Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation
Instrumented nanoindentation (NI) was used to examine the viscoelastic properties of poly(methyl methacrylate) (PMMA) as an amorphous polymer model. An evaluation combining adhesive contact and empiric spring–dashpot models has been applied to obtain the instantaneous elastic modulus E0 and the infi...
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2021
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oai:doaj.org-article:b9e3f16d34ab42949a0bc671645a860f2021-11-24T04:25:36ZComprehensive investigation of the viscoelastic properties of PMMA by nanoindentation0142-941810.1016/j.polymertesting.2020.106978https://doaj.org/article/b9e3f16d34ab42949a0bc671645a860f2021-01-01T00:00:00Zhttp://www.sciencedirect.com/science/article/pii/S0142941820322078https://doaj.org/toc/0142-9418Instrumented nanoindentation (NI) was used to examine the viscoelastic properties of poly(methyl methacrylate) (PMMA) as an amorphous polymer model. An evaluation combining adhesive contact and empiric spring–dashpot models has been applied to obtain the instantaneous elastic modulus E0 and the infinitely elastic modulus E∞ from nanoindentation creep curves. The value of E0 has been compared to moduli obtained with atomic force microscopy-based nanoindentation (AFM-NI) and compression tests. Furthermore, the elastic modulus has been evaluated by the method introduced by Oliver and Pharr (O&P) for the NI and AFM-NI results. Comparison of the elastic modulus E0 from the creep measurements of NI and AFM-NI to compression tests reveals good agreement of the results. However, only the O&P based AFM-NI results yield to lower values.Petra ChristöflCaterina CzibulaMichael BererGernot OreskiChristian TeichertGerald PinterElsevierarticleNanoindentationAmorphousCreepAFMCompression testPolymers and polymer manufactureTP1080-1185ENPolymer Testing, Vol 93, Iss , Pp 106978- (2021) |
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DOAJ |
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Nanoindentation Amorphous Creep AFM Compression test Polymers and polymer manufacture TP1080-1185 |
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Nanoindentation Amorphous Creep AFM Compression test Polymers and polymer manufacture TP1080-1185 Petra Christöfl Caterina Czibula Michael Berer Gernot Oreski Christian Teichert Gerald Pinter Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation |
description |
Instrumented nanoindentation (NI) was used to examine the viscoelastic properties of poly(methyl methacrylate) (PMMA) as an amorphous polymer model. An evaluation combining adhesive contact and empiric spring–dashpot models has been applied to obtain the instantaneous elastic modulus E0 and the infinitely elastic modulus E∞ from nanoindentation creep curves. The value of E0 has been compared to moduli obtained with atomic force microscopy-based nanoindentation (AFM-NI) and compression tests. Furthermore, the elastic modulus has been evaluated by the method introduced by Oliver and Pharr (O&P) for the NI and AFM-NI results. Comparison of the elastic modulus E0 from the creep measurements of NI and AFM-NI to compression tests reveals good agreement of the results. However, only the O&P based AFM-NI results yield to lower values. |
format |
article |
author |
Petra Christöfl Caterina Czibula Michael Berer Gernot Oreski Christian Teichert Gerald Pinter |
author_facet |
Petra Christöfl Caterina Czibula Michael Berer Gernot Oreski Christian Teichert Gerald Pinter |
author_sort |
Petra Christöfl |
title |
Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation |
title_short |
Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation |
title_full |
Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation |
title_fullStr |
Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation |
title_full_unstemmed |
Comprehensive investigation of the viscoelastic properties of PMMA by nanoindentation |
title_sort |
comprehensive investigation of the viscoelastic properties of pmma by nanoindentation |
publisher |
Elsevier |
publishDate |
2021 |
url |
https://doaj.org/article/b9e3f16d34ab42949a0bc671645a860f |
work_keys_str_mv |
AT petrachristofl comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation AT caterinaczibula comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation AT michaelberer comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation AT gernotoreski comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation AT christianteichert comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation AT geraldpinter comprehensiveinvestigationoftheviscoelasticpropertiesofpmmabynanoindentation |
_version_ |
1718415998119313408 |