Tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying

Abstract We demonstrated the design of pre-additive manufacturing microalloying elements in tuning the microstructure of iron (Fe)-based alloys for their tunable mechanical properties. We tailored the microalloying stoichiometry of the feedstock to control the grain sizes of the metallic alloy syste...

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Autores principales: Chih-Chieh Huang, Tu-Ngoc Lam, Lia Amalia, Kuan-Hung Chen, Kuo-Yi Yang, M. Rifai Muslih, Sudhanshu Shekhar Singh, Pei-I. Tsai, Yuan-Tzu Lee, Jayant Jain, Soo Yeol Lee, Hong-Jen Lai, Wei-Chin Huang, San-Yuan Chen, E-Wen Huang
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Publicado: Nature Portfolio 2021
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spelling oai:doaj.org-article:aed63981a0bc4f7490276a9b62cc91452021-12-02T14:29:09ZTailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying10.1038/s41598-021-89022-92045-2322https://doaj.org/article/aed63981a0bc4f7490276a9b62cc91452021-05-01T00:00:00Zhttps://doi.org/10.1038/s41598-021-89022-9https://doaj.org/toc/2045-2322Abstract We demonstrated the design of pre-additive manufacturing microalloying elements in tuning the microstructure of iron (Fe)-based alloys for their tunable mechanical properties. We tailored the microalloying stoichiometry of the feedstock to control the grain sizes of the metallic alloy systems. Two specific microalloying stoichiometries were reported, namely biodegradable iron powder with 99.5% purity (BDFe) and that with 98.5% (BDFe-Mo). Compared with the BDFe, the BDFe-Mo powder was found to have lower coefficient of thermal expansion (CTE) value and better oxidation resistance during consecutive heating and cooling cycles. The selective laser melting (SLM)-built BDFe-Mo exhibited high ultimate tensile strength (UTS) of 1200 MPa and fair elongation of 13.5%, while the SLM-built BDFe alloy revealed a much lower UTS of 495 MPa and a relatively better elongation of 17.5%, indicating the strength enhancement compared with the other biodegradable systems. Such an enhanced mechanical behavior in the BDFe-Mo was assigned to the dominant mechanism of ferrite grain refinement coupled with precipitate strengthening. Our findings suggest the tunability of outstanding strength-ductility combination by tailoring the pre-additive manufacturing microalloying elements with their proper concentrations.Chih-Chieh HuangTu-Ngoc LamLia AmaliaKuan-Hung ChenKuo-Yi YangM. Rifai MuslihSudhanshu Shekhar SinghPei-I. TsaiYuan-Tzu LeeJayant JainSoo Yeol LeeHong-Jen LaiWei-Chin HuangSan-Yuan ChenE-Wen HuangNature PortfolioarticleMedicineRScienceQENScientific Reports, Vol 11, Iss 1, Pp 1-12 (2021)
institution DOAJ
collection DOAJ
language EN
topic Medicine
R
Science
Q
spellingShingle Medicine
R
Science
Q
Chih-Chieh Huang
Tu-Ngoc Lam
Lia Amalia
Kuan-Hung Chen
Kuo-Yi Yang
M. Rifai Muslih
Sudhanshu Shekhar Singh
Pei-I. Tsai
Yuan-Tzu Lee
Jayant Jain
Soo Yeol Lee
Hong-Jen Lai
Wei-Chin Huang
San-Yuan Chen
E-Wen Huang
Tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying
description Abstract We demonstrated the design of pre-additive manufacturing microalloying elements in tuning the microstructure of iron (Fe)-based alloys for their tunable mechanical properties. We tailored the microalloying stoichiometry of the feedstock to control the grain sizes of the metallic alloy systems. Two specific microalloying stoichiometries were reported, namely biodegradable iron powder with 99.5% purity (BDFe) and that with 98.5% (BDFe-Mo). Compared with the BDFe, the BDFe-Mo powder was found to have lower coefficient of thermal expansion (CTE) value and better oxidation resistance during consecutive heating and cooling cycles. The selective laser melting (SLM)-built BDFe-Mo exhibited high ultimate tensile strength (UTS) of 1200 MPa and fair elongation of 13.5%, while the SLM-built BDFe alloy revealed a much lower UTS of 495 MPa and a relatively better elongation of 17.5%, indicating the strength enhancement compared with the other biodegradable systems. Such an enhanced mechanical behavior in the BDFe-Mo was assigned to the dominant mechanism of ferrite grain refinement coupled with precipitate strengthening. Our findings suggest the tunability of outstanding strength-ductility combination by tailoring the pre-additive manufacturing microalloying elements with their proper concentrations.
format article
author Chih-Chieh Huang
Tu-Ngoc Lam
Lia Amalia
Kuan-Hung Chen
Kuo-Yi Yang
M. Rifai Muslih
Sudhanshu Shekhar Singh
Pei-I. Tsai
Yuan-Tzu Lee
Jayant Jain
Soo Yeol Lee
Hong-Jen Lai
Wei-Chin Huang
San-Yuan Chen
E-Wen Huang
author_facet Chih-Chieh Huang
Tu-Ngoc Lam
Lia Amalia
Kuan-Hung Chen
Kuo-Yi Yang
M. Rifai Muslih
Sudhanshu Shekhar Singh
Pei-I. Tsai
Yuan-Tzu Lee
Jayant Jain
Soo Yeol Lee
Hong-Jen Lai
Wei-Chin Huang
San-Yuan Chen
E-Wen Huang
author_sort Chih-Chieh Huang
title Tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying
title_short Tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying
title_full Tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying
title_fullStr Tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying
title_full_unstemmed Tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying
title_sort tailoring grain sizes of the biodegradable iron-based alloys by pre-additive manufacturing microalloying
publisher Nature Portfolio
publishDate 2021
url https://doaj.org/article/aed63981a0bc4f7490276a9b62cc9145
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