Preliminary Studies on Rare Elements Addition and Effect on Oxidation Behaviour of Pack Cementation Coatings Deposited on Variety of Steels at High Temperature

The aim of the paper was to investigate the air oxidation behaviour of pack aluminised steels exposed at 650 °C for 1000 h in static natural air atmosphere. The pack coatings were doped by rare elements such as gadolinium (Gd), cerium oxide (CeO<sub>2</sub>), and lanthanum (La) in order...

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Autores principales: Tomasz Dudziak, Ewa Rząd, Tomasz Polczyk, Katrin Jahns, Wojciech Polkowski, Adelajda Polkowska, Michal Wójcicki
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Lenguaje:EN
Publicado: MDPI AG 2021
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spelling oai:doaj.org-article:b9ae7e4ff7d14c749c764babce45ad662021-11-25T18:13:41ZPreliminary Studies on Rare Elements Addition and Effect on Oxidation Behaviour of Pack Cementation Coatings Deposited on Variety of Steels at High Temperature10.3390/ma142268011996-1944https://doaj.org/article/b9ae7e4ff7d14c749c764babce45ad662021-11-01T00:00:00Zhttps://www.mdpi.com/1996-1944/14/22/6801https://doaj.org/toc/1996-1944The aim of the paper was to investigate the air oxidation behaviour of pack aluminised steels exposed at 650 °C for 1000 h in static natural air atmosphere. The pack coatings were doped by rare elements such as gadolinium (Gd), cerium oxide (CeO<sub>2</sub>), and lanthanum (La) in order to enhance the corrosion resistance and plasticity of the deposited layers. In this work, the following steels were used: 16M, T91, VM12, Super 304H, and finally SANICRO25. The results indicated a much higher corrosion resistance in the coated 16M, T91, and VM12 steels; the steels with a higher Cr content than 16 wt % Cr indicated a better behaviour in the uncoated state than in the coated state. However, the observed difference in mass gain between the uncoated and the coated austenitic steels was not enormous. Furthermore, the addition of RE elements to the coating showed some effect in terms of coating thicknesses and differences in the layer structures. The materials prior to testing and after the exposure were investigated using XRD, the SEM X-ray maps with an EDS instrument were used for particular samples to evaluate the phase identifications, element concentrations, microstructure, and chemical composition.Tomasz DudziakEwa RządTomasz PolczykKatrin JahnsWojciech PolkowskiAdelajda PolkowskaMichal WójcickiMDPI AGarticlepack cementationoxidationrare elementsXRDSEMEDSTechnologyTElectrical engineering. Electronics. Nuclear engineeringTK1-9971Engineering (General). Civil engineering (General)TA1-2040MicroscopyQH201-278.5Descriptive and experimental mechanicsQC120-168.85ENMaterials, Vol 14, Iss 6801, p 6801 (2021)
institution DOAJ
collection DOAJ
language EN
topic pack cementation
oxidation
rare elements
XRD
SEM
EDS
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
spellingShingle pack cementation
oxidation
rare elements
XRD
SEM
EDS
Technology
T
Electrical engineering. Electronics. Nuclear engineering
TK1-9971
Engineering (General). Civil engineering (General)
TA1-2040
Microscopy
QH201-278.5
Descriptive and experimental mechanics
QC120-168.85
Tomasz Dudziak
Ewa Rząd
Tomasz Polczyk
Katrin Jahns
Wojciech Polkowski
Adelajda Polkowska
Michal Wójcicki
Preliminary Studies on Rare Elements Addition and Effect on Oxidation Behaviour of Pack Cementation Coatings Deposited on Variety of Steels at High Temperature
description The aim of the paper was to investigate the air oxidation behaviour of pack aluminised steels exposed at 650 °C for 1000 h in static natural air atmosphere. The pack coatings were doped by rare elements such as gadolinium (Gd), cerium oxide (CeO<sub>2</sub>), and lanthanum (La) in order to enhance the corrosion resistance and plasticity of the deposited layers. In this work, the following steels were used: 16M, T91, VM12, Super 304H, and finally SANICRO25. The results indicated a much higher corrosion resistance in the coated 16M, T91, and VM12 steels; the steels with a higher Cr content than 16 wt % Cr indicated a better behaviour in the uncoated state than in the coated state. However, the observed difference in mass gain between the uncoated and the coated austenitic steels was not enormous. Furthermore, the addition of RE elements to the coating showed some effect in terms of coating thicknesses and differences in the layer structures. The materials prior to testing and after the exposure were investigated using XRD, the SEM X-ray maps with an EDS instrument were used for particular samples to evaluate the phase identifications, element concentrations, microstructure, and chemical composition.
format article
author Tomasz Dudziak
Ewa Rząd
Tomasz Polczyk
Katrin Jahns
Wojciech Polkowski
Adelajda Polkowska
Michal Wójcicki
author_facet Tomasz Dudziak
Ewa Rząd
Tomasz Polczyk
Katrin Jahns
Wojciech Polkowski
Adelajda Polkowska
Michal Wójcicki
author_sort Tomasz Dudziak
title Preliminary Studies on Rare Elements Addition and Effect on Oxidation Behaviour of Pack Cementation Coatings Deposited on Variety of Steels at High Temperature
title_short Preliminary Studies on Rare Elements Addition and Effect on Oxidation Behaviour of Pack Cementation Coatings Deposited on Variety of Steels at High Temperature
title_full Preliminary Studies on Rare Elements Addition and Effect on Oxidation Behaviour of Pack Cementation Coatings Deposited on Variety of Steels at High Temperature
title_fullStr Preliminary Studies on Rare Elements Addition and Effect on Oxidation Behaviour of Pack Cementation Coatings Deposited on Variety of Steels at High Temperature
title_full_unstemmed Preliminary Studies on Rare Elements Addition and Effect on Oxidation Behaviour of Pack Cementation Coatings Deposited on Variety of Steels at High Temperature
title_sort preliminary studies on rare elements addition and effect on oxidation behaviour of pack cementation coatings deposited on variety of steels at high temperature
publisher MDPI AG
publishDate 2021
url https://doaj.org/article/b9ae7e4ff7d14c749c764babce45ad66
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