti Alloys Transformation by X-ray Diffraction Profile Analysis in Mechanical Alloying
Four titanium alloys (Ti-Ta, Ti-Ta-Sn, Ti-Ta-Mn, and Ti-Nb-Sn) were synthesized by mechanical alloying (MA) in a planetary mill in different times between 2 h and 100 h. The microstructure characterization was made by X-ray diffraction (XRD), in which the Rietveld method was applied to analyze the d...
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2021
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oai:doaj.org-article:9b0f304c83a14f5a8eccb3ab48df63fa2021-11-25T18:22:20ZEvolution of Face-Centered Cubic Ti Alloys Transformation by X-ray Diffraction Profile Analysis in Mechanical Alloying10.3390/met111118412075-4701https://doaj.org/article/9b0f304c83a14f5a8eccb3ab48df63fa2021-11-01T00:00:00Zhttps://www.mdpi.com/2075-4701/11/11/1841https://doaj.org/toc/2075-4701Four titanium alloys (Ti-Ta, Ti-Ta-Sn, Ti-Ta-Mn, and Ti-Nb-Sn) were synthesized by mechanical alloying (MA) in a planetary mill in different times between 2 h and 100 h. The microstructure characterization was made by X-ray diffraction (XRD), in which the Rietveld method was applied to analyze the diffraction patterns. The study demonstrated that after short milling times between 2 h and 30 h, the fraction of hexagonal close-packed (hcp) phase decreases; at the same time, the formation of body-centered cubic (bcc) and face-centered cubic (fcc) Ti phases are promoted. Additionally, after 30 h of MA, the full transformation of hcp-Ti was observed, and the bcc-Ti to fcc-Ti phase transformation took place until 50 h. The results suggest that the addition of Ta and Sn promotes the fcc-Ti phase formation, obtaining 100% of this phase at 50 h onwards, whereas Nb and Mn show the opposite effect.Edgar PioAriosto MedinaCarola MartínezFelipe Manuel Castro CerdaClaudio AguilarMDPI AGarticleX-ray diffractionmicrostructural evolutionface-centered cubicMining engineering. MetallurgyTN1-997ENMetals, Vol 11, Iss 1841, p 1841 (2021) |
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X-ray diffraction microstructural evolution face-centered cubic Mining engineering. Metallurgy TN1-997 |
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X-ray diffraction microstructural evolution face-centered cubic Mining engineering. Metallurgy TN1-997 Edgar Pio Ariosto Medina Carola Martínez Felipe Manuel Castro Cerda Claudio Aguilar Evolution of Face-Centered Cubic Ti Alloys Transformation by X-ray Diffraction Profile Analysis in Mechanical Alloying |
description |
Four titanium alloys (Ti-Ta, Ti-Ta-Sn, Ti-Ta-Mn, and Ti-Nb-Sn) were synthesized by mechanical alloying (MA) in a planetary mill in different times between 2 h and 100 h. The microstructure characterization was made by X-ray diffraction (XRD), in which the Rietveld method was applied to analyze the diffraction patterns. The study demonstrated that after short milling times between 2 h and 30 h, the fraction of hexagonal close-packed (hcp) phase decreases; at the same time, the formation of body-centered cubic (bcc) and face-centered cubic (fcc) Ti phases are promoted. Additionally, after 30 h of MA, the full transformation of hcp-Ti was observed, and the bcc-Ti to fcc-Ti phase transformation took place until 50 h. The results suggest that the addition of Ta and Sn promotes the fcc-Ti phase formation, obtaining 100% of this phase at 50 h onwards, whereas Nb and Mn show the opposite effect. |
format |
article |
author |
Edgar Pio Ariosto Medina Carola Martínez Felipe Manuel Castro Cerda Claudio Aguilar |
author_facet |
Edgar Pio Ariosto Medina Carola Martínez Felipe Manuel Castro Cerda Claudio Aguilar |
author_sort |
Edgar Pio |
title |
Evolution of Face-Centered Cubic Ti Alloys Transformation by X-ray Diffraction Profile Analysis in Mechanical Alloying |
title_short |
Evolution of Face-Centered Cubic Ti Alloys Transformation by X-ray Diffraction Profile Analysis in Mechanical Alloying |
title_full |
Evolution of Face-Centered Cubic Ti Alloys Transformation by X-ray Diffraction Profile Analysis in Mechanical Alloying |
title_fullStr |
Evolution of Face-Centered Cubic Ti Alloys Transformation by X-ray Diffraction Profile Analysis in Mechanical Alloying |
title_full_unstemmed |
Evolution of Face-Centered Cubic Ti Alloys Transformation by X-ray Diffraction Profile Analysis in Mechanical Alloying |
title_sort |
evolution of face-centered cubic ti alloys transformation by x-ray diffraction profile analysis in mechanical alloying |
publisher |
MDPI AG |
publishDate |
2021 |
url |
https://doaj.org/article/9b0f304c83a14f5a8eccb3ab48df63fa |
work_keys_str_mv |
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1718411274375659520 |