Comparison between Hydrofluoric Acid and Single-Component Primer as Conditioners on Resin Cement Adhesion to Lithium Silicate and Lithium Disilicate Glass Ceramics

This study aimed at evaluating the effects of different surface conditionings on the microshear bond strength (µSBS) of a self-adhesive resin cement to VITA Suprinity (ZLS) and IPS e.max CAD (LD). Three surface conditioning protocols were performed on ZLS and LD before luting with a self-adhesive re...

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Autores principales: Alessandro Vichi, Riccardo Fabian Fonzar, Michele Carrabba, Chris Louca, Nicola Scotti, Claudia Mazzitelli, Lorenzo Breschi, Cecilia Goracci
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Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:a36de27a055d43dcb7c8d16512c4760b2021-11-25T18:13:28ZComparison between Hydrofluoric Acid and Single-Component Primer as Conditioners on Resin Cement Adhesion to Lithium Silicate and Lithium Disilicate Glass Ceramics10.3390/ma142267761996-1944https://doaj.org/article/a36de27a055d43dcb7c8d16512c4760b2021-11-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/22/6776https://doaj.org/toc/1996-1944This study aimed at evaluating the effects of different surface conditionings on the microshear bond strength (µSBS) of a self-adhesive resin cement to VITA Suprinity (ZLS) and IPS e.max CAD (LD). Three surface conditioning protocols were performed on ZLS and LD before luting with a self-adhesive resin cement (RelyX Unicem 2, RXU): hydrofluoric acid (HF), HF + silane (HF + S), or Monobond Etch & Prime (EP). In each group, 15 cylindrical buildups of RXU were prepared on five milled bars and submitted to a µSBS test. Data were statistically analyzed with two-way ANOVA and Tukey’s post hoc test (<i>p</i> < 0.05). Failure modes were recorded and classified as adhesive, mixed, cohesive in resin, or ceramic, and statistically analyzed with Fisher’s exact test (<i>p</i> = 0.05). One additional bar per group was used for the morphological characterization of the conditioned surface by means of SEM. The material per se did not significantly influence adhesion (<i>p</i> = 0.744). Conditioning protocol was a significant factor: EP yielded significantly higher μSBS than HF (<i>p</i> = 0.005), while no significant differences emerged between EP and HF + S (<i>p</i> = 0.107), or HF + S and HF (<i>p</i> = 0.387). The material-conditioning protocol interaction was not statistically significant (<i>p</i> = 0.109). Significant intergroup differences were found in distribution of failure modes: mixed failures were predominant in the ZLS/EP group, while the other groups showed a prevalence of adhesive failures. The self-etching primer showed promising results in terms of immediate bond strength of a self-adhesive resin cement to lithium-silica-based glass ceramics, suggesting its alternative use to hydrofluoric acid and silane conditioning protocols.Alessandro VichiRiccardo Fabian FonzarMichele CarrabbaChris LoucaNicola ScottiClaudia MazzitelliLorenzo BreschiCecilia GoracciMDPI AGarticleVITA Suprinitye.max CADlithium disilicatelithium silicatehydrofluoric acidsilaneTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6776, p 6776 (2021)
institution DOAJ
collection DOAJ
language EN
topic VITA Suprinity
e.max CAD
lithium disilicate
lithium silicate
hydrofluoric acid
silane
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
spellingShingle VITA Suprinity
e.max CAD
lithium disilicate
lithium silicate
hydrofluoric acid
silane
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
Alessandro Vichi
Riccardo Fabian Fonzar
Michele Carrabba
Chris Louca
Nicola Scotti
Claudia Mazzitelli
Lorenzo Breschi
Cecilia Goracci
Comparison between Hydrofluoric Acid and Single-Component Primer as Conditioners on Resin Cement Adhesion to Lithium Silicate and Lithium Disilicate Glass Ceramics
description This study aimed at evaluating the effects of different surface conditionings on the microshear bond strength (µSBS) of a self-adhesive resin cement to VITA Suprinity (ZLS) and IPS e.max CAD (LD). Three surface conditioning protocols were performed on ZLS and LD before luting with a self-adhesive resin cement (RelyX Unicem 2, RXU): hydrofluoric acid (HF), HF + silane (HF + S), or Monobond Etch & Prime (EP). In each group, 15 cylindrical buildups of RXU were prepared on five milled bars and submitted to a µSBS test. Data were statistically analyzed with two-way ANOVA and Tukey’s post hoc test (<i>p</i> < 0.05). Failure modes were recorded and classified as adhesive, mixed, cohesive in resin, or ceramic, and statistically analyzed with Fisher’s exact test (<i>p</i> = 0.05). One additional bar per group was used for the morphological characterization of the conditioned surface by means of SEM. The material per se did not significantly influence adhesion (<i>p</i> = 0.744). Conditioning protocol was a significant factor: EP yielded significantly higher μSBS than HF (<i>p</i> = 0.005), while no significant differences emerged between EP and HF + S (<i>p</i> = 0.107), or HF + S and HF (<i>p</i> = 0.387). The material-conditioning protocol interaction was not statistically significant (<i>p</i> = 0.109). Significant intergroup differences were found in distribution of failure modes: mixed failures were predominant in the ZLS/EP group, while the other groups showed a prevalence of adhesive failures. The self-etching primer showed promising results in terms of immediate bond strength of a self-adhesive resin cement to lithium-silica-based glass ceramics, suggesting its alternative use to hydrofluoric acid and silane conditioning protocols.
format article
author Alessandro Vichi
Riccardo Fabian Fonzar
Michele Carrabba
Chris Louca
Nicola Scotti
Claudia Mazzitelli
Lorenzo Breschi
Cecilia Goracci
author_facet Alessandro Vichi
Riccardo Fabian Fonzar
Michele Carrabba
Chris Louca
Nicola Scotti
Claudia Mazzitelli
Lorenzo Breschi
Cecilia Goracci
author_sort Alessandro Vichi
title Comparison between Hydrofluoric Acid and Single-Component Primer as Conditioners on Resin Cement Adhesion to Lithium Silicate and Lithium Disilicate Glass Ceramics
title_short Comparison between Hydrofluoric Acid and Single-Component Primer as Conditioners on Resin Cement Adhesion to Lithium Silicate and Lithium Disilicate Glass Ceramics
title_full Comparison between Hydrofluoric Acid and Single-Component Primer as Conditioners on Resin Cement Adhesion to Lithium Silicate and Lithium Disilicate Glass Ceramics
title_fullStr Comparison between Hydrofluoric Acid and Single-Component Primer as Conditioners on Resin Cement Adhesion to Lithium Silicate and Lithium Disilicate Glass Ceramics
title_full_unstemmed Comparison between Hydrofluoric Acid and Single-Component Primer as Conditioners on Resin Cement Adhesion to Lithium Silicate and Lithium Disilicate Glass Ceramics
title_sort comparison between hydrofluoric acid and single-component primer as conditioners on resin cement adhesion to lithium silicate and lithium disilicate glass ceramics
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/a36de27a055d43dcb7c8d16512c4760b
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