Densification method of air-plasma-sprayed environmental barrier coatings achieved by pre-heat treatment
High density of the top coat of environmental barrier coatings (EBC) is important for ensuring its performance in water vapor environment, which is also significant for prolonging service lifetime of SiC<sub>f</sub>/SiC aero-engine hot components. In this work, densification of the top c...
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Journal of Materials Engineering
2021
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oai:doaj.org-article:af0b5b10b1074a0bac02ac47a916f8022021-11-12T03:01:54ZDensification method of air-plasma-sprayed environmental barrier coatings achieved by pre-heat treatment1001-438110.11868/j.issn.1001-4381.2020.001156https://doaj.org/article/af0b5b10b1074a0bac02ac47a916f8022021-11-01T00:00:00Zhttp://jme.biam.ac.cn/CN/10.11868/j.issn.1001-4381.2020.001156https://doaj.org/toc/1001-4381High density of the top coat of environmental barrier coatings (EBC) is important for ensuring its performance in water vapor environment, which is also significant for prolonging service lifetime of SiC<sub>f</sub>/SiC aero-engine hot components. In this work, densification of the top coat of EBC was achieved by pre-heat treatment. In detail, the as-sprayed porous Yb<sub>2</sub>SiO<sub>5</sub> coatings were heat-treated at the high temperature of 1250℃ to 1450℃, which improve the density significantly. Changes in microstructure and mechanical properties during the pre-heat treatment were studied by classifying defects into different types. The processes of defects-healing were observed, and the mechanism responsible for coating densification was revealed. Results show that the porosity of as-sprayed Yb<sub>2</sub>SiO<sub>5</sub> coating is high due to the existence of three types of micro-defects, including two-dimensional (2D) inter-splat pores, 2D intra-splat cracks and three-dimensional (3D) spherical pores. During the pre-heat treatment process, 2D defects are healed to be reduced in a large amount in a short duration, while the 3D spherical pores seem unchanged. The mechanism of defects-healing in the heat treatment process is that grain growth inside the coating makes surface of the pores rough, which leads to multiple bridge-connection of 2D pores. As a result, the original continuous defects are divided into several sections and are further spheroidized. The method of pre-heat treatment for APS-EBC would make a fundamental contribution to its further engineering application.YANG BoLI Guang-rongXU TongYANG Guan-junJournal of Materials Engineeringarticleenvironmental barrier coatingair plasma spraypre-heat-treatmentdefects-healingdensificationMaterials of engineering and construction. Mechanics of materialsTA401-492ZHJournal of Materials Engineering, Vol 49, Iss 11, Pp 116-124 (2021) |
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environmental barrier coating air plasma spray pre-heat-treatment defects-healing densification Materials of engineering and construction. Mechanics of materials TA401-492 |
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environmental barrier coating air plasma spray pre-heat-treatment defects-healing densification Materials of engineering and construction. Mechanics of materials TA401-492 YANG Bo LI Guang-rong XU Tong YANG Guan-jun Densification method of air-plasma-sprayed environmental barrier coatings achieved by pre-heat treatment |
description |
High density of the top coat of environmental barrier coatings (EBC) is important for ensuring its performance in water vapor environment, which is also significant for prolonging service lifetime of SiC<sub>f</sub>/SiC aero-engine hot components. In this work, densification of the top coat of EBC was achieved by pre-heat treatment. In detail, the as-sprayed porous Yb<sub>2</sub>SiO<sub>5</sub> coatings were heat-treated at the high temperature of 1250℃ to 1450℃, which improve the density significantly. Changes in microstructure and mechanical properties during the pre-heat treatment were studied by classifying defects into different types. The processes of defects-healing were observed, and the mechanism responsible for coating densification was revealed. Results show that the porosity of as-sprayed Yb<sub>2</sub>SiO<sub>5</sub> coating is high due to the existence of three types of micro-defects, including two-dimensional (2D) inter-splat pores, 2D intra-splat cracks and three-dimensional (3D) spherical pores. During the pre-heat treatment process, 2D defects are healed to be reduced in a large amount in a short duration, while the 3D spherical pores seem unchanged. The mechanism of defects-healing in the heat treatment process is that grain growth inside the coating makes surface of the pores rough, which leads to multiple bridge-connection of 2D pores. As a result, the original continuous defects are divided into several sections and are further spheroidized. The method of pre-heat treatment for APS-EBC would make a fundamental contribution to its further engineering application. |
format |
article |
author |
YANG Bo LI Guang-rong XU Tong YANG Guan-jun |
author_facet |
YANG Bo LI Guang-rong XU Tong YANG Guan-jun |
author_sort |
YANG Bo |
title |
Densification method of air-plasma-sprayed environmental barrier coatings achieved by pre-heat treatment |
title_short |
Densification method of air-plasma-sprayed environmental barrier coatings achieved by pre-heat treatment |
title_full |
Densification method of air-plasma-sprayed environmental barrier coatings achieved by pre-heat treatment |
title_fullStr |
Densification method of air-plasma-sprayed environmental barrier coatings achieved by pre-heat treatment |
title_full_unstemmed |
Densification method of air-plasma-sprayed environmental barrier coatings achieved by pre-heat treatment |
title_sort |
densification method of air-plasma-sprayed environmental barrier coatings achieved by pre-heat treatment |
publisher |
Journal of Materials Engineering |
publishDate |
2021 |
url |
https://doaj.org/article/af0b5b10b1074a0bac02ac47a916f802 |
work_keys_str_mv |
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