Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation

Instrumented nanoindentation (NI) was used to examine the viscoelastic properties of poly(methyl methacrylate) (PMMA) as an amorphous polymer model. An evaluation combining adhesive contact and empiric spring–dashpot models has been applied to obtain the instantaneous elastic modulus E0 and the infi...

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Autores principales: Petra Christöfl, Caterina Czibula, Michael Berer, Gernot Oreski, Christian Teichert, Gerald Pinter
Formato: article
Lenguaje:EN
Publicado: Elsevier 2021
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AFM
Acceso en línea:https://doaj.org/article/b9e3f16d34ab42949a0bc671645a860f
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spelling oai:doaj.org-article:b9e3f16d34ab42949a0bc671645a860f2021-11-24T04:25:36ZComprehensive investigation of the viscoelastic properties of PMMA by nanoindentation0142-941810.1016/j.polymertesting.2020.106978https://doaj.org/article/b9e3f16d34ab42949a0bc671645a860f2021-01-01T00:00:00Zhttp://www.sciencedirect.com/science/article/pii/S0142941820322078https://doaj.org/toc/0142-9418Instrumented nanoindentation (NI) was used to examine the viscoelastic properties of poly(methyl methacrylate) (PMMA) as an amorphous polymer model. An evaluation combining adhesive contact and empiric spring–dashpot models has been applied to obtain the instantaneous elastic modulus E0 and the infinitely elastic modulus E∞ from nanoindentation creep curves. The value of E0 has been compared to moduli obtained with atomic force microscopy-based nanoindentation (AFM-NI) and compression tests. Furthermore, the elastic modulus has been evaluated by the method introduced by Oliver and Pharr (O&P) for the NI and AFM-NI results. Comparison of the elastic modulus E0 from the creep measurements of NI and AFM-NI to compression tests reveals good agreement of the results. However, only the O&P based AFM-NI results yield to lower values.Petra ChristöflCaterina CzibulaMichael BererGernot OreskiChristian TeichertGerald PinterElsevierarticleNanoindentationAmorphousCreepAFMCompression testPolymers and polymer manufactureTP1080-1185ENPolymer Testing, Vol 93, Iss , Pp 106978- (2021)
institution DOAJ
collection DOAJ
language EN
topic Nanoindentation
Amorphous
Creep
AFM
Compression test
Polymers and polymer manufacture
TP1080-1185
spellingShingle Nanoindentation
Amorphous
Creep
AFM
Compression test
Polymers and polymer manufacture
TP1080-1185
Petra Christöfl
Caterina Czibula
Michael Berer
Gernot Oreski
Christian Teichert
Gerald Pinter
Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation
description Instrumented nanoindentation (NI) was used to examine the viscoelastic properties of poly(methyl methacrylate) (PMMA) as an amorphous polymer model. An evaluation combining adhesive contact and empiric spring–dashpot models has been applied to obtain the instantaneous elastic modulus E0 and the infinitely elastic modulus E∞ from nanoindentation creep curves. The value of E0 has been compared to moduli obtained with atomic force microscopy-based nanoindentation (AFM-NI) and compression tests. Furthermore, the elastic modulus has been evaluated by the method introduced by Oliver and Pharr (O&P) for the NI and AFM-NI results. Comparison of the elastic modulus E0 from the creep measurements of NI and AFM-NI to compression tests reveals good agreement of the results. However, only the O&P based AFM-NI results yield to lower values.
format article
author Petra Christöfl
Caterina Czibula
Michael Berer
Gernot Oreski
Christian Teichert
Gerald Pinter
author_facet Petra Christöfl
Caterina Czibula
Michael Berer
Gernot Oreski
Christian Teichert
Gerald Pinter
author_sort Petra Christöfl
title Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation
title_short Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation
title_full Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation
title_fullStr Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation
title_full_unstemmed Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation
title_sort comprehensive investigation of the viscoelastic properties of pmma by nanoindentation
publisher Elsevier
publishDate 2021
url https://doaj.org/article/b9e3f16d34ab42949a0bc671645a860f
work_keys_str_mv AT petrachristofl comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation
AT caterinaczibula comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation
AT michaelberer comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation
AT gernotoreski comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation
AT christianteichert comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation
AT geraldpinter comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation
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