In Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level

This work summarizes the most commonly used in situ techniques for the study of Li-ion batteries from the micro to the atomic level. In situ analysis has attracted a great deal of interest owing to its ability to provide a wide range of information about the cycling behavior of batteries from the be...

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Autores principales:	Maryam Golozar, Raynald Gauvin, Karim Zaghib
Formato:	article
Lenguaje:	EN
Publicado:	MDPI AG 2021
Materias:	in situ in operando lithium-ion battery solid state SEM TEM Inorganic chemistry QD146-197
Acceso en línea:	https://doaj.org/article/a33125f6500340c8a9d4e031f677a5f2
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spelling	oai:doaj.org-article:a33125f6500340c8a9d4e031f677a5f22021-11-25T17:58:59ZIn Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level10.3390/inorganics91100852304-6740https://doaj.org/article/a33125f6500340c8a9d4e031f677a5f22021-11-01T00:00:00Zhttps://www.mdpi.com/2304-6740/9/11/85https://doaj.org/toc/2304-6740This work summarizes the most commonly used in situ techniques for the study of Li-ion batteries from the micro to the atomic level. In situ analysis has attracted a great deal of interest owing to its ability to provide a wide range of information about the cycling behavior of batteries from the beginning until the end of cycling. The in situ techniques that are covered are: X-ray diffraction (XRD), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), and Scanning Transmission Electron Microscopy (STEM). An optimized setup is required to be able to use any of these in situ techniques in battery applications. Depending on the type of data required, the available setup, and the type of battery, more than one of these techniques might be needed. This study organizes these techniques from the micro to the atomic level, and shows the types of data that can be obtained using these techniques, their advantages and their challenges, and possible strategies for overcoming these challenges.Maryam GolozarRaynald GauvinKarim ZaghibMDPI AGarticlein situin operandolithium-ion batterysolid stateSEMTEMInorganic chemistryQD146-197ENInorganics, Vol 9, Iss 85, p 85 (2021)
institution	DOAJ
collection	DOAJ
language	EN
topic	in situ in operando lithium-ion battery solid state SEM TEM Inorganic chemistry QD146-197
spellingShingle	in situ in operando lithium-ion battery solid state SEM TEM Inorganic chemistry QD146-197 Maryam Golozar Raynald Gauvin Karim Zaghib In Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level
description	This work summarizes the most commonly used in situ techniques for the study of Li-ion batteries from the micro to the atomic level. In situ analysis has attracted a great deal of interest owing to its ability to provide a wide range of information about the cycling behavior of batteries from the beginning until the end of cycling. The in situ techniques that are covered are: X-ray diffraction (XRD), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), and Scanning Transmission Electron Microscopy (STEM). An optimized setup is required to be able to use any of these in situ techniques in battery applications. Depending on the type of data required, the available setup, and the type of battery, more than one of these techniques might be needed. This study organizes these techniques from the micro to the atomic level, and shows the types of data that can be obtained using these techniques, their advantages and their challenges, and possible strategies for overcoming these challenges.
format	article
author	Maryam Golozar Raynald Gauvin Karim Zaghib
author_facet	Maryam Golozar Raynald Gauvin Karim Zaghib
author_sort	Maryam Golozar
title	In Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level
title_short	In Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level
title_full	In Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level
title_fullStr	In Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level
title_full_unstemmed	In Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level
title_sort	in situ and in operando techniques to study li-ion and solid-state batteries: micro to atomic level
publisher	MDPI AG
publishDate	2021
url	https://doaj.org/article/a33125f6500340c8a9d4e031f677a5f2
work_keys_str_mv	AT maryamgolozar insituandinoperandotechniquestostudyliionandsolidstatebatteriesmicrotoatomiclevel AT raynaldgauvin insituandinoperandotechniquestostudyliionandsolidstatebatteriesmicrotoatomiclevel AT karimzaghib insituandinoperandotechniquestostudyliionandsolidstatebatteriesmicrotoatomiclevel
_version_	1718411764054360064

In Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level

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