Ag2CO3 containing magnetic nanocomposite as a powerful and recoverable catalyst for Knoevenagel condensation
Abstract In this paper, the synthesis, characterization and catalytic application of a novel magnetic silica-supported Ag2CO3 (MS/Ag2CO3) with core–shell structure are developed. The MS/Ag2CO3 nanocomposite was prepared through chemical modification of magnetic MS nanoparticles with AgNO3 under alka...
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2021
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oai:doaj.org-article:a9beb2f1542b42a38e3d3536f5a15eae2021-12-02T15:14:37ZAg2CO3 containing magnetic nanocomposite as a powerful and recoverable catalyst for Knoevenagel condensation10.1038/s41598-021-98287-z2045-2322https://doaj.org/article/a9beb2f1542b42a38e3d3536f5a15eae2021-09-01T00:00:00Zhttps://doi.org/10.1038/s41598-021-98287-zhttps://doaj.org/toc/2045-2322Abstract In this paper, the synthesis, characterization and catalytic application of a novel magnetic silica-supported Ag2CO3 (MS/Ag2CO3) with core–shell structure are developed. The MS/Ag2CO3 nanocomposite was prepared through chemical modification of magnetic MS nanoparticles with AgNO3 under alkaline conditions. The structure, chemical composition and magnetic properties of MS/Ag2CO3 were investigated by using VSM, PXRD, FT-IR, EDX and SEM techniques. The MS/Ag2CO3 nanocomposite was used as an effective catalyst for the Knoevenagel condensation under solvent-free conditions at 60 °C in an ultrasonic bath. The recovery and leaching tests were performed to study the nature of the MS/Ag2CO3 catalyst under applied conditions.Fatemeh KarimkhahDawood ElhamifarMasoumeh ShakerNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 11, Iss 1, Pp 1-11 (2021) |
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Medicine R Science Q Fatemeh Karimkhah Dawood Elhamifar Masoumeh Shaker Ag2CO3 containing magnetic nanocomposite as a powerful and recoverable catalyst for Knoevenagel condensation |
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Abstract In this paper, the synthesis, characterization and catalytic application of a novel magnetic silica-supported Ag2CO3 (MS/Ag2CO3) with core–shell structure are developed. The MS/Ag2CO3 nanocomposite was prepared through chemical modification of magnetic MS nanoparticles with AgNO3 under alkaline conditions. The structure, chemical composition and magnetic properties of MS/Ag2CO3 were investigated by using VSM, PXRD, FT-IR, EDX and SEM techniques. The MS/Ag2CO3 nanocomposite was used as an effective catalyst for the Knoevenagel condensation under solvent-free conditions at 60 °C in an ultrasonic bath. The recovery and leaching tests were performed to study the nature of the MS/Ag2CO3 catalyst under applied conditions. |
format |
article |
author |
Fatemeh Karimkhah Dawood Elhamifar Masoumeh Shaker |
author_facet |
Fatemeh Karimkhah Dawood Elhamifar Masoumeh Shaker |
author_sort |
Fatemeh Karimkhah |
title |
Ag2CO3 containing magnetic nanocomposite as a powerful and recoverable catalyst for Knoevenagel condensation |
title_short |
Ag2CO3 containing magnetic nanocomposite as a powerful and recoverable catalyst for Knoevenagel condensation |
title_full |
Ag2CO3 containing magnetic nanocomposite as a powerful and recoverable catalyst for Knoevenagel condensation |
title_fullStr |
Ag2CO3 containing magnetic nanocomposite as a powerful and recoverable catalyst for Knoevenagel condensation |
title_full_unstemmed |
Ag2CO3 containing magnetic nanocomposite as a powerful and recoverable catalyst for Knoevenagel condensation |
title_sort |
ag2co3 containing magnetic nanocomposite as a powerful and recoverable catalyst for knoevenagel condensation |
publisher |
Nature Portfolio |
publishDate |
2021 |
url |
https://doaj.org/article/a9beb2f1542b42a38e3d3536f5a15eae |
work_keys_str_mv |
AT fatemehkarimkhah ag2co3containingmagneticnanocompositeasapowerfulandrecoverablecatalystforknoevenagelcondensation AT dawoodelhamifar ag2co3containingmagneticnanocompositeasapowerfulandrecoverablecatalystforknoevenagelcondensation AT masoumehshaker ag2co3containingmagneticnanocompositeasapowerfulandrecoverablecatalystforknoevenagelcondensation |
_version_ |
1718387591555842048 |